• Journal of Information Technology Applications and Management
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• v.31 no.1
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• pp.11-25
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• 2024

The purpose of this study is to investigate the improvement of prediction performance and changes in variable importance in SEM-ANN two-stage analysis. 366 cosmetics repurchase-related survey data were analyzed and the results were presented. The results of this study are summarized as follows. First, in SEM-ANN two-stage analysis, SEM and ANN models were trained with train data and predicted with test data, respectively, and the R² was showed. As a result, the prediction performance was doubled from SEM 0.3364 to ANN 0.6836. Looking at this degree of R² improvement as the effect size f² of Cohen (1988), it corresponds to a very large effect at 110%. Second, as a result of comparing changes in normalized variable importance through SEM-ANN two-stage analysis, variables with high importance in SEM were also found to have high importance in ANN, but variables with little or no importance in SEM became important in ANN. This study is meaningful in that it increased the validity of the comparison by using the same learning and evaluation method in the SEM-ANN two-stage analysis. This study is meaningful in that it compared the degree of improvement in prediction performance and the change in variable importance through SEM-ANN two-stage analysis.

• Journal of Korean Society for Atmospheric Environment
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• v.15 no.2
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• pp.175-182
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• 1999

Scanning electron microscopy (SEM) has played an important role in receptor modeling area because it is a powerful tool for characterizing individual particles. The purpose of the study was to classify individual diesel particles base on statistical analysis and image analysis by SEM/EDX (energy dispersive x-ray analyser). The diesel particles were sampled by both a modified CVS 75 mode and a high speed mode with a chassis dynamometer. The SEM/EDX system provides various physical parameters including particle's particle diameter and chemical information. Thus density and mass of the diesel particle were estimated cased on its chemical composition and further fractal dimensions of the diesel particle were obtained by the Hurst exponent method. The fractal dimension in the sample of modified CVS 75 mode was higher than the high speed mode. Finally, mass fractions for a diesel vehicle as a source profile were estimated cased on a particle class concept.

• Mass Spectrometry Letters
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• v.7 no.3
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• pp.64-68
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• 2016

Scanning electron microscopy combined with thermal ionization mass spectrometry (SEM-TIMS) was used to determine the precise isotope ratios of ultra-trace levels of uranium contained in individual microparticles. An advanced multiple ion counter system consisting of three secondary ion multipliers and two compact discrete dynodes was used for complete simultaneous ion detection. For verification purposes, using TIMS with complete simultaneous measurement, isotopes were analyzed in 5 pg of uranium of a certified reference material. A microprobe in the SEM was used to transfer individual particles from a NUSIMEP-7 sample to TIMS filaments, which were then subjected to SEM-TIMS and complete simultaneous measurement. The excellent agreement in the resulting uranium isotope ratios with the certified NUSIMEP-7 values shows the validity of SEM-TIMS with complete simultaneous measurement for the analysis of uranium isotopes in individual particles. Further experimental study required for investigation of simultaneous measurement using the advanced multiple ion counter system is presented.

• Ceramist
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• v.22 no.4
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• pp.368-380
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• 2019

A ceramic is used as a key material in various fields. Accordingly, the use of scanning electron microscopy is increased for the purpose of evaluating the reliability and defects of advanced ceramic materials. The scanning electron microscope is developed to overcome the limitations of optical microscopy and uses accelerated electrons for imaging. Various signals such as SE, BSE and characteristic X-rays provide useful information about the surface microstructure of specimens and, the content and distribution of chemical components. The development of electron guns, such as FEG, and the improved lens system combined with the advanced in-lens detectors and STEM-in-SEM system have expanded the applications of SEM. Automated SEM-EDS analysis also greatly increases the amount of data, enabling more statistically reliable results. In addition, X-ray CT, XRF, and WDS, which are installed in scanning electron microscope, have transformed SEM a more versatile analytical equipment. The performance and specifications of the scanning electron microscope to evaluate ceramics were reviewed and the selection criteria for SEM analysis were described.

• Proceedings of the KSME Conference
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• 2007.05a
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• pp.1288-1293
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• 2007

The present study covers the design and analysis of a thermionic scanning electron microscope (SEM) column. The SEM column contains an electron optical system in which electrons are emitted and moved to form a focused beam, and this generates secondary electrons from the specimen surfaces, eventually making an image. The electron optical system mainly consists of a thermionic electron gun as the beam source, the lens system, the electron control unit, and the vacuum unit. In the design process, the dimension and capacity of the SEM components need to be optimally determined with the aid of finite element analyses. Considering the geometry of the filament, a three-dimensional (3D) finite element analysis is utilized. Through the analysis, the beam emission characteristics and relevant trajectories are predicted from which a systematic design of the electron optical system is enabled. The validity of the proposed 3D analysis is also discussed by comparing the directional beam spot radius. As a result, a prototype of a thermionic SEM is successfully developed with a relatively short time and low investment costs, which proves the adoptability of the proposed 3D analysis.

• Journal of Information Technology Applications and Management
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• v.30 no.6
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• pp.91-111
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• 2023

This study aims to identify the influencing factors of intention to use cloud services using the SEM-ANN two-step approach. In previous studies of SEM-ANN, SEM presented R² and ANN presented MSE(mean squared error), so analysis performance could not be compared. In this study, R² and MSE were calculated and presented by SEM and ANN, respectively. Then, analysis performance was compared and feature importances were compared by sensitivity analysis. As a result, the ANN default model improved R² by 2.87 compared to the PLS model, showing a small Cohen's effect size. The ANN optimization model improved R² by 7.86 compared to the PLS model, showing a medium Cohen effect size. In normalized feature importances, the order of importances was the same for PLS and ANN. The contribution of this study, which links structural equation modeling to artificial intelligence, is that it verified the effect of improving the explanatory power of the research model while maintaining the order of importance of independent variables.

• Journal of the Korean Wood Science and Technology
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• v.35 no.1
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• pp.36-43
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• 2007

Elemental analysis, SEM-EDX, X-ray diffraction (XRD) and IR analysis were adopted to examine the quality of charred woods excavated from the underground of the Daewoongjeon Hall of Youngguksa Temple, Youngdong-gun, Chungbuk, Korea. A large amount of calcium was detected in SEM-EDX analysis. The analyses of chemical elements suggested that completely charred wood was carbonized at about $500^{\circ}C$. The XRD results indicated the destruction of cellulose crystalline region. The IR analysis exhibited that thermal degradation of wood component was different depending upon the carbonization temperature. It can be suggested from the results that PEG with different molecular weights should be used for the conservation of excavated charred woods.

• Tribology and Lubricants
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• v.23 no.5
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• pp.195-200
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• 2007

This paper presents the friction induced scuffing and wear defects analysis of a pin bushing bearing based on the chemical composition using a scanning microscopy (SEM) and an energy dispersive X-ray analyzer (EDX). The SEM/EDX system, which may provide good information on the surface thermal defects and chemical compositions, provides impurities such as an aluminum, a silicon, a ferrous component and an oxygen, especially. The EDX measured results show that the oxygen may reduce the strength and a hardness of a pin busing, which may lead to a scuffing and a seizure on the rubbing contact surface. The current technology fabricated by a sintering for a pin bushing bearing should be modified or changed to reduce the oxygen composition and the impurities in pin bushing materials.

• Mass Spectrometry Letters
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• v.4 no.3
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• pp.51-54
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• 2013

Isotopic analysis using thermal ionization mass spectrometry coupled with scanning electron microscopy (SEM-TIMS) was performed to determine the isotopic ratios of uranium contained in micro-particles in the 6th Nuclear Signatures Interlaboratory Measurement Evaluation Programme (NUSIMEP-6) sample. Elemental analysis by energy dispersive X-ray spectroscopy (EDS) was conducted on uranium-bearing mirco-particles, which were transferred to rhenium filaments for TIMS loading using a micromanipulation system in a SEM. A multi-ion-counter system was utilized to detect the ion signals of the four isotopes of uranium simultaneously. The isotope ratios of uranium corrected by bracketing using a reference material showed excellent agreement with the certified values. The measurement accuracy for $n(^{234}U)/n(^{238}U)$ and (b) $n(^{235}U)/n(^{238}U)$ was 10% and 1%, respectively, which met the requirements for qalification for the NetWork of Analytical Laboratories (NWAL).

• Transactions of the Korean Society of Machine Tool Engineers
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• v.16 no.5
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• pp.140-144
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• 2007

As an electron scanning microscopes has traditionally required a considerably large room equipped with several service and pipe lines due to its inherent size. As an alternative, a small sized SEM, simply called a mini-SEM, is introduced even if the performance in terms of magnification and resolution is a little inferior to a classical thermal SEM. However, the size and fabrication cost is dramatically reduced, dedicating to opening a new market. The optical system in the mini-SEM is redesigned and specimen stage is quitely reduced and vertical axis is excluded. The design tools and calibration techniques to develope the mini-SEM are introduced and its performance is verified through numerical analysis experiments.