• Tribology and Lubricants
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• v.23 no.5
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• pp.195-200
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• 2007

This paper presents the friction induced scuffing and wear defects analysis of a pin bushing bearing based on the chemical composition using a scanning microscopy (SEM) and an energy dispersive X-ray analyzer (EDX). The SEM/EDX system, which may provide good information on the surface thermal defects and chemical compositions, provides impurities such as an aluminum, a silicon, a ferrous component and an oxygen, especially. The EDX measured results show that the oxygen may reduce the strength and a hardness of a pin busing, which may lead to a scuffing and a seizure on the rubbing contact surface. The current technology fabricated by a sintering for a pin bushing bearing should be modified or changed to reduce the oxygen composition and the impurities in pin bushing materials.

• Journal of the Korean institute of surface engineering
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• v.37 no.3
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• pp.137-145
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• 2004

This study surveys the microscopic wear of CVD TiN coatings in repeated sliding, using the SEM Tribosystem as in-situ system. According to the research, the depth of wear groove and the specific wear amount are changed by the transition of the microscopic wear mode. This investigation leads to the fact that the change of wear characteristics produces the transition of the wear mode. In this survey, four modes are observed for CVD TiN coatings with the thickness of 1.6$\mu\textrm{m}$: ploughing, powder formation, flake formation and coating delimitation. The microscopic wear properties is quantitatively evaluated in terms with the microscopic wear mode and the specific wear amount. These relationships prove that the observation of wear modes with a SEM Tribosystem is useful to evaluate wear properties.

• Journal of the Ergonomics Society of Korea
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• v.20 no.3
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• pp.47-60
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• 2001

The purpose of this paper is propose an analytical method for evaluating user satisfaction of Internet website and identifying casual relationships between user satisfaction of Internet website and performance measures as like revisit intention and complaints using the structural equation model (SEM). This paper is intended to identify critical evaluation factors of user satisfaction for Internet website to determine criteria for evaluating the website. and use the criteria to develop a SEM model for quantitatively evaluation of each factors effects of user preference. The SEM model used 5 latent variables for the evaluation factors of website user satisfaction and 2 latent variables for performance evaluation. 2 portal sites were evaluated to construct the SEM model. and 74 subjects participated the website evaluation using the walk-through and face-to face survey method. Analysis results showed that the SEM model was statistically significant for all the 2 websites evaluated.

• KSBB Journal
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• v.16 no.3
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• pp.295-301
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• 2001

The leaching effect of Thiobacillus ferrooxidance (ATCC 19859) upon polished pyrite ore in 9K medium at $30^{circ}C$ for 30 days was investigated. The surface atomic ratios for Fe, S, Al, Si, and Cu were analyzed by EPMA using fresh and leached samples. The atomic ratio of Fe and S were changed to Fe rich phase as leaching progressed over 13 days but the Fe/S ratio became constant between 13 and 30 days. SEM imaging showed that $10\mum$ oblong shapes formed on the surface after 13 days and that these further developed until 23 days. Fe, S and K atomic ratios were analyzed by SEM-EDS.

• Journal of the Ergonomics Society of Korea
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• v.22 no.2
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• pp.45-56
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• 2003

The purpose of this study is to develop the model including multiple causal relationship between factors to evaluate overall user satisfaction and develop an objective method to quantify the impacts and scores of each qualitative factors on overall user satisfaction using Structural Equation Model(SEM) and also test the feasibility to construct a comprehensive website evaluation model including qualitative and quantitative factors. The SEM model used 2 qualitative factors of usability and esthetic factors for the evaluation factors of user satisfaction and select 4 attributes of each factors using factor analysis. 3 shopping mall sites were evaluated to construct the SEM model, and 155 subjects participated the website evaluation using the walk-through and face-to-face survey method. Analysis results showed that the SEM model was statistically significant for all the 3 websites evaluated. Both the usability and esthetic factors showed significant effects to user satisfaction of websites and have positive correlation. The user satisfaction was more effected by the usability factor than esthetic factors, and the simplification and harmonization were the most critical attributes of the usability and esthetic factors.

• Proceedings of the Korean Vacuum Society Conference
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• 2014.02a
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• pp.107.2-107.2
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• 2014

다양한 산업분야에서의 급격한 Packing Density 증가 추세로 인하여 영상분석기기 분야도 기술적으로 매우 진보되어왔다. 특히 전자현미경(SEM : Scanning Electron Microscope)은 반도체, 디스플레이 및 부품 소재의 고집적화와 더불어 기술의 발전 속도가 빠르게 이루어지고 있으며, 매우 고도화 되고 있다. 이에 따른 다양한 응용분야에서 전자현미경의 수요도 꾸준히 증가되고 있는 추세이다. 그러나 기초 과학기술을 기반으로 하는 전자현미경 산업분야는 높아진 국내 수요대비 자체 기술 발전이 미약한 실정이다. 이러한 현실속에서 국내 기술력으로 FE-SEM을 개발하였고 상용화를 눈앞에 두고 있다. 국산화된 FE-SEM은 Outer Lens방식으로 Schottky cathode와 60o conical Lens를 적용하여 고분해능을 구현함과 동시에 Scan generator, Auto-stepping및 Retarding 기능들도 추가 장착하여 제품경쟁력을 극대화 하고자 하였다. 본 발표는 개발된 FE-SEM의 기술적 특징과 개발 과정 및 결과를 소개하고자 하였다. 또한 해외 경쟁사들의 선행 기술동향 대비 현재 국내 기술 수준을 비교하여 향후 나아갈 방향을 고찰하고자 하였으며, 이를 기반으로 진행 중에 있는 초 저-가속전압 및 Semi In-Lens Optic구현을 위한 국내 기술개발 추진 현황도 간략하게 논하고자 한다. 이러한 고찰을 통하여 해외 선진 경쟁사 대비 후 발업체로써 낙후되어있는 국내기술의 격차를 빠르게 좁혀 나아가고 Global 경쟁력을 갖춘 제품을 구현하기 위하여 국내 전문가들과의 협력을 통한 선행 요소기술 및 차별화된 제품기술 확보 방법을 강구하고자 한다.

• Journal of the korean society of oceanography
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• v.39 no.4
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• pp.243-250
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• 2004

Sediment microcosm experiments were conducted for 14 and 28 days using Zn spiked sediment to examine the changing distribution of bioavailab1e sediment-bound Zn at different SEM (simultaneously extracted metal)-Zn/ AVS (acid volatile sulfide) mole ratios as a function of time and amphipod density. In surficial sediments (0-1cm), AVS concentrations significantly decreased due to bioturbation and oxidation, while SEM-Zn concentrations remained unchanged. As a result, SEM-Zn/AVS ratios in the surface sediment were greater one although the ratios were designed as less than one initially. With increasing SEM-Zn/AVS ratios in surficial sediments, concentrations of potentially bioavailable $MgCl_2$extractable-Zn, NaOAc extractable-Zn and pore water-Zn significantly increased, while concentrations of SEM-Zn were not significantly varied. Results suggested that as AVS concentrations decreased, AVS bound Zn was partitioned to other sediment fractions (i.e. $MgCl_2$ and NaOAc extractable) and the pore water, resulting in changes in Zn bioavailability in surficial sediments. Concentrations of AVS, SEM-Zn and pore water-Zn remained unchanged in the deeper layers (>1 cm) of the sediment.

• Transactions of the Korean hydrogen and new energy society
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• v.16 no.3
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• pp.238-243
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• 2005

Mg and Mg-based alloys are most important hydrogen storage materials. It is a lightweight and low-cost materials with high hydrogen storage capacity. However, the formation of hydride at high temperature, the deterioration effect, the hydriding and dehydriding kinetics are bad factor for application. In this study, Mg and Ni have been produced by hydrogen induced mechanical alloying(HIMA) process. The raw materials, Mg(purity 99.9%) chip and Ni(purity 99.95%) chip was prepared by using a planetary ball mill apparatus(FRITSCH pulverisette 5). The balls to chips mass ratio(BCR) are 30:1. The hydrogen pressure induced 2.0MPa and milling times were 12, 24, 48, 72, 96 hours with a rotating speed of 200rpm. X-ray diffraction(XRD) analysis was made to characterize the crystallite size and misfit strain. The crystallite size measured by laser particle size analysis(PSA). Microstructure changes were investigated by scanning electron microscopy(SEM) and the transmission electron microscopy(TEM). The hydrogen storage properties were evaluated by using an Sivert's type automatic pressure-composition-therm(PCT) apparatus.

• Applied Microscopy
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• v.42 no.2
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• pp.111-114
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• 2012

The scanning electron microscopy is an ideal technique for examining plant surface at high resolution. Most hydrate samples, however, must be fix and dehydrate for observation in the scanning electron microscope. Because the microscopes operate under high vacuum, most specimens, especially biological samples, cannot withstand water removal by the vacuum system without morphological distortion. Cryo-techniques can observe in their original morphology and structure without various artifacts from conventional sample preparation. Rapid cooling is the method of choice for preparing plant samples for scanning electron microscopy in a defined physiological state. As one of cryo-technique, high-pressure freezing allows for fixation of native non-pretreated samples up to $200{\mu}M$ thick and 2 mm wide with minimal or no ice crystal damage for the freezing procedure. In this study, we could design to optimize structural preservation and imaging by comparing cryo-SEM and convention SEM preparation, and observe a fine, well preserved Arabidopsis stem's inner ultrastructure using HPF and cryo-SEM. These results would suggest a useful method of cryo-preparation and cryo-SEM for plant tissues, especially intratubule and vacuole rich structure.

• Journal of the Korean Chemical Society
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• v.54 no.5
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• pp.551-555
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• 2010

Cinnamomum Iners (Darchini, 쟈 바 계피), Elettaria Cardamomum (Elachi, 백두구, 소두구, 카다몬, 카도몬), Punica Granatum (Anar Dana, 석류), Curcuma Longa (Haldi, 터메릭, 투메릭, 심황, 울금, 울금은, 컬쿠마), Piper Nigrum (Kali Mirch, 페퍼, 페퍼블랙, 후추, 블랙 페퍼), Syzygium aromaticum (Loung, 클로브, 정향, 정향나무,), Capsicum Annum (Laal Mirch, Red Pepper), Mentha Arvensis (Pahari Podina), Curcuma Zedoaria (Kachur, 가쥬츠, 봉출, 아출, 커큐머 제도) Zingiber officinale (Adrak, 건강, 생강, 진저) and Garam Masala (Hot Spice, a mixture) have been analyzed in the present work for their metallic components with the help of SEM-EDS and ICP-AES. Minor concentrations have been determined with ICP-AES and major concentrations with the help of SEM-EDS.