• 제목/요약/키워드: SEM Micrographs

검색결과 137건 처리시간 0.033초

Preparation and Characterization of Ultra Thin TaN Films Prepared by RF Magnetron Sputtering

  • ;조현철;이기선
    • 한국재료학회:학술대회논문집
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    • 한국재료학회 2011년도 추계학술발표대회
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    • pp.32.1-32.1
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    • 2011
  • Ultra thin tantalum nitride (TaNx) films with various thicknesses (10 nm to 40 nm) have been deposited by rf magnetron sputtering technique on glass substrates. The as deposited films were systematically characterized by several analytical techniques such as X-ray diffraction, X-ray photoelectron spectroscopy, field emission scanning electron microscopy, atomic force microscopy, UV-Vis-NIR double beam spectrophotometer and four point probe method. From the XRD results, the as deposited films are in amorphous nature, irrespective of the film thicknesses. The films composition was changed greatly with increasing the film thickness. SEM micrographs exhibited the densely pack microstructure, and homogeneous surface covered by small size grains at lower thickness deposited films. The surface roughness of the films was linearly increases with increasing the films thickness, consequently the transmittance decreased. The absorption edge was shifted towards higher wavelength as the film thickness increases.

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무기계 방오기능성 혼화제를 사용한 콘크리트 특성에 관한 실험적 연구 (Experimental study on Properties of Concrete Using Inorganic Antifouling Agent)

  • 김연봉;강용식;이병기;김도수;길배수;남재현
    • 한국콘크리트학회:학술대회논문집
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    • 한국콘크리트학회 2004년도 춘계 학술발표회 제16권1호
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    • pp.604-607
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    • 2004
  • Concrete structures in the marine environment often deteriorate in the early stage of their service life because of contact with various aggressive conditions. In recent years, the study on the concrete in the marine environment are carried out to increase their service life. In this experimental study, the concrete specimens were prepared with various adding contents of inorganic antifouling agent$(0\~3.0wt\%)$ composed to some fluosilicate solution. For evaluatin of the physical and chemical properties of concretes containing inorganic antifouling agent, various tests such as setting time, slump loss, compressive strength, water absorption rate, freezing and thawing resistance and SEM micrographs of concrete, were conducted. As the results, physical and chemical properties of concretes were improved with an adding of inorganic antifouling agent. From the results of various tests, the optimal adding contents of antifouling agent was $1.0wt\%$.

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반복 사용된 치과용 비귀금속에 의한 주조체의 식각표면에 대한 연구 (The Etched Surface of the Repeatedly Cast Dental Base Metal Alloy)

  • 이선형
    • 대한치과의사협회지
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    • 제23권7호통권194호
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    • pp.577-583
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    • 1985
  • The purpose of this investigation was to evaluate scanning electron micrographs of repeatedly cast base metal alloy. For this study two Ni-Cr-Be alloys were used; Rexillium III and Verabond. They were repeatedly cast without addition o new alloy melting with an electric resistant furnace (Castron 8, Yoshida dental equipment Mfg.Co.). They were etched with 10% H₂SO₄ Sol. at 300mA/㎠ for 3 minutes with the use of metal etching unit Oxyetch (OXY dental product Inc.), and ultrasonic cleaning in 18% HC1 Sol. was done. Etched surfaces were examined under a SEM at x 200 and x 750. The surfaces are shown in legends.

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Pantel/apsis Species (Copepoda, Pontellidae) in the Korean Waters, with Notes on the Female Genital Structures and Their Zoogeography

  • Jeong, Hyeon-Gyeong;Suh, Hae-Lip;Soh, Ho-Young
    • Animal cells and systems
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    • 제13권2호
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    • pp.187-203
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    • 2009
  • Neustonic calanoid copepods were collected at the South Sea of Korea using a David-Hempel neuston net. Four Pantel/apsis species (P. armata Giesbrecht, P. rega/is Dana, P. vil/asa Brady and P. yamadae Mori) were identified and the former three species were first recorded in the Korea. We present redescription of the four species with SEM micrographs of female genitalia. Female genital structure is species-specific and can be very useful for species classification in the genus Pantel/apsis. Also we discuss zoogeography of Pantel/apsis species and provide with a key to the species hitherto known in the Korean waters.

Fretting Wear Mechanisms of Zircaloy-4 and Inconel 600 Contact in Air

  • Kim, Tae-Hyung;Kim, Seock-Sam
    • Journal of Mechanical Science and Technology
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    • 제15권9호
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    • pp.1274-1280
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    • 2001
  • The fretting wear behavior of the contact between Zircaloy-4 tube and Inconel 600, which are used as the fuel rod cladding and grid, respectively, in PWR nuclear power plants was investigated in air. In the study, number of cycles, slip amplitude and normal load were selected as the main factors of fretting wear. The results indicated that wear increased with load, slip amplitude and number of cycles but was affected mainly by the slip amplitude. SEM micrographs revealed the characteristics of fretting wear features on the surface of the specimens such as stick, partial slip and gross slip which depended on the slip amplitude. It was found that fretting wear was caused by the crack generation along the stick-slip boundaries due to the accumulation of plastic flow at small slip amplitudes and by abrasive wear in the entire contact area at high slip amplitudes.

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SiO2/ZnS:Cu/ZnS Triplex Layer Coatings for Phosphorescence Enhancement

  • Zhang, Wen-Tao;Lee, Hong-Ro
    • 한국표면공학회지
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    • 제41권4호
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    • pp.169-173
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    • 2008
  • The objective of this study is to coat the $SiO_2$ layer uniformly on the ZnS:Cu phosphors by using Sol-Gel method. From results of SEM micrographs observation, XRD and XPS analysis, it could be confirmed that $SiO_2$ layer was relatively well coated on ZnS:Cu particles. $Ag_2S$ was used as a decoding chemical to analyze the dense and uniform coating performance of $SiO_2$ layer on phosphor particles. It could be concluded that phosphors synthesized from our two step replacement method showed strong blue peak comparing to other method and rather weak green peak also. Obtained particle size of phosphors were about 20m diameter. Luminescence properties of the phosphors were examined by photoluminescence spectra at the excitation wavelength of 270 nm.

양모의 포말세정에 관한 연구 (Studies on the Foam Washing of Wool)

  • 정두진;개천기
    • 한국의류학회지
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    • 제9권3호
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    • pp.53-61
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    • 1985
  • This paper has been studied on the method of washing without any damage on wool, namely foam washing method. Effect of washing was obtained with experimental equipment manufactured by way of trial. but some deflects were found that the volume of detergent solution and blow ratio changed with time passes by. This difficulties should be improved by farther studies. The solution mixed with sodium oleate ($0.5\%$) and sodium carbonate ($0.3\%$) was found suitable for detergent solution, and under the conditions of washing temperature at $50\~60^{\circ}C$ and washing time for 5 minutes, the washing effect was obtained good. Desoaping treatment with $Na_2CO_3$ solution after washing might be thought to be necessary, and from the scanning electron micrographs (SEM), no damage on wool and wool sureface washed was, observed. From the results of this study foam washing of wool may be expected to be very effective.

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용융황 침투에 의한 콘크리트 구조물의 물성 증진에 관한 연구 (Reinforcement of Concrete Structure by Impregnation of Molten Sulfur)

  • 김종국;오준택;설용건;김우식
    • 한국세라믹학회지
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    • 제26권6호
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    • pp.729-736
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    • 1989
  • This study aims to reinforce concrete structure by impregnation of molten sulfur. The improved properties of sulfur impregnated concerete were confirmed by compressive strength test and water proof effect. Following variables were adopted to evaluate impregnation parameters ; 1) the effect of water content in concrete structure (0-8%) 2) impregnation time of molten sulfur(0-22hr) 3) impregnation temprature of molten sulfur(13$0^{\circ}C$, 14$0^{\circ}C$). In partial ponding experiments, the concrete specimen of sulfur impregnated by 2wt% yields 1.5 times higher value of compressive strength than that of control one(non-impregnated concerte). In complete ponding experiments, the mortar specimen of slufur impregnated by 12-14wt% yields 2-3 times higher value of compressive strength than that of control one (non-impregnated mortar). From the examination of X-ray diffractions, $\alpha$-sulfur was found in concrete pores. Homogeneous impregation of molten sulfur into concrete pores was also identified with poresize analysis and micrographs of SEM.

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SiC-ZrB$_2$계 도전성 복합 세라믹스의 방전가공 (Electrical discharge Machining of SiC-ZrB$_2$Electroconductive Ceramic Composities)

  • 신용덕
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 1996년도 추계학술대회 논문집
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    • pp.320-325
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    • 1996
  • The influences of ZrB$_2$additives to the SiC and pulse width on electrical discharge machining of SiC-ZrB$_2$electroconductive ceramic composites were investigated. IIigher-flexural strength materials show a trend toward smaller crater volumes, leaving a soother surface; the average surface roughness of the SiC-ZrB$_2$15 Vol.% Composite with the flexural strength of 375㎫ was 3.2${\mu}{\textrm}{m}$,whereas the SiC-ZrB$_2$30 Vol.% composite of 457㎫ was 1.35${\mu}{\textrm}{m}$. In the SEM micrographs of the fracture surface of SiC-ZrB$_2$composites, the SiC-ZrB$_2$two phaes are distinct; the white phase is the ZrB$_2$. In the micrograph of the EDM surface, however, these phases are no longer distinct because of thicker recast layer of resolidified-melt-formation droplets present.

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Preparation and Characterization of Biopolymer-Based Nanocomposite Films: Chitosan-Based Nanocomposite Films with Antimicrobial Activity

  • 임종환
    • 한국포장학회:학술대회논문집
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    • 한국포장학회 2006년도 정기총회 및 추계학술발표대회
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    • pp.54-73
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    • 2006
  • Four different types of chitosan-based nanocomposite films were prepared using a solvent casting method by incorporating with four types of nanoparticles, i.e., an unmodified montmorillonite (Na-MMT), an organically modified montmorillonite (Cloisite 30B), a Nano-silver, and a Ag-zeolite (Ag-Ion). X-ray diffraction patterns of the nanocomposite films indicated that a certain degree of intercalation was formed in the nanocomposite films, with the highest intercalation in the Na-MMT-incorporated films followed by films with Cloisite 30B and Ag-Ion. SEM micrographs showed that in all the nanocomposite films, except the Nanosilver-incorporated one, nanoparticles were dispersed homogeneously throughout the chitosan polymer matrix. Consequently, mechanical and barrier properties of chitosan films were affected through intercalation of nanoparticles, i.e., tensile strength (TS) increased by 7-16%, while water vapor permeability (WVP) decreased by 25-30% depending on the nanoparticle material tested. In addition, chitosan-based nanocomposite films, especially silver-containing ones, showed a promising range of antimicrobial activity.

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