• 제목/요약/키워드: Rock specimens

검색결과 292건 처리시간 0.028초

이온보조반응법으로 처리한 알루미나 코아의 인장결합강도에 관한 연구 (TENSILE BOND STRENGTH OF ALUNMINA CORE TREATED BY ION ASSISTED REACTION)

  • 김형섭;우이형;권긍록;최부병;최원국
    • 대한치과보철학회지
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    • 제38권5호
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    • pp.704-723
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    • 2000
  • This study was undertaken to evaluate the tensile bond strength of In-Ceram alumina core treat-ed by ion assisted reaction(IAR). Ion assisted reaction is a prospective surface modification technique without damage by a keV low energy ion beam irradiation in reactive gas environments or reactive ion itself. 120 In-Ceram specimens were fabricated according to manufacturer's directions and divided into six groups by surface treatment methods of In-Ceram alumina core. SD group(control group): sandblasting SL group: sandblasting + silane treatment SC group: sandblasting + Siloc treatment IAR I group: sandblasting + Ion assisted reaction with argon ion and oxygen gas IAR II group: sandblasting + Ion assisted reaction with oxygen ion and oxygen gas IAR III group: sandblasting + Ion assisted reaction with oxygen ion only For measuring of tensile bond strength, pairs of specimens within a group were bonded with Panavia 21 resin cement using special device secured that the film thickness was $80{\mu}m$. The results of tensile strength were statistically analyzed with the SPSS release version 8.0 programs. Physical change like surface roughness of In-Ceram alumina core treated by ion assistad reaction was evaluated by Contact Angle Measurement, Scanning Electron Microscopy, Atomic Force Microscopy; chemical surface change was evaluated by X-ray Photoelectron Spectroscopy. The results as follows: 1. In tensile bond strength, there were no statistically significant differences with SC group, IAR groups and SL group except control group(P<0.05). 2. Contact angle measurement showed that wettability of In-Ceram alumina core was enhanced after IAR treatment. 3. SEM and AFM showed that surface roughness of In-Ceram alumina core was not changed after IAR treatment. 4. XPS showed that IAR treatment of In-Ceram alumina core was enabled to create a new functional layer. A keV IAR treatment of In-Ceram alumina core could enhanced tensile bond strength with resin cement. In the future, this ion assisted reaction may be used effectively in various dental materials as well as in In-Ceram to promote the bond strength to natural tooth structure.

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조립재료의 입도특성에 따른 동적 변형특성 평가 (Dynamic Deformation Properties of Coarse Granular Materials with Respect to Gradation Characteristics)

  • 하익수;김남룡
    • 한국지반공학회논문집
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    • 제29권8호
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    • pp.5-14
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    • 2013
  • 굵은 자갈 이상의 대입경 입자를 포함하는 조립질 지반재료는 댐, 제방, 철도 등 대형 지반구조물의 성토 및 채움재료로 널리 사용되며, 이러한 구조물의 동적 해석을 위해서는 축조재료의 변형특성에 대한 엄밀한 평가가 필수적이다. 본 연구에서는 대입경 조립재료의 동적 변형특성 평가를 위하여 지름 200mm, 높이 400mm의 공시체에 대한 시험이 가능하도록 개발된 대형 공진주시험기를 활용하여 댐 축조용 사력재의 최대전단탄성계수, 전단탄성계수감소곡선 및 감쇠비를 평가하였으며, 재료의 최대입경과 균등계수와 같은 입도분포특성이 재료의 변형특성에 미치는 영향을 확인하였다. 재료의 입경이 동적 변형특성에 미치는 영향을 평가한 결과, 동일한 균등계수에서 평균입경의 범위에 따른 전단탄성계수감소곡선에 차이가 발생함을 확인하였다. 동일한 최대입경에 대하여 균등계수를 달리하는 경우 균등계수에 따라 최대전단탄성계수의 구속압 영향계수가 증가함을 확인하였다. 결과적으로 조립재료의 입도 특성 중 최대입경은 전단탄성계수감소곡선을, 균등계수는 미소변형영역의 구속압 영향계수에 대한 영향요소임을 확인하였으며, 조립재료의 동적 변형특성을 엄밀히 평가하기 위한 대형 공진주시험기의 효용성을 확인하였다.

인공치의 표면처리가 3D 프린팅 의치상레진과의 전단결합강도에 미치는 영향 (Effect of surface treatment on shear bond strength between artificial resin teeth and 3D printing denture base resin)

  • 최지혜;이영후;홍성진;백장현;노관태;배아란;권긍록;김형섭
    • 대한치과보철학회지
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    • 제58권4호
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    • pp.300-305
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    • 2020
  • 목적: 인공치의 표면처리가 3D 프린팅 의치상레진과의 전단결합강도에 미치는 영향을 알아보고 임상적용에 있어 참고하기 위함이다. 재료 및 방법: 3D 프린팅 의치상레진을 3D 프린터를 이용하여 시편을 제작하였고, 인공치의 표면처리는 sandblasting, 프라이머의 적용 유무에 따라 5가지 군으로 나누어, 각 군마다 10개씩 진행하였다. Universal testing machine을 이용하여 전단 결합 강도를 측정하였고, 측정값은 one-way ANOVA로 통계분석 후 Turkey test를 통해 사후검정하였다. 이후 파절된 시편을 주사전자현미경을 이용하여 관찰하였다. 결과: 평균전단결합강도는 표면 처리 하지 않은 군에서 가장 낮은 값을 나타내었으며, 프라이머 처리한 군에서 유의하게 높은 결과 값을 나타내었다(P < .05). 또한 프라이머 처리한 군에서 대부분 응집파절을 나타내었다. 결론: 3D 프린팅 의치상레진에 인공치를 결합 시 인공치의 기계적·화학적 표면처리는 전단결합강도를 증가시켜 3D 프린팅 방식을 사용하여 의치를 제작할 경우 기계적·화학적 표면처리를 통해 인공치의 탈락을 줄일 수 있으며, 특히 sandblasting 과 프라이머를 처리하는 방법이 추천된다.

처분 복합환경을 고려한 KURT 화강암의 Mazars 손상모델 평가 (Evaluation of Mazars damage model of KURT granite under simulated coupled environment of geological disposal)

  • 김진섭;홍창호;김건영
    • 한국터널지하공간학회 논문집
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    • 제22권4호
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    • pp.419-434
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    • 2020
  • 본 연구에서는 처분장의 장기 건전성 평가모델을 확보하기 위해 한국원자력연구원 내 지하처분연구시설의 화강암을 대상으로 심층 처분복합환경을 모사한 암석시편의 Mazars 손상모델 상수를 측정하였다. 이를 위하여 실제 처분장 특성을 고려한 3가지 온도(15℃, 45℃, 75℃)와 건조/포화 조건에서 일축압축강도 및 간접인장강도 실험을 수행하였다. 최대유효인장변형률, At, Bt, Ac, Bc 등 주요 파라미터들은 콘크리트 대상으로 연구된 참고문헌의 값들과 차이를 보였으며 이는 암석과 콘크리트 시료의 탄성계수 차이 때문으로 판단된다. 시험결과 시료의 포화로 인해 Bt와 Bc의 값은 증가하였다. 또한 온도증가로 인해 최대 유효인장변형률과 Bt는 증가하였고 Bc는 감소하는 것을 확인하였다. 본 연구를 통해 도출된 손상모델은 한국원자력연구원 내에서 현재 개발 중인 Coupled Thermo-Hydro-Mechanical Damage 수치해석의 손상모델로 이용될 계획이다.

STRAIN CHANGES OF ACRYLIC RESIN SPECIMENS CURED BY THREE CURING CYCLES

  • Kang, In-Ho;Kim, Yung-Soo;Kim, Chang-Whe
    • 대한치과보철학회지
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    • 제40권3호
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    • pp.236-245
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    • 2002
  • The acrylic resin was first introduced as denture base materials in 1937 and it is commonly used for denture base fabrication nowadays. Three different curing cycles (Conventional curing cycle, short curing cycle and long curing cycle) and three commercially available heat-activated acrylic resins (Vertex RS, Lucitone 199 and ProBase Hot) were investigated to find the curing cycle and material that showed the minimum shrinkage of the resin during polymerization process. A brass master mold was fabricated and duplicated by additional silicone impression material. Stone molds were made by pouring of type III dental stone (SILKY-ROCK YELLOW, Whip-Mix, Louisville, Kentucky). It was embedded in the flask. Strain gauge and thermocouple were embedded in the specimen. Strain gauge and thermocouple were connected to signal conditioning amplifier and data was recorded by pre-programmed software. The parameters ESmax (Maximum expansion strain), Sb (Strain measured just before deflasking procedure), Sa (Strain measured just after deflasking procedure) and Sf (Strain measured at the end of the experiment) were measured. ${\Delta}$S was calculated from Sb and Sa (${\Delta}$S=Sb-Sa). In the experiment concerned about materials, the parameters 90-ESmax (Maximum expansion strain measured during early 90 minutes of curing procedure), 180-ESmax (Maximum expansion strain measured from 90 minutes to 180 minutes), Sb, Sa, ${\Delta}$S and Sf were measured and the following conclusions were made. 1. The ESmax value of conventional curing cycle showed the largest value and the 180-ESmax value of Lucitone 199 showed the smallest value. 90-ESmax values showed no significant difference (p<0.05). 2. ${\Delta}$S values of conventional curing cycle showed the positive values. ${\Delta}$S values of short curing cycle and long curing cycle showed the negative values. All three materials cured by conventional curing cycle showed the positive values. 3. The Sf values of long curing cycle and ProBase Hot (cured by conventional curing cycle) showed the smallest values.

Impact of surface roughness of gypsum materials on adaptation of zirconia cores

  • Kim, Ki-Baek;Kim, Jae-Hong;Kim, Sa-Hak
    • The Journal of Advanced Prosthodontics
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    • 제7권3호
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    • pp.199-206
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    • 2015
  • PURPOSE. The present study investigated the influences of various gypsum materials on the precision of fit of CAD/CAM-fabricated prostheses and analyzed their correlation with surface roughness. MATERIALS AND METHODS. The master model of the mandibular right first molar was replicated, and four experimental groups based on two types of Type IV stone (GC Fujirock EP, Die keen) and two types of scannable stone (Aesthetic-Basegold, Everest Rock) were created to include a total of 40 specimens, 10 in each group. The surface roughness of the working models for the respective experimental groups was measured. Once the zirconia cores had been fabricated, the marginal and internal fits were measured with a digital microscope using the silicone replica technique. The mean and standard deviation of the respective points of measurement were computed and analyzed through the one-way ANOVA and Tukey's HSD test. The correlation between surface roughness and the precision of fit of the zirconia core was analyzed using the Pearson correlation analysis (${\alpha}$=.05). RESULTS. The zirconia cores fabricated from the scannable stone working models exhibited a superior precision of fit as compared to those fabricated from the Type IV stone working models. The correlation analysis results showed a clear positive correlation between surface roughness and the precision of fit of zirconia cores in all of the experimental groups (P<.05). CONCLUSION. The results confirmed that the surface roughness of dental working models has a decisive influence on the precision of fit of zirconia cores.

옥상녹화용 방근층 구성재료의 방근성능에 관한 실험적 연구 (Resistance to Root Penetration of Root Barrier for Green Roof System)

  • 김현수;장대희;최수경
    • 한국건축시공학회지
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    • 제8권6호
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    • pp.123-129
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    • 2008
  • The purpose of this study is to test performances of 14 types of root barrier materials by applying testing plant: and soils suitable for weather and natural features of Korea. For testing Plants, Plioblastus pygmaed Mitford A and Pyracantha angustifolia have been selected. For testing soil, mixture of pearlite and peat moss in 3:1 ratio Testing container has been fabricated with duplicated structure having inner and outer containers. And the outer container has 2 hinges on its side wall to allow opening and closing. Wet rock wool with 50mm in thickness has been inserted between inner and outer containers to allow root to penetrate through root barrier material and continue to grow. We planted 12 Plioblastus pygmaed Mitford A. and 4 Pyracantha angustifolia per one testing container. Three testing samples have been made for 1 type of root barrier material, which become a total 42 specimens. Planted testing samples have been installed within the greenhouse, which will be observed regularly for 2 years from now on. We started test from July 11, 2008 and had performed intermediate observations every month for initial 3 months. From the 3rd intermediate observation on Sept. 18, we confirmed that 6 types of roe barrier materials have penetrated roots. Even though two types of them have been generally used as root barrier materials for roof planting system, all of three testing samples have a lot of penetrated roots. This result proves that it is not reasonable to introduce testing methods of root barrier from Europe. USA or Japan.

경북(慶北) 봉화군에 분포(分布)는 장산규암층(壯山硅岩層)의 암석학적(岩石學的) 및 지구화학적(地球化學的) 연구(硏究) (Petrological and Geochemical Studies on Quartzite from the Jangsan Quartzite Formation in the Bonghwa-Gun, Korea)

  • 안건상;이현구
    • 자원환경지질
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    • 제28권1호
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    • pp.43-51
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    • 1995
  • The Jangsan Quartzite is a basal unit of the Cambro-Odovician sequence, in Socheon-Myeon, Bonghwa-Gun, Gyeongsangbug-Do, South Korea, was petrologically and geochemically investigated. The quartzite consists mainly of quartz and muscovite, assosiated with tourmaline and graphite. The quartzite shows white and/or gray color and various green color in hand specimens. The white and gray colored rocks have very low vanadium contents, but a dark green colored rock contains 8960 ppm vanadium. The muscovites in the quartzite show colorless and green color, of which green ones range from pale blue green to pale green. The dark green colored muscovites have above 8 wt. % vanadium and pale green ones have 1-3 wt. % vanadium. Vanadium contents in moscovite increase with decreasing $Al^{v1}$ contents. It suggests that vanadium substitutes for octahedral aluminium in moscovite. In general, it tends to large volumes of muscovite (up to 14 modal %) in deep green colored rocks, and high vanadium contents in their muscovites. Most of the moscovite flakes occur along the quartz boundaries and some are enclosed by quartz grain. The moscovite grains intergrowth each other in the former. The mouscovite aggragates are divided into two types on the basis of their intergrowth(cut) times. Two cut times and one cut time are named T type and D type, respectively. The T type is mainly distributed at western part (near of the Chunyang granite), whereas the D type is distributed from middle to estern part(near the Janggunbong) of the formation. The boundary is consistent with metamorphic isograd between andalusite and sillimanite zone by Ahn et. al. (1993).

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국내 바다거북류의 출현 현황과 주요 출현 2종의 형태적 특징 (Occurrence of Sea Turtles in the Korean Waters and the Morphological Characteristics of Two Major Species)

  • 김일훈;문대연;조인영;김민섭;안용락;한동욱;한원민;한동진;박대식
    • 한국수산과학회지
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    • 제50권3호
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    • pp.311-318
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    • 2017
  • Four species of sea turtles (Chelonia mydas, Caretta caretta, Dermochelys coriacea, and Eretmochelys imbricata) have been recorded in Korean waters. However, nationwide surveys on the distribution and occurrence of each species have rarelybeen conducted in Korean waters. In this study, we comparatively analyzed the trends in occurrence of sea turtles and their morphological characteristics based on 148 reliable observations and stuffed specimen data and suggested Korean names for each species. Chelonia mydas (57 cases, 58.8%) and C. caretta (52 cases, 31.5%) were dominant species, and occupied > 90% of all observations. Most of observations of sea turtles in Korean waters were obtained through stranding (61 cases) and incidental catches (62 cases). A coastal set net was the main fishing gear for incidental catches (82%). Sea turtles were found mainly around Jeju-do and the Korea Strait from June to November. Most C. caretta found were adults, whereas most C. mydas were juveniles. Additionally, we provide detailed morphological characteristics of C. mydas (n=8) and C. caretta (n=4) using stuffed specimens. Finally, based on a literature search, we suggest appropriate Korean names, such as "Pureunbada-geobuk" for C. mydas, "Bulgeunbadageobuk" for C. caretta, "Jangsu-geobuk" for D. coriacea, and "Maeburibada-geobuk" for E. imbricate.

옥상녹화용 방근층의 방근성 시험조건 설정 및 주요 방근소재에 대한 3개월간의 중간관찰 결과 (Examination Conditions of Root Barrier for Green Roof System and Result of Intermediate Observation of Three Months against Representative Root Barrier)

  • 신윤호;장대희;김현수;최수경
    • 한국건축시공학회:학술대회논문집
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    • 한국건축시공학회 2008년도 추계 학술논문 발표대회
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    • pp.245-249
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    • 2008
  • The purpose of this study is to test performances of 14 types of root barrier materials by applying testing plants and soils suitable for weather and natural features of Korea. For testing plants, Plioblastus pygmaed Mitford A. and Pyracantha angustifolia have been selected. For testing soil, mixture of pearlite and peat moss in 3:1 ratio(volume). Testing container has been fabricated with duplicated structure having inner and outer containers. And the outer container has 2 hinges on its side wall to allow opening and closing. Wet rock wool with 50mm in thickness has been inserted between inner and outer containers to allow root to penetrate through root barrier material and continue to grow. We planted 12 Plioblastus pygmaed Mitford A. and 4 Pyracantha angustifolia per one testing container. Three testing samples have been made for 1 type of root barrier material, which become a total 42 specimens. Planted testing samples have been installed within the greenhouse, which will be observed regularly for 2 years from now on. We started test from July 11, 2008 and had performed intermediate observations every month for initial 3 months. From the 3rd intermediate observation on Sept. 18, we confirmed that 6 types of root barrier materials have penetrated roots. Even though two types of them(EDPM Sheet, Polyethylene Sheet) have been generally used as root barrier materials for roof planting system, all of three testing samples have a lot of penetrated roots. This result proves that it is not reasonable to introduce testing methods of root barrier from Europe or Japan.

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