• 제목/요약/키워드: SCC Fracture Surface

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Al-Cu-Mn주조합금의 SCC특성에 미치는 Cd첨가의 영향 (Effect of Cd Addition on the SCC Properties of Al-Cu-Mn Cast Alloys)

  • 이찬희;김경현;김인배
    • 한국재료학회지
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    • 제11권4호
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    • pp.266-271
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    • 2001
  • Al-Cu-Mn 주조합금의 응력부식균열 저항성에 미치는 Cd첨가의 영향을 C-ring test와 전기전도도 시험을 통하여 조사하였다. Cd첨가량이 증가함에 따라 전기전도도가 증가하였고 SCC 저항성도 증가하였다. SCC 시험결과 균열이 입계를 따라 전파되는 입계파괴가 일어났으며, 파면은 취성파괴양상을 나타내었고, 입계를 따라 조대 석출물과 무석출대가 나타난 것으로 보아서 이 합금의 SCC 기구는 anodic dissolution model이라고 판단된다. Cd을 첨가하지 않은 경우 최대경도값은 127Hv였으나, Cd을 첨가한 경우 최대경도값은 138∼146Hv로 증가하였다.

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저변형률시험법에 의한 섬유강화 복합재료의 응력부식균열에 관한 연구 (A Study on Stress Corrosion Cracking of Fiber Reinforced Composite by Slow Strain Rate Test)

  • 임재규;최태수
    • 대한기계학회논문집A
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    • 제20권11호
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    • pp.3433-3440
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    • 1996
  • This paper was investigation of the stres corrosion cracking(SCC) mechanism and the properties of corrosion fracture surface of glass fiber reinforced plastics(GFRP) produced by hand lay up(HLU) method in synthetic sea water. Test material is GFRP, that was used vinylester type epoxy acrylate resin and an unsaturated polyester as the matrix and the chopped strand mat(CSM) type E-glss fiber as the reinforcement. The slow strain rate test(SSRT) was performed on dry, wet and saturated wet specimens in sea water. Here the pH concentration of synthetic sea water was 8.2 and the strain rate is 1 x $10^{-6}$($sec^{-1}$) and test temperature ranges varied from $-60^{\circ}C$ to $80^{\circ}C$. It could be confirmed the fact that wet specimens tested at a particular test temperature ranges were appeared the eviences of SCC such as con-planar, mirror and hackle zone. Moreover, SCC of GFRP in sea water was characterised by falt fracture surfaces with only small amounts of fiber pull-out, in partial.

Al-Cu-Mn 주조합금의 SCC 특성에 미치는 Sn 첨가의 영향 (Effect of Sn Addition on the SCC Properties of Al-Cu-Mn Cast Alloy)

  • 김광년;김경현;김인배
    • 한국재료학회지
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    • 제12권6호
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    • pp.436-441
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    • 2002
  • Effect of Sn addition on the stress corrosion cracking(SCC) resistance of the Al-Cu-Mn cast alley was investigated by C-ring teat and electrical conductivity measurement, The electrical conductivity and SCC resistance increased by Sn addition. The alley containing 0,10%Sn showed maximum electrical conductivity and the best SCC resistance. At the same composition, the electrical conductivity and SCC resistance increased from peak aged condition to ever aged condition. The PFZ and coarse precipitates along the grain boundary were observed from TEM micrographs. The fracture mode of the alloy was confirmed as intergranular type and showed brittle fracture surface. The SCC mechanism of the alloy was concluded as the anodic dissolution model, The maximum hardness was increased from 130Hv in the Sn-free alloy to 156Hv in the 0.10%Sn added alloy.

고강도 Al-Zn-Mg-Cu 합금에서 조성에 따른 응력부식균열 특성 (Stress Corrosion Cracking of High Strength Al-Zn-Mg-Cu Aluminum Alloy with Different Compositions)

  • 김준탁;김상호
    • 한국표면공학회지
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    • 제41권3호
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    • pp.109-113
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    • 2008
  • High strength 7xxx series Al-Zn-Mg alloy have been investigated for using light weight automotive parts especially for bump back beam. The composition of commercial 7xxx aluminum has the Zn/Mg ratio about 3 and Cu over 2 wt%, but this composition isn't adequate for appling to automotive bump back beam due to its high resistance to extrusion and bad weldability. In this study the Zn/Mg ratio was increased for better extrusion and Cu content was reduced for better welding. With this new composition we investigated the effect of composition on the resistivity against stress corrosion cracking. As the Zn/Mg ratio is increased fracture energy obtained by slow strain rate test was decreased, which means degradation of SCC resistance. While the fracture energy was increased with Cu contents although it is below 1%, which means improvement of SCC resistance. These effects of composition change on the SCC resistivity were identified by observing the fracture surface and crack propagation.

고온수중에서 STS 304 스테인리스강의 응력부식균열 성장속도 (Stress Corrosion Crack Rate of STS 304 Stainless Steel in High Temperature Water)

  • 김정기
    • 대한기계학회논문집A
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    • 제24권1호
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    • pp.156-162
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    • 2000
  • Sensitized STS 304 stainless steel crack growth rate(CGR) in high temperature water was investigated under trapezoidal wave loading test using fracture mechanics techniques. The CGR, due to stress corrosion cracking(SCC), were systematically measured as a function of the stress intensity factor and stress. holding time under trapezoidal wave loading. In high temperature water, CGR was enhanced by a synergistic effects in combination with an aggressive environment and mechanical damage. The CGR, $(da/dN)_{env}$ was basically described as a summation of the environmentally assisted crack growth rate $(da/dN)_{SCC}$, $(da/dN)_{CF}$ and fatigue crack growth rate in air $(da/dN)air,. The CGR, $(da/dN)_{env}$, increased linearly with increasing stress holding time. The CGR, $(da/dN)_{SCC}$ decreased linearly with increasing stress holding time. Fracture surface mode varied from trans-granular cracking to inter-granular cracking with increasing stress holding time.

시추코어를 이용한 암석의 mode II 파괴인성 시험법 개발과 적용 (Development and Application of Mode II Fracture Toughness Test Method Using Rock Core Specimen)

  • 정용복;박의섭;김현우
    • 터널과지하공간
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    • 제26권5호
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    • pp.396-408
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    • 2016
  • 암석파괴역학은 토목공학과 암반공학의 다양한 분야에서 널리 적용되는 학문이다. 그러나 대부분의 암반 공학 문제에서 mode II 거동이 우세함에도 불구하고 관련 연구는 mode I 거동에 대한 것이 대부분이다. 현재 mode I의 경우 4개, mode II 파괴인성의 경우 단 한 개의 ISRM 표준시험법이 있다. 본 연구에서 제안하는 새로운 시험법은 문헌조사를 통해서 필요조건으로 구속압 가능 여부, 노치성형의 용이성, 기존 시험장비의 활용, 단순한 시험절차를 정하고 이에 부합하도록 개발하였으며 SCC(Short Core in Compression)로 이름을 정하였다. Mode II 파괴인성 계산에 필요한 응력확대계수 계산식을 3차원 수치해석을 통해 선하중과 분포하중 조건에 대해서 구하였고 노치성형을 위한 지그도 제작하였다. 개발된 시험법을 MTS 시스템을 사용하여 화강암에 적용하였으며 가압속도는 0.002 mm/s로 하였다. 시험 결과 $2.33MPa{\sqrt{m}}$의 mode II 파괴인성을 얻었다. 동일한 화강암 블록에서 확보한 시험편에 대하여 간접인장시험으로 구한 mode I 파괴인성은 $1.12MPa{\sqrt{m}}$였다. 따라서 $K_{IIC}/K_{IC}=2.08$로 mode II 파괴인성이 mode I보다 크게 나타났다. 또한 비교적 매끄러운 파괴면과 암분의 생성을 통하여 SCC 시험법이 mode II 거동을 잘 표현함을 확인하였다. 따라서 제안된 SCC 시험법은 암석의 mode II 파괴인성을 결정하는 데 사용할 수 있을 것으로 판단된다.

요드분위기에서 지르칼로이 피복재의 저변형율속도 의존성(I) (The Slow Strain Rate Dependence of Zircaloy-4 Cladding Tube in Iodine Atmosphere (I))

  • 최용;강영환;류우석;임창생
    • Nuclear Engineering and Technology
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    • 제17권3호
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    • pp.211-215
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    • 1985
  • 온도 및 연신율 변촤가 Zircaloy-4의 요드 응력부식 거동에 미치는 영향을 30$0^{\circ}C$에서 일정 하중법과 300, 350, 40$0^{\circ}C$에서 일정 연신율법으로 ($10^{-5}$sec~$10^{-6}$ sec) 3.34mg $I_2$/㎤의 요드분위기에서 연구하였다. 요드 응력부식균열에 대한 저항성은 온도가 상승하거나 변형속도가 감소하면 감소했고 파손 시간과 응력과의 관계는1/tf∝exp (0.3$\sigma$/$\sigma$uTs-31.5)로 표시할 수 있었다. 30$0^{\circ}C$에서 요드 응력 부식 균열에 대한 저항성을 불활성 분위기에서의 파손에너지에 대한 요드분위기에서의 파손 에너지의 비율로 표시할 때 변형속도가 7.6$\times$$10^{-6}$ sec 부근에서 저항성이 가장 낮았고 온도가 35$0^{\circ}C$, 40$0^{\circ}C$ 로 증가함에 따라 보다 높은 변형속도에서 최저 저항성을 나타내는 경향을 보였다. 요드 응력부식 균열의 파단면에서 준-벽계 파면(quasi-cleavage fracture)을 관찰했다. 전술한 결과에 의하면 Zircaloy-4의 요드 응력부식균열의 기구에 있어서 보호 피막파손단계 (film rupture step)가 중요한 과정으로 추정된다.

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해양구조물용 알미늄 합금의 SCC에 의한 파괴연구 (The Fracture Study of SCC of Al - Alloy for Marine Structures)

  • 김귀식
    • 수산해양기술연구
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    • 제19권1호
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    • pp.79-84
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    • 1983
  • 분극전위변화에 따른 고역 내식성 알미늄합금(5083)의 SCC 거동을 연구 검토한 결과를 요약하면 다음과 같다. 1. 5083 알미늄합금의 K 하(IC)은 134.81~148.38kg/mm 상(3/2)이며, 전위변화에 따라 K 하(Ii)은 75.92~145.78kg/mm 하(3/2)이다. 2. K 하(I)-V의 거동은 양분극시 Region I 과 II가 나타나고, K 하(Ii)/K 하(IC)의 비가 작을수록 crack성장속도도 빠르게 나타난다. 3. 분극전위 -987mV SCE에서 crack성장속도가 가장 지연되므로 122mV SCE을 음분극하면 SCC 방지효과를 얻을 수 있을 것으로 생각된다. 4. 입계의 $\beta$상의 석출은 분극전위가 클수록 크게 나타난다.

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New test method for real-time measurement of SCC initiation of thin disk specimen in high-temperature primary water environment

  • Geon Woo Jeon;Sung Woo Kim;Dong Jin Kim;Chang Yeol Jeong
    • Nuclear Engineering and Technology
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    • 제54권12호
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    • pp.4481-4490
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    • 2022
  • In this study, a new rupture disk corrosion test (RDCT) method was developed for real-time detection of stress corrosion cracking (SCC) initiation of Alloy 600 in a primary water environment of pressurized water reactors. In the RDCT method, one side of a disk specimen was exposed to a simulated primary water at high temperature and pressure while the other side was maintained at ambient pressure, inducing a dome-shaped deformation and tensile stress on the specimen. When SCC occurs in the primary water environment, it leads to the specimen rupture or water leakage through the specimen, which can be detected in real-time using a pressure gauge. The tensile stress applied to the disk specimen was calculated using a finite element analysis. The tensile stress was calculated to increase as the specimen thickness decreased. The SCC initiation time of the specimen was evaluated by the RDCT method, from which result it was found that the crack initiation time decreased with the decrease of specimen thickness owing to the increase of applied stress. After the SCC initiation test, many cracks were observed on the specimen surface in an intergranular fracture mode, which is a typical characteristic of SCC in the primary water environment.

원자력 배관 이종금속 용접부 웅력부식균열의 역학적 평가 (Mechanics Evaluations of Stress Corrosion Cracking for Dissimilar Welds in Nuclear Piping System)

  • 박준수;나복균;김인용
    • 대한용접접합학회:학술대회논문집
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    • 대한용접접합학회 2005년도 추계학술발표대회 개요집
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    • pp.38-40
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    • 2005
  • Fracture mechanics evaluation of stress corrosion cracking (SCC) in the dissimilar metal weld (DMW) for the nuclear piping system is performed; simulating the transition joint of the ferritic nozzle to austenitic safe-end fabricated with the Inconel Alloy A82/182 buttering and welds. Residual stresses in the DMW are computed by the finite element (FE) analyses Then, to investigate the SCC in the weld root under the combined residual and system operation stresses, the fracture mechanics parameters for a semi-elliptical surface crack are evaluated using the finite element alternating method (FEAM). As a result, it is found that the effect of weld residual stresses on the crack-driving forces is dominant, as high as three times or more than the operation stresses.

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