• 한국세라믹학회지
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• 제34권10호
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• pp.1037-1044
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• 1997

Mechanical properties and water stability of HAC/PVA based MDF cement composite were investigated using polyurethane(PU) resin, silane coupling agent and various PVA. The results were as follows ; The flexural strength of MDF cement composite increased as increasing with PVA content. Low-viscosity PVA developed higher flexural strength than high-viscosity PVA under a drying curing condition. But the strength of water immersed specimen decreased. Water stability of MDF cement improved as increasing with content of PU. Consequently, water stability of polyurethane 7% added MDF cement was about 2 times higher than that of the controlled specimen. Furthermore, the strength and water stability of diamine group based silane couling agent in using MDF cement increased and improved dramatically.

• Advanced Composite Materials
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• 제16권2호
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• pp.181-194
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• 2007

This paper presents the mechanical properties of a composite consisting of acrylonitrile-butadiene-styrene (ABS) resin mixed with carbon fiber reinforced plastics (CFRP) pieces (CFRP/ABS). CFRP pieces made by crushing CFRP wastes were utilized in this material. Nine kinds of CFRP/ABS compounds with different weight fraction and size of CFRP pieces were prepared. Firstly, tensile and flexural tests were performed for the specimens with various CFRP content. Next, fracture surfaces of the specimens were microscopically observed to investigate fracture behavior and fiber/resin interface. Finally, the tensile modulus and strength were discussed based on the macromechanical model. It is found that the elastic modulus increases linearly with increasing CFRP content while the strength changes nonlinearly. Microscopic observation revealed that most carbon fibers are separated individually and dispersed homogeneously in ABS resin. Epoxy resin particles originally from CFRP are dispersed in ABS resin and seem to be in good contact with surrounding resin. The modulus and strength can be expressed using a macromechanical model taking account of fiber orientation, length and interfacial bonding in short fiber composites.

• 한국치위생학회지
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• 제19권2호
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• pp.307-315
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• 2019

Objectives: The aim of this study was to investigate the characterization of composite resin inlay surface with silane and non-thermal atmospheric pressure plasma treatment. Methods: Composite resin inlay was used as a specimen, which was treated by sandblasting + silane and sandblasting + plasma. The untreated specimens were assigned to the control group. Specimens were analyzed for surface roughness, color change, and chemical composition. Statistical analyses were performed using one-way ANOVA test (p<0.05). Results: The present findings showed that the roughness and color changes of the plasma-treated surface were significantly lower than those of the silane-treated surface. In addition, a change in the chemical composition was observed on the plasma-treated surface. Conclusions: Based on the results, non-thermal atmospheric pressure plasma could be a potential tool for the cementation of composite resin inlay.

• 대한치과의료관리학회지
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• 제11권1호
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• pp.38-46
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• 2023

Composite resins, commonly used in clinical practice, have been developed to improve aesthetics to obtain smooth surfaces. Although the restored composite resin has a smooth surface, it gradually becomes rough over time. Therefore, this study measured glossiness to evaluate the surface of various composite resins and attempted to evaluate the maintenance of glossiness of composite resins by observing surfaces that change to roughness. Specimens were produced using resin used in clinical practice: Gradia direct anterior (GA), Tetric N-Ceram (TN), Ceram.X Sphere TEC one (CX), Filtek Z350XT (FT), Estelite sigma quick (ES). After creating a smooth surface with slide glass, five locations were randomly selected to measure surface gloss, and the average was the representative value of the specimen. Roughness was applied to the specimen under water pouring at the same speed and pressure using SiC paper #2400, 1200, and 400. The gloss unit of different SiC papers was measured. To evaluate the gloss unit and gloss retention between composite resins, one-way analysis of variance and Tukey multiple comparisons test were used. As a result of the study, there was a difference in gloss unit of specimens produced under the same conditions. Although the degree differed depending on the composite resin, there was also a difference in gloss retention. Based on the findings, composite resins show differences in gloss due to their different characteristics. Ceram.X Sphere TEC one (CX) showing the lowest gloss retention and Estelite sigma quick (ES) showing the highest.

• 한국세라믹학회지
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• 제37권3호
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• pp.280-287
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• 2000

Adsorption behavior and amount of phenolic resin followed silica (SiO2) formation onto silicon nitride(Si3N4) surface were investigated using electrokinetic sonic amplitude (ESA) technique and with UV spectrometer, to fabricate Si3N4/SiC nano-composite based on reaction between SiO2 formed and phenolic resin absorbed onto Si3N4 particle. The amount of SiO2 formed and carbon from phenolic resin absorbed onto Si3N4 surface were calculated quantitatively to adjust the reaction between SiO2 and phenolic resin, resulting in no residual SiO2 and carbon. As a result, pre-heated tempeature for optimized reaction was below 25$0^{\circ}C$, in which there was no residual SiO2 and carbon.

• Composites Research
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• 제30권6호
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• pp.393-398
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• 2017

손상된 치아의 복구에 사용되는 재료인 치과용 복합레진 Clearfil AP-X (Kuraray, Japan)을 대상으로 디지털 이미지 상관법을 이용하여 광중합 시 발생하는 수축분포를 관찰하였다. 디지털 이미지 상관분석법을 위해, CCD 카메라를 이용하여 광조사 중과 광조사 이후의 촬영 조건을 달리하여 사진을 획득하였다. 광조사중의 최적의 촬영 조건을 설정하기 위하여 노출시간을 0.15 ms부터 0.55 ms까지 0.05 ms 간격으로 촬영한 사전 실험을 통해 촬영 조건을 획득하였다. DIC 분석 결과 복합레진의 비균일한 수축 분포를 관찰하였으며 복합레진의 중심 부분에서 시편의 계면부보다 좀 더 자유로운 유동성으로 더 큰 수축이 발생하였다. 복합레진의 중합수축은 초기 20 s 의 광조사에서 최종경화수축률의 50~60% 수준까지 발생하였다. 이러한 치과용 복합레진의 큰 수축량은 레진/기질계면 근처에서 인장응력이 집중하도록 영향을 주었다.

• 대한소아치과학회지
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• 제37권4호
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• pp.438-444
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• 2010

자이오머는 불소를 유리하는 최근 개발된 광중합 레진 제재이다. 본 실험에서는 복합레진, 자이오머, 컴포머를 이용하여 $5^{\circ}C$와 $55^{\circ}C$에서 5000번 열순환 후 압축강도와 미세경도 변화를 비교 평가하였다. 1. 열순환 전.후 모두 압축강도는 복합레진이 가장 높았으며, 자이오머, 컴포머 순으로 낮아졌다. 복합레진은 자이오머, 컴포머와 통계학적으로 유의차를 보였고(p<0.05), 자이오머와 컴포머 사이에는 유의차가 없었다. 2. 열순환 전.후 미세경도는 복합 레진, 자이오머, 컴포머 순으로 낮아졌으며, 각각 통계학적으로 유의차를 보였다(p<0.05). 3. 복합레진, 자이오머, 컴포머는 열순환 후 통계학적으로 유의하게 미세경도가 감소하였다(p<0.05). 이상의 결과를 종합해보면, 자이오머는 컴포머보다 높은 미세경도를 보이지만, 복합레진보다 낮은 압축강도와 미세경도를 보인다. 열순환 후 미세경도가 감소하므로 임상적 사용시 물리적 성질에 대한 충분한 고찰이 필요할 것으로 사료된다.

• 대한소아치과학회지
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• 제50권4호
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• pp.443-451
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• 2023

The purpose of this study was to evaluate whether the newly introduced calcium silicate-based materials with fast-setting properties could be appropriately used as basement materials in indirect pulp treatment (IPT). This was performed by quantifying the durability of adhesion between the material and composite resin, measured by the shear bond strength (SBS). Five calcium silicate-based materials, TheraCal LC^® (TLC), TheraCal PT^® (TPT), TheraBase^® (TB), Well-Root^TM PT (WPT), and Endocem^® MTA (EMTA), as well as two glass ionomer-based materials, Fuji II and Fuji II LC, were included. Specimens containing these materials were manufactured and bonded to composite resin with a universal adhesive applied in self-etch mode. The SBS values and failure modes were recorded, and the mean SBSs of the materials were compared. Both TPT and TB exhibited SBS values that were similar to TLC, while both WPT and EMTA appeared to have statistically lower SBS values. Mixed failure was commonly observed in TLC and TPT, while all WPT and EMTA samples showed cohesive failure. In comparison with TLC and TPT, more samples with cohesive failure were observed in TB, implying that this material forms a stronger bond with composite resin. Together with the ability of TB to chemically bind to dentin due to its 10-methacryloyloxydecyl dihydrogen phosphate component, TB seems to be a promising material for IPT within the limitations of this in vitro study.

• Restorative Dentistry and Endodontics
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• 제42권3호
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• pp.157-167
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• 2017

This systematic review aims to summarize the current clinical studies that investigated survival rates against fracture of endodontically treated posterior teeth restored with crowns or resin composite restorations. Literature search were performed using keywords. Publications from 1980 to 2016 were searched in PubMed, ScienceDirect, ISI Web of SCIENCE, MEDLINE, and SCOPUS. Included studies were selected based on inclusion and exclusion criteria. Three clinical studies were included: 1 randomized controlled trial and 1 prospective and 1 retrospective cohort studies. Pooled survival rates ranged from 94%-100% and 91.9%-100% for crowns and resin composite, respectively. The majority of teeth had no more than 3 surface loss of tooth structure. The studies included were heterogeneous, and were not appropriate for further meta-analysis. Current evidence suggested that the survival rates against the fracture of endodontically treated posterior teeth restored with crowns or resin composites were not significantly different in the teeth with minimum to moderate loss of tooth structure.

• Composites Research
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• 제31권4호
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• pp.161-170
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• 2018

원통형 복합재 격자 구조체는 필라멘트 와인딩 기법으로 제작되며 제작 공정에서 발생할 수 있는 섬유체적비 불균일과 수지응집층은 구조체의 강성도 및 강도에 영향을 줄 수 있다. 구조체의 주요 요소인 후프 및 헬리컬 리브의 단면 분석을 통해 섬유체적비 불균일 및 수지응집층의 존재 여부를 확인하였으며, 단면 분석 결과를 바탕으로 후프 및 헬리컬 리브에 대한 실험 및 이론적 접근을 통해 섬유체적비 불균일 및 수지응집층이 리브 요소의 강성도에 미치는 영향을 분석하였다. 섬유체적비 불균일이 후프 리브의 굽힘 거동에 영향을 미치는 것을 확인하였으며 헬리컬 리브의 경우 섬유체적비 불균일 및 수지응집층에 의해 강성도에 변화가 있음을 확인하였다.