• 분석과학
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• 제6권2호
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• pp.217-223
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• 1993

저항가열식 진공중착기를 이용하여 실온(ambient temp.)과 $250^{\circ}C$에서 알루미나 기판 위에 Au/Cr, Au/Ni/Cr 및 Au/Pd/Cr 박막을 제조하였으며, 공기 중에서 $300^{\circ}C$, $450^{\circ}C$, $600^{\circ}C$의 온도로 각각 1시간 동안 열처리하였다. Au, Ni(또는 Pd) 및 Cr 박막의 두께는 각각 $1000{\AA}$, $300{\AA}$, 및 $50{\AA}$이었다. 박막 제조시 기판의 온도와 박막 제조 후 열처리 온도는 각 층의 상호확산으로 인하여 박막의 면저항값에 영향을 주었다. Auger depth profile 분석결과, Au/Cr 시스템에서는 기판의 온도는 $250^{\circ}C$로 하여 박막을 제조할 때 이미 Cr은 Au 표면으로 확산되었으며, 열처리 후에는 Au의 분포도만 변화하였다. Au/Ni/Cr과 Au/Pd/Cr 시스템의 경우 Ni와 Pd 모두 확산현상이 발견되었으며, 특히 Ni(약 45 at.%)는 Au 박막 표면으로 확산되어 산화되었다.

• Elastomers and Composites
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• 제15권3호
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• pp.147-154
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• 1980

The cellular rubber products for industrial purpose have been applied in many fields such as auto-motive parts, ship-building, machinery, sports goods, diving suit or interior housings etc. The purpose of this dissertation is to study the physical properties of celluar rubber products particulary for those elastomers such as EPDM, CR and NBR with heat resistance property, weather proofness, and oil resistance characteristics respectively, aiming at improving their quality, and renovating the manufacturing know-how which is beyond our technical power at the present time in Korea. In order to meet this requirement an ideal recipe is being shown for the three elastomers, and also a practical recipe which is easily available in terms of compounding ingredients in domestic market has set up as shown in Table 1. for the investigation of vulcanization characteristics by means of Rheometer. The optimum Mooney viscosity of compounded rubber was found to be approximately $ML_{1+4}(100^{\circ}C)$ $30\sim45$. Excess mustication makes a dispersion of ingredients worse, consequently it causes deformation of shapes and heterogenous cell distribution. In other words the articles are rejected because of its insufficient workmanship. The results of physical properties of the products are indicated in Table 3. It has shown that the quality meet requirement when tested in accordance with ASTM D572, 573 and D 395. The test results o CR/IR blends in terms of hardness, volume change by blowing, tensile strength and elongation have been shown.

• The Journal of Advanced Prosthodontics
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• 제16권2호
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• pp.115-125
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• 2024

PURPOSE. The purpose of this in vitro study was to investigate the fracture resistance, surface hardness, and color stain of 3D printed, CAD-CAM milled, and conventional interim materials. MATERIALS AND METHODS. A total of 80 specimens were fabricated from auto polymerizing polymethyl methacrylate (PMMA), bis-acryl composite resin, CAD-CAM polymethyl methacrylate resin (milled), and 3D printed composite resin (printed) (n = 20). Forty of them were crown-shaped, on which fracture strength test was performed (n = 10). The others were disc-shaped specimens (10 mm × 2 mm) and divided into two groups for surface hardness and color stainability tests before and after thermal cycling in coffee solution (n = 10). Color parameters were measured with a spectrophotometer before and after each storage period, and color differences (CIEDE2000 [DE00]) were calculated. The distribution of variables was measured with the Kolmogorov Smirnov test, and one-way analysis of variance (ANOVA), Tukey HSD, Kruskal-Wallis, Mann-Whitney U tests were used in the analysis of quantitative independent data. Paired sample t-test was used in the analysis of dependent quantitative data (P < .05). RESULTS. The highest crown fracture resistance values were determined for the 3D printed composite resin (P < .05), and the lowest were observed in the bis-acryl composite resin (P < .05). Before and after thermal cycling, increase in mean hardness values were observed only in 3D printed composite resin (P < .05) and the highest ΔE₀₀ value were observed in PMMA resin for all materials (P < .05). CONCLUSION. 3D printing and CAD-CAM milled interim materials showed better fracture strength. After the coffee thermal cycle, the highest surface hardness value was again found in 3D printing and CAD-CAM milled interim samples and the color change of the bis-acryl resin-based samples and the additive production technique was higher than the PMMA resin and CAD-CAM milled resin samples.

• Structural Engineering and Mechanics
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• 제47권5호
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• pp.623-641
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• 2013

The fiber-reinforced polymer (FRP) composite panel, with the benefits of light weight, high strength, good corrosion resistance, and long-term durability, has been considered as one of the prosperous alternatives for structural retrofits and replacements. Although with these advantages, a further application of FRPs in bridge engineering may be restricted, and that is partly due to some unsatisfied thermal performance observed in recent studies. In this regard, Kansas Department of Transportation (DOT) conducted a field monitoring program on a bridge with glass FRP (GFRP) honeycomb hollow section sandwich panels. The temperatures of the panel surfaces and ambient air were measured from December 2002 to July 2004. In this paper, the temperature distributing behaviors of the panels are firstly demonstrated and discussed based on the field measurements. Then, a numerical modeling procedure of temperature fields is developed and verified. This model is capable of predicting the temperature distributions with the local environmental conditions and material's thermal properties. Finally, a parametric study is employed to examine the sensitivities of several temperature influencing factors, including the hollow section configurations, environmental conditions, and material properties.

• 대한기계학회논문집B
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• 제25권6호
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• pp.819-828
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• 2001

The operating point of a small-sized axial fan is strongly dependent upon the system resistance. Therefore, the turbulent flow characteristics around a small-sized axial fan may change significantly according to the operating point. This study represents three-dimensional turbulent flow characteristics around a small-sized axial fan measured at the ideal design point $\phi$=0.25, which is equivalent to the maximum total efficiency point, by using three dimensional fiber-optic type LDA system. This LDA system is composed of a 5 W Argon-ion laser, two optics in back-scatter mode, three BSAs, a PC, and a three-dimensional automatic traversing system. A kind of paraffin fluid is used to supply particles by means of fog generator. Mean velocity profiles downstream of a small-sized axial fan along the radial distance show that the streamwise and the tangential components exist in a predominant manner, while the radial component has a small scale distribution and shows the inflection which its flow direction is inward or outward. Moreover, the turbulent intensity profiles show that the radial component exists the most greatly among turbulent energies.

• Composites Research
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• 제14권2호
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• pp.33-42
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• 2001

DSC(differential scanning calorimetry)를 이용하여 S2-유리섬유/폴리에스터 프리프레그 복합재료의 경화반응식을 구성하였다. 구성된 경화식과 블리더의 수지 함침에 의한 열전달 조건의 변화를 고려하여, 두꺼운 복합재료의 두께 방향 위치에 따른 온도분포를 계산하였다. 유래섬유 복합재료의 경화중 온도과승을 줄이기 위한 방법으로 냉각 및 재가열 구간을 도입하여 경화 사이클을 개선하였다. 냉각-재가열 구간이 없는 기존의 경화 사이클과 개선된 경화 사이클로 두꺼운 복합재료를 각각 제조하여 short beam shear 시험 및 Barcol 경도시험을 실시하고, 그 결과를 비교하였다.

• Journal of Microbiology and Biotechnology
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• 제22권4호
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• pp.547-554
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• 2012

Chromium is generated from several industrial processes. It occurs in different oxidation states, but Cr(III) and Cr(VI) are the most common ones. Cr(VI) is a toxic, soluble environmental contaminant. Some bacteria are able to reduce hexavalent chromium to the insoluble and less toxic Cr(III), and thus chromate bioremediation is of considerable interest. An indigenous chromium-reducing bacterial strain, Rb-2, isolated from a tannery water sample, was identified as Ochrobactrum intermedium, on the basis of 16S rRNA gene sequencing. The influence of factors like temperature of incubation, initial concentration of Cr, mobility of bacteria, and different carbon sources were studied to test the ability of the bacterium to reduce Cr(VI) under variable environmental conditions. The ability of the bacterial strain to reduce hexavalent chromium in artificial and industrial sewage water was evaluated. It was observed that the mechanism of resistance to metal was not due to the change in the permeability barrier of the cell membrane, and the enzyme activity was found to be inductive. Intracellular reduction of Cr(VI) was proven by reductase assay using cell-free extract. Scanning electron microscopy revealed chromium precipitates on bacterial cell surfaces, and transmission electron microscopy showed the outer as well as inner distribution of Cr(VI). This bacterial strain can be useful for Cr(VI) detoxification under a wide range of environmental conditions.

• 한국염색가공학회지
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• 제28권3호
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• pp.164-174
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• 2016

In this study, dye-encapsulated microcapsules were produced by emulsion polymerization using styrene monomer. The study showed that the average size of microcapsules were $2{\sim}5{\mu}m$ in normal distribution. These microcapsules induced pale yellow(A12) and reddish yellow(B24) color by thermochromic fluoran yellow(dye A) and red(dye B). These microcapsules were changed to dark yellow(A12) and scarlet(B24) color depending on temperature change. The weight of microcapsules decreased by 7% to 11% during the heating ranges from $320^{\circ}C$ to $350^{\circ}C$ implying that the styrene microcapsules had thermal stability upto $300^{\circ}C$.

• 대한전기학회논문지:시스템및제어부문D
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• 제50권10호
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• pp.494-501
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• 2001

In this study, the effects of vascular parameter changes and electrodes on VOP measurement based on IPG were simulated mathematically. For the evaluation of the effects of hemodynamic changes on VOP, a mathematical model, which consists of cardiovascular system model and venous occlusion model, was developed and the model solution representing the blood flow and pressure in measuring point was found by 2nd order Runge-Kutta method. And, with sensitivity coefficients obtained from finite element solution of electric field in measuring point, the effects of electrode system on measurement were evaluated. As increasing the resistance, the venous capacitance was not changed but the venous outflows were decreased and the decreased compliance reduced the venous capacitance. And, for several configurations of round electrodes and band electrodes, the sensitivity coefficients were computed using the electric field distribution along deep vein. In conclusion, the proposed mathematical cardiovascular model could be applied to the simulation study on the effects of hemodynamic parameters on DVT diagnosis with IPG. And, also the sensitivity coefficients could provide effective electrode configuration for exact measurement of VOP.

• 한국전기전자재료학회논문지
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• 제26권7호
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• pp.563-566
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• 2013

We investigated the variation of anion exchange membrane of hydrogen generator of alkaline electrolysis. We detected the variation of elements and change of anion exchange membrane using EDS and FE-SEM. We detected two different sites of membrane because of different structure of membrane. $Sp_1$ shows that the distribution ratio of C, O, Al is 98% very higher than $Sp_2$ of 78%. Especially, the main elements of STS316 which is P, S, Fe, Ni were more detected at $Sp_2$ than $Sp_1$. We think that this result depends on the structure of membrane. This also affect the resistance, lifetime of membrane and decrease the efficiency of hydrogen production. We hope that this article is a foundation of developing of hydrogen production technology.