• 제목/요약/키워드: SEM Micrographs

검색결과 137건 처리시간 0.027초

SEM 해석을 이용한 시멘트 안정처리 카올린의 공학적 특성 (Mechanical characteristics of cement-stabilized kaolin by SEM analysis)

  • 이규환;정대석
    • 한국지반공학회:학술대회논문집
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    • 한국지반공학회 2006년도 춘계 학술발표회 논문집
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    • pp.1142-1147
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    • 2006
  • Cement-stabilized clay has widespread applications in Deep Mixing projects, whereby soft deep clay deposits are improved through the addition of cement. While much research on this subject has taken place over the past decade, the strength and deformation behaviour of cement-stabilized clay is still not well understood. An extensive laboratory program was conducted on kaolin stabilized with up to 10% cement. Water curing was employed for durations up to 112 days. To study the microstructure of raw and stabilized soil, use is made of SEM. Micrographs of selected raw and stabilized soil were obtained. These micrographs were closely analyzed for any change in the microstructure of the soil as a result of stabilization.

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초음파 진동 부가에 의한 세라믹 복합체의 형조방전가공 (Die-sinking Electrical Discharge Machining with Ultrasonic Emission for Ceramic Matrix Composite)

  • 왕덕현;우정윤;윤존도
    • 한국정밀공학회지
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    • 제16권8호
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    • pp.9-15
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    • 1999
  • Die-sinking electrical discharge machining(EDM) for conductive ceramic matrix composite(CMC) of Tic/$Al_2O_3$ was experienced with addition of ultrasonic emission, and the results were compared with ones obtained by the EDM only. From this experimental study, the values of material removal rate(MRR) and surface roughness($R_{max}$), scanning electron microscope(SEM) micrographs, and weibull probability distribution of bending strength for the specimens were obtained and compared. The trend of MRR was found to be increased slightly with the current and the duty factor for both EDM only and EDM with ultrasonic emission. The MRR values were found to be increased for EDM with ultrasonic emission. The SEM micrographs of EDMed surface by under various operating conditions showed less micro cracks in various places. Although smaller bending strength value was obtained by EDMed surface with ultrasonic emission by weibull probability distribution analysis of bending strength.

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Biomedical Applications of Stereoscopy for Three-Dimensional Surface Reconstruction in Scanning Electron Microscopes

  • Kim, Ki Woo
    • Applied Microscopy
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    • 제46권2호
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    • pp.71-75
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    • 2016
  • The scanning electron microscope (SEM) offers two-dimensional (2D) micrographs of three-dimensional (3D) objects due to its inherent operating mechanisms. To overcome this limitation, other devices have been used for quantitative morphological analysis. Many efforts have been made on the applications of software-based approaches to 3D reconstruction and measurements by SEM. Based on the acquisition of two stereo images, a multi-view technique consists of two parts: (i) geometric calibration and (ii) image matching. Quantitative morphological parameters such as height and depth could be nondestructively measured by SEM combined with special software programs. It is also possible to obtain conventional surface parameters such as roughness and volume of biomedical specimens through 3D SEM surface reconstruction. There is growing evidence that conventional 2D SEM without special electron detectors can be transformed to 3D SEM for quantitative measurements in biomedical research.

고온고압수중에서 접촉형상에 따른 마멸거동 분석 (Analysis of Wear Behaviour Corresponding to Contact Shape in High Temperature and High Pressure Environment)

  • 송주선;김형규;이영호;김재훈
    • 한국윤활학회:학술대회논문집
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    • 한국윤활학회 2004년도 학술대회지
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    • pp.31-36
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    • 2004
  • In this paper, fretting wear tests were conducted in air at room temperature (RT) and in water at high temperature and high pressure (HTHP) environment to analyze the wear characteristic. As for the supporting condition between the tube and spring/dimple, the gap of 0.2 mm in air at RT and the normal force of 10 N and the slip of $50\;{\mu}\;m$ in water at HTHP were applied. Four different shapes of spring/dimple specimen (type A, B, C, D) were used. Detail eaxamination of wear scar was also performed using SEM micrographs. As a result, in the case of the spring of truncated wedge, severer wear occurs than the others. Protrusion part was found and larger in air at RT. It is thought that the difference in the wear volume and the protrusion is caused by the different wear mechanism corresponding to the different environment.

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Influence of Allylamine Plasma Treatment Time on the Mechanical Properties of VGCF/Epoxy

  • Khuyen, Nguyen Quang;Kim, Jin-Bong;Kim, Byung-Sun;Lee, Soo
    • Advanced Composite Materials
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    • 제18권3호
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    • pp.221-232
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    • 2009
  • The allylamine plasma treatment is used to modify the surface properties of vapor grown carbon fibers (VGCF). It is to improve the interfacial bonding between the VGCF and epoxy matrix. The allylamine plasma process was performed by batch process in a vacuum chamber, using gas injection followed by plasma discharge for the durations of 20, 40 and 60 min. The interdependence of mechanical properties on the VGCF contents, treatment time and interfacial bonding between VGCF/ep was investigated. The interfacial bonding between VGCF and epoxy matrix was observed by scanning electron microscopy (SEM) micrographs of nanocomposites fracture surfaces. The changes in the mechanical properties of VGCF/ep, such as the tensile modulus and strength were discussed. The mechanical properties of allylamine plasma treated (AAPT) VGCF/ep were compared with those of raw VGCF/ep. The tensile strength and modulus of allyamine plasma treated VGCF40 (40 min treatment)/ep demonstrated a higher value than those of other samples. The mechanical properties were increased with the allyamine plasma treatment due to the improved adhesion at VGCF/ep interface. The modification of the carbon nanofibers surface was observed by transmission electron microscopy (TEM). SEM micrographs showed an excellent dispersion of VGCF in epoxy matrix by ultrasonic method.

Achene wall anatomy and surface sculpturing of Launaea Cass. (Compositae: Cichorieae) with notes on their systematic significance

  • Zareh, Momen Mustafa;Faried, Ahmed Mohamed;Mohamed, Mona Hassan
    • 식물분류학회지
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    • 제46권2호
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    • pp.187-198
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    • 2016
  • This is the first study to deal in-depth with the achene ultra-structure of the genus Launaea Cass. in Egypt. It focuses on 12 taxa belonging to 10 species of this genus. The achene wall anatomy and surface sculpturing of those taxa were studied using scanning electron microscopy (SEM). Important aspects of the investigated taxa based on the achene characters as well as SEM micrographs of the achene surface and anatomical sections are given. Main and secondary costa of the inner achenes are used for easy differentiation between L. intybacea and L. massauensis.

Surface Modification of Multi-walled Carbon Nanotubes for Enhancement of Dispersion and Electrochemical Properties

  • Kim, Young-Ja;Zhang, Wentao;Lee, Hong-Ro;Kim, Jong-Hyee
    • 한국표면공학회지
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    • 제41권5호
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    • pp.194-198
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    • 2008
  • Several methods for improving dispersion of carbon nanotubes (CNTs) have been investigated. CNTs modified by acids and hydrogen peroxide ($H_2O_2$) showed improved dispersion. From SEM micrographs and photos of dispersion, CNTs modified with nitric acid and $H_2O_2$, showed no agglomeration in solution even standing for 4 months, which means successfully improved dispersion property. TEM micrographs of surface modified single CNT treated with 69% $HNO_3$ in boiling acid solution as the optimum method were obtained. For confirmation of CNTs' application to EDLC electrode materials, characteristics of EDLC have been analyzed by cyclic voltammetry curve, specific capacitance of unit cell, electrode discharge curves and AC impedance curve. From the results, it could be confirmed that electrochemical properties of CNTs were enhanced after surface modification with 69% $HNO_3$ acid treatment.

Performance evaluation of β-glucan treated lean clay and efficacy of its choice as a sustainable alternative for ground improvement

  • Kumara, S. Anandha;Sujatha, Evangelin Ramani
    • Geomechanics and Engineering
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    • 제21권5호
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    • pp.413-422
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    • 2020
  • The choice of eco-friendly materials for ground improvement is a necessary way forward for sustainable development. Adapting naturally available biopolymers will render the process of soil stabilization carbon neutral. An attempt has been made to use β-glucan, a natural biopolymer for the stabilization of lean clay as a sustainable alternative with specific emphasis on comprehending the effect of confining stresses on lean clay through triaxial compression tests. A sequence of laboratory experiments was performed to examine the various physical and mechanical characteristics of β-glucan treated soil (BGTS). Micro-analysis through micrographs were used to understand the strengthening mechanism. Results of the study show that the deviatoric stress of 2% BGTS is 12 times higher than untreated soil (UTS). The micrographs from Scanning Electron Microscopy (SEM) and the results of the Nitrogen-based Brunauer Emmett Teller (N2-BET) analysis confirm the formation of new cementitious fibres and hydrogels within the soil matrix that tends to weld soil particles and reduce the pore spaces leading to an increase in strength. Hydraulic conductivity (HC) and compressibility reduced significantly with the biopolymer content and curing period. Results emphases that β-glucan is an efficient and sustainable alternative to the traditional stabilizers like cement, lime or bitumen.

치과 임플란트용 bioactive 세라믹 복합재료의 제조와 미세조직 (Microstructure and Processing of Bioactive Ceramic Composites as Dental Implants)

  • 김부섭
    • 대한치과기공학회지
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    • 제25권1호
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    • pp.21-28
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    • 2003
  • The purpose of this study was to process bio-active glass ceramic composite, reinforced with sapphire fibers, by hot press. Also to study the interface of the matrix and the sapphire fiber, and the mechanical properties. Glass raw materials melted in Pt crucible at 1300$^{\circ}C$ during 3.5 hours. The melt was crushed in ball mill and then crushed material, ground and sieved to $<40{\beta}{\mu}m$. Sapphire fibers cut (30mm) and aligned. Powder and fibers hot pressed. The micrographs show good bonding between the matrix and the fiber and no porosity in the glass matrix. This means ideal fracture phenomena. Glass is fractured before the fiber. This is indication of good fracture strength. EDXS showing aluminum rich phase and crystalline phase. Bright field image of the matrix showing crystalline phase. Also diffraction pattern of TEM showing the crystalline phase and more than one phase. Strength of the samples was determined by 3 point bend testing. Strength of the 10vol% sample was approximately 69MPa, while strength of the control sample is 35MPa. Conclusions through this study as follow: 1. Micrographs show no porosity in the glass matrix and the interface. 2. The interface between the fiber and the glass matrix show no gaps. 3. Fracture of the glass indicates characteristic fiber-matrix separation. 4. Presence of crystalline phase at high processing temperature. 5. Sapphire is compatible with bioactive glass.

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