• Journal of the Korean Ceramic Society
• /
• v.32 no.9
• /
• pp.1056-1064
• /
• 1995

95Pb(Mg1/3Nb2/3)O3-5PbTiO3 (hereinafter designated as 95PMN-5PT) system was prepared by the columbite-precursor method with 2 mol% excess PbO to compensate the PbO loss during thermal process. The amount of CuO was 1~10 mol%, and the effects of CuO addition on the dielectric properties of this system have been investigated. From the microstructures, XRD analysis and dielectric measurements, the solubility limit of CuO in 95PMN-5PT was found to be around 3 mol%. Lattice parameter and Curie temperature were found to be decreased as the amount of CuO increased up to the solubility limit. This result confirmed that the Cu2+-ions substituted the Pb2+-ions. It was revealed that the addition of CuO on 95PMN-5PT promoted the sinterability and properties. The room temperature dielectric constant, the loss factor and the specific resistivity of the specimens processed with optimum conditions were 23000, 1%, and 8$\times$1011Ω.cm, respectively.

• Journal of Magnetics
• /
• v.11 no.3
• /
• pp.126-129
• /
• 2006

The phosphate coating on the $(Fe_{0.97}Cr_{0.03})_{76}(Si_{0.5}B_{0.5})_{22}C_2$ amorphous powders with an average size of 10 ${\mu}m$ in diameter has been carried out in aqueous 1.0-2.0 wt% $H_3PO_4$ solutions, and the consolidation behavior and magnetic properties of their compressed powder cores has been investigated. The phosphate coating could provide efficient electrical insulation between amorphous powders and improved consolidation ability at room temperature. Especially when the powders were treated in more concentrated phosphoric acid solution, enhanced phosphate covering and higher frequency/dc-bias stability were achieved. The powder cores phosphate-coated in 2.0 wt% $H_3PO_4$ solution exhibited constant permeability of 21 up to 10 MHz, 110 of the quality factor at 0.9 MHz, 610 mW/cm3 core loss at 100 kHz/0.1 T and 89 of percent permeability at 100 kHz.

• Journal of Magnetics
• /
• v.12 no.4
• /
• pp.137-140
• /
• 2007

We have studied the temperature dependent magnetic properties and crystalline phase transitionn in small amount Fe doped nickel chromite. The Crystalline structure of $NiCr_{1.7}Fe_{0.3}O_4$ is spinel cubic (Fd-3m) structure with a lattice constant $a_0=8.317\AA$ at room temperature. The magnetic $N\acute{e}el$ temperature $(T_N)$ of the Fe doped nickel chromite sample is determined to be 250 K. The $M\ddot{o}ssbauer$ spectra exhibit that there are two magnetic phases with the two different sites for the $Cr^{3+}$ ions. The spectrum at 4.2 K is fitted to two magnetic components of the magnetic hyperfine fields $H_{hf}=496$ and 485 kOe. From the spectrum at 295 K, the electric quadrupole splittings are observed with large values of 0.49 and 0.50 mm/s, respectively. The values of the isomer shifts at all temperature ranges show that the Fe ions are ferric states. We are suggested that the dynamic Jahn-Teller distortion and anisotropic magnetic relaxation effects due to the crystalline phase transition.

• 한국태양에너지학회:학술대회논문집
• /
• 2011.04a
• /
• pp.199-203
• /
• 2011

With the improvement of standard of manufacturing process, oil cooling unit for manufacturing machine has been developed. A control system must be designed in order to keep oil temperature of the machine within a very restricted range and also to reduce energy consumption. In order to get the low deviation of the controlled temperature and the low efficiency, the on/off control scheme is gradually being replaced by a variable speed refrigeration system (VSRS) with an inverter driven compressor over recent decades. This paper gives the flowchart to control the compressor speed and also the electronic expansion valve (EEV) aperture in oil cooling unit refrigeration system using R22 as the refrigerant. This control scheme has already tested in experiment apparatus with room temperature condition constant at $25^{\circ}C$ and variable load condition at 4kW, 6kW, 7kW, 8kW and 10kW.

• Journal of Power System Engineering
• /
• v.18 no.2
• /
• pp.62-69
• /
• 2014

In this paper, in order to investigate the effects of marco and microscopic observations of fatigue crack growth in friction stir welded (FSWed) 7075-T651 aluminum alloy plates, fatigue crack growth tests were performed under constant amplitude loading condition at room temperature with three different pre-cack locations, namely base metal (BM-CL) and two kinds of pre-crack locations in welded joints, weld metal (WM-CL) and heat affected zone (HAZ-CL) specimens. The fatigue crack growth behavior of FSWed 7075-T651 aluminum alloy plates were discussed based on the marco and microscopic fractographic observations. The marcoscopic aspects of surface crack growth path for BM-CL and HAZ-CL specimens indicate relatively straight lines, however, the crack growth paths of WM-CL specimens grow first straight and by followed toward the TMAZ and HAZ. The microscopic aspects of fatigue fracture for BM-CL and HAZ-CL specimens indicate typical fatigue striation, but WM-CL showed intergranular fracture pattern by micro structural changes of FSW process.

• Transactions of Materials Processing
• /
• v.19 no.6
• /
• pp.357-362
• /
• 2010

Dry sliding wear behavior of pure Fe and Cu which have BCC and FCC crystal structure, respectively, was investigated. The wear characteristics of the pure metals with different crystal structure were compared. Dry sliding wear tests were carried out using a pin-on-disk wear tester at various loads under the constant sliding speed condition of 0.15 m/s against a silica ball at room temperature. Sliding distance was fixed as 600 m for all wear tests. Wear rate of a specimen was calculated by dividing the weight loss of the specimen after the test by the specific gravity and sliding distance. Worn surfaces and wear debris were analyzed by SEM. The wear of both pure Fe and Cu proceeded with surface deformation, resulting in similar wear rates despite of their structure difference under the current test conditions. Wear rates of both metals were low if the surface deformation due to wear forms thick surface-deformation layer that is strain hardened beneath the wearing surface. The pure Cu specimens showed a lot of oxides on the worn surface when tested at low loads less than 5 N, which resulted in very low wear rate.

• Transactions of the Korean Society of Mechanical Engineers
• /
• v.12 no.1
• /
• pp.152-162
• /
• 1988

In recent years, attention has been paid to the ceramic material next to metals and plastics due to its inherent characteristics, i.e., good hardness, resistance to heat and corrosion. Recently, various kinds of ceramic dielectrics have been developed for application in industry. It is of prime importance to know the thermophysical properties for wider use of these new materials. However, no extensive effort has been made for systematic measurement of the properties. In this paper, the dielectric constant of five different kinds of ceramic dielectrics ware measured. We call these samples as MgO.SiO$_{2}$, MgTiO$_{3}$, TiO$_{2}$, CaTiO$_{3}$, and BaTiO$_{3}$. Which are currently in commercial sue. The values of thermal dirrusivities, specific heats, and thermal conductivities of these ceramic dielectrics sere measured as a function of temperature ranging from room temperature to about 1300k.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.28 no.12
• /
• pp.847-851
• /
• 2015

The effects of Al-substitution on thermoelectric and charge transport properties of BiCuOSe compounds were investigated. The compounds were prepared by a solid-state reaction and consolidated by SPS (spark plasma sintering). In spite of the increase in the hole concentration with increasing Al amounts in BiCuOSe compound, the electrical conductivity at room temperature was kept constant due to the reduction of mobility. However, electrical conductivities of Al-substituted BiCuOSe compounds at elevated temperature (> 600 K) were higher than those of BiCuOSe, and this result was discussed in terms of it's the band gap energy. The Seebeck coefficient was drastically reduced when Al was substituted in Bi site, which indicated that the electronic structure was influenced by the Al-substitution into Bi-site.

• Journal of The Korean Society of Agricultural Engineers
• /
• v.57 no.6
• /
• pp.131-140
• /
• 2015

This paper presents overall procedure by experimental study in order to deriving design factors of snow removal machine on roof of multi-span greenhouse. For the purpose of the testing, the scale model of the machine was made in the form to drive above the monorail. The test was performed in order to calculating friction coefficient of the machine and shear coefficient between sliced horizontal section of snow at constant temperature and humidity room in National Academic of Agricultural Science. As a result of the laboratory test, shear coefficient between sliced horizontal section of snow were calculated 1.60~2.37. Further investigation, we will study to derive the relationship between the real and scaled model through the field test.

• YAKHAK HOEJI
• /
• v.36 no.5
• /
• pp.506-511
• /
• 1992

The Prostaglandins were derivatized rapidly with monodansyl cadaverine as a fluorophore in mild conditions. The carboxylic moiety of prostaglandins was activated with diethyl phosphorocyanidate and successively coupled with fluorophore in dimethylformamide at room temperature. The labeling yield was reached about 95% at 15 min using arachidic acid $(C_{20:0})$ as a test sample. This derivative showed constant fluorescent intensity at $4^{\circ}C$ for 180 days. The derivatives of prostaglandins were shown high solvent selectivity with tetrahydrofuran in reversed-phase column. therefore, these derivatives could be successfully separated on YMC pack A-212(S-5 120A C8) column in tetrahydrofuran-based eluents. The detection limits of these derivatives was ca. 500 fmol and determination limits was ca. 5 pmol as injected amount in fluorescent detection $({\lambda}ex.\;340\;nm,\;{\lambda}em.\;520\;nm)$. In this method, the ranges of recovery and coefficient of variation were $93.6{\sim}102.7%$ and $4.3{\sim}5.8%$, respectively.