• Title/Summary/Keyword: SEM (scanning electron microscope)

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Gallium Nitride Epitaxy films Growth with Lower Defect Density (결함밀도가 낮은 Gallium Nitride Epitaxy 막 제조)

  • 황진수
    • Korean Journal of Crystallography
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    • v.9 no.2
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    • pp.131-137
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    • 1998
  • 결정결함의 밀도가 낮은 GaN epitaxy 막을 MOCVD(metal organic chemical vapour deposition) 방법에 의해 성장시켰다. 기판은 6H-SiC를 사용하였으며, AlN과 GaN으로 구성된 이중 buffer 층을 도입하였다. GaN buffer 층은 반응원료인 trimethyl gallium(TMG)과 NH3 가스를 교호식펄스공급(alternating pulsative supply, APS)방법에 의해 만들었다. AlN buffer/6H-SiC 위에 초기단계에 형성되는 GaN 섬은 APS처리에 의해 크기가 커지는 것을 AFM(atomic force microscope)으로 관찰하였다. Buffer 층의 역할은 그 위에 성막시킨 GaN epitaxy 막의 결정성과 결함밀도에 의해 조사하였다. 성막된 GaN의 결정구조와 결정성은 DCXRD(double crystal X-ray diffractormeter)에 의해 측정되었다. 결정결함은 EPD(etching pit density)를 측정하는 방법으로 알칼리혼합용에서 처리된 막을 SEM(scanning electron microscope)으로 관찰하였다.

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A Study on Mechanical Properties of Carbon Nanofiber/Epoxy Composites with Dispersion Methods (분산 방법에 따른 탄소나노섬유/에폭시 복합재료의 기계적 물성에 관한 연구)

  • Kong Jin-Woo;Chung Sang-Su;Kim Tae-Wook
    • Proceedings of the Korean Society For Composite Materials Conference
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    • 2004.04a
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    • pp.151-154
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    • 2004
  • Despite of the excellent properties of carbon nanofiber, The properties of carbon nanofiber filled polymer composites were not increased largely. The reason is that it is still difficult to ensure the uniform dispersion of carbon nanofiber in a polymer matrix. In this study, For improvement properties of carbon nanofiber filled epoxy composites, the effect of dispersion was investigated. The compounds were prepared by two methods, solution blending and mechanical mixing. Mixing of solution blending method was used using ultrasonic. Dispersion of carbon nanofiber was observed by optical microscope and scanning electron microscope (SEM). UV adsorption and turbidity measured by UV spectrometer was used for the comparison of dispersion of carbon nanofiber.

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A cost-effective and simple culture method for primary hepatocytes

  • Adaya, Sezin;Hasircib, Nesrin;Gurhana, Ismet Deliloglu
    • Animal cells and systems
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    • v.15 no.1
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    • pp.19-27
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    • 2011
  • Hepatocytes, the major epithelial cells of the liver, maintain their morphology in culture dishes coated with extracellular matrix (ECM) components such as collagen and fibronectin or biodegradable polymers (e.g. chitosan, gelatin). In these coated dishes, survival of cells and maintaining of liver-specific functions may increase. The aim of this study was to determine a suitable, cost-effective and simple system for hepatocyte isolation and culture which may be useful for various applications such as in vitro toxicology studies, hepatocyte transplantation and bioartificial liver (BAL) systems. In order to obtain primary cultures, hepatocytes were isolated from liver by an enzymatic method and cultured on plates coated with collagen, chitosan or gelatin. Collagen, gelatin-sandwich and gelatin-cell mixture methods were also evaluated. Morphology and attachment of the cells were observed by inverted microscope and scanning electron microscope (SEM). An MTT assay was used to determine cell viability and mitochondrial activity.

Study on the Microcapsule Emulsion Containing Taraxacum platycarpum (포공영을 이용한 마이크로캡슐 에멀젼에 관한 연구)

  • Cho, Woo-A;Kim, Young-Hun;Jang, Min-Jung;Cheon, Soon-Ju;Lee, Jin-Tae
    • Journal of the Korean Society of Fashion and Beauty
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    • v.5 no.4
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    • pp.145-148
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    • 2007
  • The aims of this study was assess to preparation and stability of emulsion containing Taraxacum platycarpum ethanol extract our team was found to shape and size of capsule by optical microscope and Scanning Electron Microscope (SEM). In the stability test of the emulsion including Taraxacum platycarpum ethanol extract, it was stable of pH, viscosity during 30days. According to all the test results that have been given, it is possible that the ethanol extract of Taraxacum platycarpum can be used as a new cosmetics material.

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Dispersion of nanodiamond by Chemical treatment (나노다이아몬드의 화학적 처리에 따른 분산 특성)

  • Park, Jong-Soon;Kim, Hong;Kang, Soon-Kuk
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.12 no.2
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    • pp.999-1004
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    • 2011
  • In this study, nanodiamod's surface have formed carboxyl, hydroxyl, amine radical for the purpose of use of nanodiamond synthesized by detonation, and then it has widely stable dispersion and slowly sedimentation in solvent. Thus nanodiamonds obtained by chemical treatment were used to analyze the structure, surface statement, particle size and sedimentation specification in solvent for method X-ray diffration(XRD), scanning electron microscope energy diffraction spectroscopy(SEM-EDS), Fourier transform infrared spectroscopy (FTIR), automic force microscope(AFM).

Evaluation of Microstructure and Mechanical Property of Inconel 600 Degraded under High Temperature (고온 열화된 Inconel 600강의 미세조직 및 기계적 특성 평가)

  • Jung, Kwang-Hu;Kim, Seong-Jong
    • Journal of the Korean institute of surface engineering
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    • v.50 no.6
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    • pp.492-497
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    • 2017
  • In this study, we investigated the effect of thermal aging on mechanical characteristics of Inconel 600 nickel-based alloy. The thermal aging was conducted up to 1000 hours at an atmosphere of $650^{\circ}C$. The microstructure of thermally aged specimens was investigated by an optical microscope (OM), scanning electron microscope (SEM) and energy dispersive spectrometer (EDS). In addition, tensile test (strain rate: 2 mm/min) and micro Vickers hardness test were conducted to evaluate mechanical properties with time. As a result of the experiment, Cr-rich carbide continuously precipitated during thermal aging, leading to the change of the mechanical characteristics and fracture mode. With the increase of aging time, tensile strength, yield strength, and hardness gradually decreased. The fracture mode changed from ductile to brittle with the increase of grain boundary carbide.

Study on Abrasive Wear Behaviour of a Carbon Fiber Composites (탄소 섬유 강화 고분자 복합재의 연삭마모 특성에 관한 연구)

  • Koh, S.W.;Yang, B.C.;Kim, H.J.;Kim, J.D.
    • Journal of Power System Engineering
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    • v.10 no.1
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    • pp.46-51
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    • 2006
  • Present study was investigated the effect of the particle of the counterface of unidirectional carbon fiber reinforced composite. The friction coefficient of composite and the specific wear rate different sliding velocity were measured for this materials. The friction track of counterface was observed by an optical microscope and scanning electron microscope. There were insignificant effects of the specific wear rate under lower Sic abrasive particle, however it showed high effect on $30{\mu}m$ abrasive particle size. There were significant effects of friction and wear behavior of the fiber direction under 0.3m/s sliding speed. Major failure mechanisms can be classified such as microfracture, plowing, microcutting, cutting and cracking.

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Electrochemical Signal Amplification by Gap Electrodes and Control of Gap Distances

  • Park, Dae Keun
    • KEPCO Journal on Electric Power and Energy
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    • v.5 no.3
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    • pp.197-200
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    • 2019
  • We report on electrochemical signal amplification using gap electrodes based on the redox cycling between gap electrodes. The distance between electrodes was controlled from $2{\mu}m$ to a few hundreds of nanometer by chemical deposition of reduced Au ion on the pre-defined electrodes. Enhanced redox current of ferri/ferrocyanide was obtained by redox cycling between the two working electrodes. The faradaic current is amplified about a thousand times in this redox system. Since the signal amplification is due to the shortened diffusion length between the two electrodes, the narrower the nanogap was, the better detection limit, calibration sensitivity, and dynamic range. The experimental results were discussed on the basis of the cyclic voltammetry (CV), atomic force microscope (AFM) and scanning electron microscope (SEM) measurements.

Development of Electrospray Micro Thruster with Super-Hydrophobic PTFE Surface Nozzle Treated by Ar and Oxygen Ion Beam

  • Lee, Y.J.;Byun, D.Y.;Si, Bui Quang Tran;Kim, S.H.;Park, B.H.;Yu, M.J.;Kim, M.Y.
    • Proceedings of the Korean Society of Propulsion Engineers Conference
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    • 2008.03a
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    • pp.877-880
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    • 2008
  • In this article, in order to fabricate polymer based electrospray device with super hydrophobic nozzle we use PTFE(polyfluorotetraethylene) plate and PMMA(polymethylmethacrylate). To obtain the super hydrophobic surface nozzle, PTFE surface is treated by argon and oxygen plasma treatment process. And evaluate the treated surface, perform measuring contact angle, SEM(Scanning Electron Microscope) and AFM(Atomic Force Microscope). We compare the performance of the super hydrophobic PTFE surface nozzle with raw PTFE and PMMA surface nozzle. For the ion beam treated PTFE nozzle, the liquid doesn't overflow and it keeps initial position and meniscus shape. From these results, we expect in cease of superhydrophobic surface nozzle jetting becomes more stable and repeatable.

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Fouling resistant membrane tailored by polyethylene glycol in oxidative environment for desalination

  • Kavaiya, Ashish R.;Raval, Hiren D.
    • Membrane and Water Treatment
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    • v.10 no.5
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    • pp.381-385
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    • 2019
  • Surface modification is very efficient and scalable approach to achieve improved membrane performance. We treated Reverse Osmosis Thin Film Composite (TFC RO) membrane with various concentrations of Polyethylene Glycol (PEG), a hydrophilic polymer after activation with sodium hypochlorite. This treatment resulted in an increment of the water flux by 43% and the salt rejection by 2.36% for the 3000 mg/l PEG-treated membrane. Further, these PEG-treated membranes were exposed to a mixture of 3000 mg/l PEG and 1000 mg/l sodium hypochlorite for 1 hour. Further modification of this membrane by PEG and sodium hypochlorite mixture increased the water permeance up to 133% when compared with the virgin TFC RO membrane. We characterized the treated membranes to understand the changes in wettability by contact angle analysis, changes in surface morphology and roughness by scanning electron microscope (SEM) and atomic force microscope (AFM) analysis.