• Proceedings of the Korean Institute of Building Construction Conference
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• 2021.11a
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• pp.252-253
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• 2021

In this study, butyl rubber, which is the main material constituting the self-adhesive butyl rubber waterproofing sheet, was mixed with reclaimed rubber, and tensile strength, tear strength, peeling resistance strength, and adhesion strength were measured for sample prepared by mixing ratio. As a result, it was confirmed that peeling resistance strength and adhesion strength decreased as the reclaimed rubber content increased, and tensile strength and tear strength did not change significantly.

• Journal of the Korean Chemical Society
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• v.45 no.4
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• pp.341-350
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• 2001

Aluminum Hydroxide was employed as a thermal retardent and flame retardent for Chloropolyethylene (CPE) rubbery materials which is the construction material of automotive oil cooler hose. and then cure characteristics, physical properties, thermal resistance and flame retardation of compounded rubber were investigated, and optimum mixing conditions of rubber and flame retarding agent were deduced from the experimental results. CPE rubber material which has excellent properties of chemical corrosion resistance and cold resistance and inexpensive in price was used to prepare rubber specimen. The by-product of ething, produced from the process of surface treatment of aluminum was processed to aluminum hydroxide via crushing and purification, which is characterized by XRD, PSA, SEM and ICP-AES techniques in terms of phase, size, distribution, morphology and components of particles and then mixed to CPE rubber materials in the range of 0~80 phr. Hardness, tensile strength, elongation and thermal properties of compounded rubber specimens were tested. The optimum mixing ratio of rubber to additives to give maximum effect on thermal resistance and flame retardation, within the range of tolerable specification for rubber materials, was determined to be 40 phr. The flame retardation of CPE rubber materials was found to be increased by 5 times at this mixing ratio.

• Elastomers and Composites
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• v.45 no.2
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• pp.112-121
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• 2010

In this study, styrene butadiene rubber(SBR)/organoclay nanocomposites were manufactured using the latex method with 3-aminopropyltriethoxysilane(APTES) as a modifier. The X-ray diffraction(XRD), transmission electron microscopy(TEM) images, Fourier transform infrared(FTIR) spectroscopy, swelling ratio and mechanical properties were measured in order to study the interaction between filler and rubber according to the mixing temperature in the internal mixer. In the case of SBR/APTES-MMT compounds, the dispersion of the silicates within the rubber matrix was enhanced, and thereby, the mechanical properties were improved. The characteristic bands of Si-O-C in APTES disappeared after hydrolysis reaction in the MMT-suspension solution and the peak of hydroxyl group was increased. Therefore the formation of chemical bonds between the hydroxyl group generated from APTES on the silicate surface and the ethoxy group of bis(triethoxysilylpropyl) tetrasulfide(TESPT) was possible. Consequently, the 300% modulus of SBR/APTES-MMT compounds was further improved in the case of using TESPT as a coupling agent. However, the silanization reaction between APTES and TESPT was not affected significantly according to the increase of mixing temperature in the internal mixer.

• Journal of Environmental Science International
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• v.13 no.4
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• pp.421-427
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• 2004

With the help of mechanical mixing method such as Banbury mixer and open 2 roll mill, ethylene propylene diene terpolymer (EPDM) was blended with the chloroprene rubber (CR) then mechanical properties and ozone resistance test of blends were subsequently investigated. It was noted that the hardness increased with an increasing of CR contents. Generally the hardness was increased with heat aging time most likely due to the post cure. In ozone resistance test of blend, after 8 hours a portion of fine crack is obtained for pure CR. It is confirmed that ozone resistance is greatly improved by addition of 25wt% EPDM to CR.

• Textile Coloration and Finishing
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• v.28 no.3
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• pp.183-188
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• 2016

The uniformly dispersed p-Aramid chopped fiber in a variety of rubber was investigated. The cross section and surface properties in a variety of rubber were characterized by scanning electron microscopy(SEM), weight, tensile strength, cold resistance measurements. The 1mm p-Aramid chopped fiber better uniformly dispersed than the other p-Aramid chopped fiber. The p-Aramid of lmm chopped fiber showed excellent adhesion in rubber composite because of homogeneous dispersion. Consequently, the best 1mm chopped fiber and rubber improved the strength of the composite.

• Elastomers and Composites
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• v.46 no.4
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• pp.324-328
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• 2011

Blends were prepared by mixing BR, SBR and NBR to CIIR, which is used for outsole, at various mixing ratio, and effect of the mixing ratio on abrasion resistance and coefficient of friction was analyzed. CIIR interferes the crystalline formation of BR in BR/CIIR blends and this could be one of the factors that rapidly decreases abrasion resistance of BR/CIIR blends. $Tan{\delta}$ peak area of CIIR/BR blends decreased as the amount of BR present in the blends increased, and similarly, the coefficient of friction tended to decrease. Stress relaxation rate and rebound resilience of CIIR/BR blends decreased with increasing BR content, and it was presumed that their rebound resilience was affected by stress relaxation rate.

• Advances in concrete construction
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• v.11 no.5
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• pp.409-417
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• 2021

The incorporation of non-biodegradable tyre waste in cement-based material has gained more interest towards sustainable construction these days. Crumb rubber (CR) from waste tyre is an alternative for sand replacement in low strength applications. Many researchers have studied CR cement-based materials produced by normal mixing (NM) method and reported a significant decrease in compressive strength due to CR. To compensate this strength loss, this research aims to study the innovative incorporation of CR in cement composite via the preplaced mixing (PM) method. In this investigation, cement composite was produced with NM and PM methods by replacing sand with 0%, 50%, and 100% CR by volume. The test results showed no significant difference in terms of densities of cement composite prepared with both mixing methods. However, cement composite prepared with PM method had lower strength reduction (about 10%) and lowered drying shrinkage (about 20%). In addition, the sound absorption coefficient and noise reduction coefficient of CR cement composite prepared by PM method were in similar range as those prepared with NM method. Overall, the results demonstrate that the PM method is promising, and the maximum replacement level of 50% is recommended for CR in the cement composite.

• Design & Manufacturing
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• v.7 no.1
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• pp.55-59
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• 2013

A Light Emitting Diode(LED) is a semiconductor device which converts electricity into light. LEDs are widely used in a field of illumination, LCD(Liquid Crystal Display) backlight, mobile signals because they have several merits, such as low power consumption, long lifetime, high brightness, fast response, environment friendly. In general, LEDs production does die bonding and wire bonding on board, and do silicon and phosphor dispensing to protect LED chip and improve brightness. Then lens molding process is performed using mixed liquid silicon rubber(LSR) by resin and hardener. A mixture of resin and hardener affect the optical characteristics of the LED lens. In this paper, computational design of static mixer was performed for mixing of liquid silicon. To evaluate characteristic of mixing efficiency, finite element model of static mixer was generated, and fluidic analysis was performed according to length of mixing element. Finally, optimal condition of length of mixing element was applied to static mixer from result of fluidic analysis.

• Elastomers and Composites
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• v.51 no.2
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• pp.106-112
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• 2016

Maleimidopropyltriethoxysilane grafted natural rubber (MISNR) was prepared by reaction of maleic anhydride grafted natural rubber and 3-aminopropyl triethoxysilane. MISNR was used as the compatibilizer of natural rubber/silica composites. The composites were prepared by two-step mixing procedures. The final mixtures were cured with optimum cure condition, which was established by a rheometer. Effects of the amounts of compatibilizer in the composites on the cure characteristics, morphology, thermal stability, and physical and mechanical behaviors were investigated. The composites having MISNR had shown cure characteristics and physical and mechanical properties superior to those without MISNR. Silica particles in the former appeared to be more uniform and reduced in size compared with the latter. The effects of the types of silica were also evaluated.

• Elastomers and Composites
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• v.46 no.4
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• pp.329-334
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• 2011

In general, butyl rubber(IIR : isobutylene isoprene rubber) has excellent gas permeability resistance and impact absorbance property as low resilience elastomer. In this experiment butyl rubber blends with EPDM(ethylene propylene diene monomer) were prepared by mechanical mixing method. Curing behavior, physical properties and ozone resistance etc. were subsequently examined. Measurement results of gas transmission rate test shows that butyl rubber contents above 50 wt% showed significant decrease in gas permeability resistant property. However, in butyl rubber/EPDM blend, EPDM contents above 25 wt% indicates no surface change due to improvement of ozone resistance under the condition of 50 pphm, $50^{\circ}C$, 120 hrs.