• Title/Summary/Keyword: Rotational Viscometer

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Correlation between the Properties of Superpave Binder and Engineering Properties of Recycled Aged CRM Mixtures (재생 CRM 바인더와 혼합물의 성능 상관성 연구)

  • Kim, Hyun Hwan;Jeong, Kyu Dong;Lee, Moon Sup;Lee, Soon Jae
    • International Journal of Highway Engineering
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    • v.18 no.2
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    • pp.1-9
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    • 2016
  • PURPOSES : The performance properties (indirect tensile strength, rutting resistance, and resilient modulus) of recycled aged CRM mixtures and their correlation with Superpave binder properties (viscosity, high failure temperature, $G^*sin{\delta}$, and stiffness) were investigated. METHODS: A series of Superpave binder tests was performed by using a rotational viscometer, DSR, and BBR to evaluate the performance properties. In addition, the CRM mixes were artificially aged through accelerated aging processes, and their properties were evaluated. The correlation between the properties of recycled aged CRM binders and the engineering properties of recycled aged CRM mixtures was experimentally determined. RESULTS : The rut depth values decreased and the ITS values increased with increasing high failure temperature. In general, the resilient modulus properties seemed to be poorly correlated with the high-temperature values, regardless of the aggregate source. CONCLUSIONS: The recycled aged CRM binders and mixtures can lead to satisfactory performance, and the properties of these binders are strongly correlated with the engineering properties of the mixtures.

A Comparative Study on the Characteristics of Nanofluids to the Shape of Graphene and Carbon Nanotube (그래핀과 탄소나노튜브의 형상에 따른 나노유체의 열전도도 특성 비교 연구)

  • Park, Sung-Seek;Han, Sang-Pil;Jeon, Yong-Han;Kim, Jong-Yoon;Kim, Nam-Jin
    • Journal of the Korean Solar Energy Society
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    • v.33 no.3
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    • pp.99-106
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    • 2013
  • Recently, high-thermal-conductivity graphene and carbon nanotube nanoparticles have attracted particularly close attention from researchers. In the present study, the thermal conductivity and viscosity properties of two kinds of graphene and carbon nanotube nanofluids added to distilled water - two graphenes and carbon nanotubes of differing size - were compared and analyzed. The thermal conductivities of the nanofluids, formulated in the usual manner by adding graphene and carbon nanotube to distilled water and subjecting the mixture to ultrasonic dispersion, were measured by the transient hot-wire method, and the viscosities were determined using a rotational digital viscometer. As a result, we concluded that the nanofluid of small particle diameter of graphene have outstanding properties as heat transfer media, due to their excellent thermal conductivity and viscosity, compared with the other nanofluid.

The Equilibrium between Dilatant and Thixotropic Flow Units

  • 방정환;김남정;최상원;김응렬;한상준
    • Bulletin of the Korean Chemical Society
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    • v.17 no.3
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    • pp.262-268
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    • 1996
  • Flow properties of all suspensions are controlled by their flow units. The factors effecting on the flow units are the characteristics of the particle itself (surface properties, particle sizes, particle shapes and etc.), the electrostatic interactions among the particles and the influences of the medium in the suspensions. Here, we studied the transition between the flow units with shear rate which can be added to the above factors. For the concentrated starch-water suspensions, by using the Couette type rotational viscometer, we confirmed that at low shear rate, dilatancy is appeared, but it is transformed to thixotropy with increasing shear rate. In order to explain this fact, we derived the following flow equation, representing the transition from dilatancy to thixotropy with shear rate, by assuming the equilibrium between the flow units. f = X1β1s./α1 + 1/(1+Kexp(c0s.2/RT))((1-X1)/α2)sinh-1{(β2)0 s. exp(c2s.2/RT)} + K exp(c0s.2/RT)/(1+K exp(c0s.2/RT))((1-X1)/α3)sinh-1{(β3)0 s. exp(-c3s.2/RT)} By applying this flow equation to the experimental flow curves for the concentrated starch-water suspensions, the flow parameters were obtained. And, by substituting the obtained flow parameters to the flow equation, the theoretical flow curves were reproduced. Also, Ostwald curve was represented by applying the flow equation, and the applicability for stress relaxation was discussed.

A Comparative Study on the Thermal Conductivities and Viscosities of the Pure Water and Ethanol Carbon Nanofluids (순수 물과 에탄올 산화 탄소나노유체의 열전도도 및 점도 특성 비교 연구)

  • An, Eoung-Jiw;Park, Sung-Seek;Chun, Won-Gee;Park, Yoon-Chul;Jeon, Youn-Han;Kim, Nam-Jin
    • Journal of the Korean Solar Energy Society
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    • v.32 no.spc3
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    • pp.213-219
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    • 2012
  • Nanofluids are advanced concept fluid that solid particles of nanometer size are stably dispersed in fluid likes water, ethylene glycol and others. They have higher thermal conductivities than base fluids. If using this characteristic, efficiencies of heat exchangers can be increased. Therefore in this study, we measured thermal conductivity and viscosity of carbon nanofluids. They were made to ultra sonic dispersed oxidized multi-walled carbon nanotubes(OMWCNTs) in distilled water and ethanol, respectively. The mixture ratios of OMWCNTs were from 0.0005 vol% ~ 0.1 vol%. Thermal conductivity and viscosity was measured by transient hot-wire method and rotational viscometer. The results of an experiment are as in the following: thermal conductivity of the 0.1 vol% pure-water nanofluid improved 7.98% ($10^{\circ}C$), 8.34% ($25^{\circ}C$), and 9.14% ($70^{\circ}C$), and its viscosity increased by 37.08% ($10^{\circ}C$), 33.96% ($25^{\circ}C$) and 21.64% ($70^{\circ}C$) than the base fluids. Thermal conductivity of the 0.1 vol% ethanol nanofluids improved 33.72% ($10^{\circ}C$), 33.14% ($25^{\circ}C$), and 32.25% ($70^{\circ}C$), and its viscosity increased by 35.12% ($10^{\circ}C$), 32.01% ($25^{\circ}C$) and 19.12% ($70^{\circ}C$) than the base fluids.

Studies on Rheological Characteristics of Red Pepper Pastes (고추장의 유동(流動) 특성(特性)에 관(關한) 연구(硏究))

  • Pyun, Yu-Ryang;Lee, Shin-Young;Lee, Sang-Kyo;Yu, Ju-Hyun;Kwon, Yoon-Jung
    • Korean Journal of Food Science and Technology
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    • v.12 no.1
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    • pp.18-23
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    • 1980
  • Rheological behaviors of red pepper paste acre investigated with rotational viscometer at $25{\sim}55^{\circ}C$ and the following results were obtained. 1. At shear rate of $0.323{\sim}1.653\;sec^{-1}$, red pepper paste was found to be a thixotropic food product which showed pseudoplastic proper ties and also exhibited a yield stress and time dependent characteristics. 2. At a shear rate of 0.978 $sec^{-1}$, flow behavior index, consistency index and yield stress were 0.597, 192.3 dyne $sec^s/cm^{2}$, and 91 dyne/$cm^{2}$ respectively. 3. Variation of consistency of red pepper paste with time was found to be decayed by a second order kinetic equation and thereafter nearly time independent. 4. Variation of consistency of red pepper paste with temperature was found to follow Andrade's equation and the activation energy as calculated on the basis of this equation was $1.03\;kcal/g{\cdot}mole$.

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Evaluation of Applicability of Heavy Oil Upgrading By-Product (Pitch) as A Pavement Paving Material (중질유 고도정제 부산물의 도로포장용 역청재료로서의 적용성 평가)

  • Yang, Sung Lin
    • International Journal of Highway Engineering
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    • v.16 no.5
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    • pp.9-18
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    • 2014
  • PURPOSES : The objective of this study is to evaluate the applicability of the pitch, which is produced during SDA petroleum upgrading process, as a pavement paving material. In order for the purpose, the physical and chemical properties of the pitch are analyzed, and then the various plasticizers are applied in the pitch. METHODS : Two types of pitch are selected from oil refinery companies, which are owned the SDA petroleum upgrading process. Also, two types of asphalt binders, PG 64-22 and PG 58-22, are employed to compare with the pitch because these two types of asphalt binders are currently used as paving materials. For the chemical property of the pitch, the composition of SARA (Saturate, Aromatic, Resin, Asphaltene), the elementary composition, and the functional group are analyzed. For the physical property of the pitch, the basic material property tests, such as penetration test, softening point test, flash point test, ductility test, and rotational viscometer test, are performed. Also, the DSR (Dynamic Shear Rheometer) test and the BBR (Bending Beam Rheometer) test are conducted using asphalt binder specimens obtained by both short term aging (Rolling Thin Film Oven, RTFO) and long term aging (Pressure Aging Vessel, PAV) processes. The rheological property of each pitch type is evaluated as a function of temperatures and loading cycles. PG 64-22 asphalt binder is used as a control material. RESULTS AND CONCLUSIONS : The Pitch may not be suitable for the pavement paving material without modifications, but the pitch can be used as alternatives of modified addictive or asphalt. If low molecular component, such as saturate and aromatic components, are added in the pitch based on the development of various plasticizers, it has a strong possibility for the pitch to be used as a alternative. However, in order to verify the performance property of the pitch, further research is needed.

Laboratory Performance Evaluation of Recycled Asphalt Binders with Differing Rejuvenators (재생 첨가제를 활용한 재활용 아스팔트 바인더의 실내 공용성 평가)

  • Kim, Yeong Min;Im, Jeong Hyuk;Hwang, Sung Do;Jeong, Kyu Dong;Rhee, Suk Keun
    • International Journal of Highway Engineering
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    • v.17 no.6
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    • pp.55-63
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    • 2015
  • PURPOSES : The objective of this study is to investigate the properties of recycled asphalt binders with five different rejuvenators, in order to evaluate the applicability of the recycled asphalt binders compared with the original asphalt binder. METHODS : In order to simulate recycled asphalt binders, fresh asphalt binders are aged by various Superpave aging procedures, such as the rolling thin-film oven (RTFO) and the pressure aging vessel (PAV). Then, selected rejuvenators are added to the aged asphalt binders in the amount of 5%, 10%, and 15%. The asphalt binder properties are evaluated by the dynamic shear rheometer (DSR), the rotational viscometer (RV), and the bending beam rheometer (BBR). In this study, AP-5 (penetration grade 60-80, PG 64-16) asphalt binder is used. A total of five types of rejuvenators are employed. RESULTS AND CONCLUSIONS : When considering aged asphalt without a new asphalt binder, it seems that the percentage of rejuvenator used in Korea is a bit too low, and that it fails to possess the characteristics of the original binder. From the current practice of evaluating the properties of recycled binder based on penetration ratio only, the amount of rejuvenator required is similar for the long-term-aged binder, but is excessive for the longest-term aged binder, causing deterioration of workability and stiffness of the recycled binder.

A Comparative Study on the Characteristics of the Pure water and Ethanol Carbon Nanofluids for Applying Solar Collector (태양열 집열기 적용을 위한 순수 물과 에탄올 탄소나노유체의 특성 비교 연구)

  • An, Eoung-Jin;Park, Sung-Seek;Chun, Won-Gee;Park, Yoon-Chul;Kim, Nam-Jin
    • 한국태양에너지학회:학술대회논문집
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    • 2012.03a
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    • pp.194-199
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    • 2012
  • In this study, for increasing the efficiency of solar collector, the thermal conductivities and viscosities of the pure water and ethanol oxidized multi-walled carbon nanofluids were measured. Nanofluids were manufactured by ultra-sonic dispersing oxidized multi-walled carbon nanotubes(OMWCNTs) in the pure-water and ethanol at the rates of 0.0005 ~ 0.1 vol%. the Thermal conductivities and viscosities of manufactured nanofluids were measured at the low temperature($10^{\circ}C$), the room temperature($25^{\circ}C$) and the high temperature($70^{\circ}C$). For measuring thermal conductivity and viscosity, we used Transient Hot-wire Method and Rotational Digital Viscometer, respectively. As a result, under given temperature conditions, thermal conductivity of the 0.1 vol% pure-water nanofluid improved 7.98% ($10^{\circ}C$), 8.34% ($25^{\circ}C$), and 9.14% ($70^{\circ}C$), and its viscosity increased by 37.08% ($10^{\circ}C$), 33.96% ($25^{\circ}C$) and 21.64% ($70^{\circ}C$) than the base fluids. Thermal conductivity of the 0.1 vol% ethanol nanofluids improved 33.72% ($10^{\circ}C$), 33.14% ($25^{\circ}C$), and 32.36% ($70^{\circ}C$), and its viscosity increased by 37.93% ($10^{\circ}C$), 31.92% ($25^{\circ}C$) and 29.42% ($70^{\circ}C$) than the base fluids.

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GENE EXPRESSION AFTER THE APPLICATION OF THE FLUID-INDUCED SHEAR STRESS ON THE GINGIVAL FIBROBLAST (유체에 의해 유발된 전단력이 치은 섬유아세포 유전자 발현 변화에 미치는 영향에 관한 연구)

  • Jeong, Mi-Hyang;Choi, Je-Yong;Chae, Chang-Hoon;Kim, Seong-Gon;Nahm, Dong-Seok
    • Maxillofacial Plastic and Reconstructive Surgery
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    • v.27 no.5
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    • pp.424-430
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    • 2005
  • The oral cavity is humid environment mainly due to the continuous salivary flow. The reaction of oral mucosa to fluid flow is important for homeostasis and pathogenesis. The objective of this study is the screening the change of gene expression after the application of fluid induced shear stress (FISS) on the gingival fibroblast using cDNA microarray assay. The immortalized human gingival fibroblasts were grown and FISS was applied using a cone viscometer at a rotational velocity of 40 rpm, respectively for periods of 2 and 4 hours. The synthesis of cDNA was done from the extracted total RNA and cDNA microarray assay was done subsequently. The genes that showed over 1.6 in the Cy3/Cy5 or the Cy5/Cy3 value were regarded as genes influenced significantly by the FISS application ion (/M/>0.7). The " RUNX-1" was increased its expression in 2 hours group and " RUN and SH3 domain containing 1" was increased its expression in 4 hours group. The "CC020415", "cyclin L1", "interferon regulatory factor1", "early growth response 1", "immediate early response 2", and "immediate early response 3" genes were increased their expression in 2 and 4 hours after FISS application. In conclusion, we could find many genes that were probably related to the FISS application. Interestingly, most of them were placed in similar molecular pathways and these findings improve the reliability of chip data and usefulness in overall screening. From this experiment, we could find many items for further study and it will make improvement in the understanding of intracellular events in response to FISS.

Rheological Measurement of Fiber Spinnability of PVA Solution Dopes in DMSO

  • Chae, Dong-Wook
    • Textile Coloration and Finishing
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    • v.22 no.3
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    • pp.187-193
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    • 2010
  • The effects of molecular weight (MW) and concentration on the rheological properties of poly(vinyl alcohol) (PVA) solutions in dimethyl sulfoxide (DMSO) were investigated at $30^{\circ}C$. Ubbelohde viscometer and rotational rheometer were employed for dilute and concentrated regime, respectively. In the dilute regime, the Mark-Houwink exponent ($\alpha$) of the solutions determined from three different MWs proved 0.73. The critical concentration (C*), in which the entanglement and overlap of polymer molecules began to take place, decreased with increasing the MW of PVA. Huggins constant ($K_H$) values ranged from 0.33 to 0.45 over the MW examined. In the log-log plot of $\eta_{sp}$ versus [$\eta$]C, the PVA with higher degree of polymerization (DP) gave a greater slope exhibiting the inflection point in the vicinity of C*. In the dynamic viscosity ($\eta'$) curve, the PVA solutions of DP 1700 presented Newtonian fluid behavior over most of the frequency range examined. However, the lower Newtonian flow region reduced with increasing the DP. As the PVA concentration increased, $\eta'$ was increased and the onset shear rate for pseudoplasticity was decreased. In the Cole-Cole plot, PVA solutions showed almost a single master curve in a slope of ca. 1.65 regardless of the DP. However, the increase of the concentration from 8 to 12 wt% for PVA solutions of DP 5000 decreased the slope from 1.73 to 1.57. In the tan $\delta$ curve, the onset frequency for sol-gel transition was shifted from 154 to 92 rad/s with increasing the DP from 3300 to 5000 and from 192 to 46 rad/s with increasing the concentration from 8 to 12 wt%. In addition, longer relaxation time ($\lambda$) was observed with increasing the DP and concentration.