• Title/Summary/Keyword: Resin series

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The Recovery of Carbon Fiber from Carbon Fiber Reinforced Epoxy Composites Applied to Railway Vehicles (철도차량용 폐 복합소재로부터 탄소섬유 회수)

  • Lee, Suk-Ho;Kim, Jung-Seok;Lee, Cheul-Kyu;Kim, Yong-Ki;Ju, Chang-Sik
    • Journal of the Korean Society for Railway
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    • v.12 no.6
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    • pp.1059-1066
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    • 2009
  • Recently, the amount of thermosetting plastic wastes has increased with the production of reinforced plastic composites and causes serious environmental problems. The epoxy resins, one of the versatile thermosetting plastics with excellent properties, cannot be melted down and remolded as what is done in the thermoplastic industry. In this research, a series of experiments that decompose epoxy resin and recover carbon fibers from carbon fiber reinforced epoxy composites applied to railway vehicles was performed. We experimentally examined various decomposition processes and compared their decomposition efficiencies and mechanical property of recovered carbon fibers. For the prevention of tangle of recovered carbon fibers, each composites specimen was fixed with a Teflon supporter and no mechanical mixing was applied. Decomposition products were analyzed by scanning electron microscope (SEM), gas chromatography mass spectrometer (GC-MS), and universal testing machine (UTM). Carbon fibers could be completely recovered from decomposition process using nitric acid aqueous solution, liquid-phase thermal cracking and pyrolysis. The tensile strength losses of the recovered carbon fibers were less than 4%.

Performance of a 5 L Liquid Hydrogen Storage Vessel (5 L급 액체수소 저장용기의 성능특성 연구)

  • KARNG, SARNG WOO;GARCEAU, NATHANIEL;LIM, CHANG MU;BAIK, JONG HOON;KIM, SEO YOUNG;OH, IN-HWAN
    • Transactions of the Korean hydrogen and new energy society
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    • v.26 no.3
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    • pp.234-240
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    • 2015
  • In the face of the world's growing energy storage needs, liquid hydrogen offers a high energy density solution for the storage and transport of energy throughout society. A 5 L liquid hydrogen storage tank has been designed, fabricated and tested to investigate boil-off rate of liquid hydrogen. As the insulation plays a key role on the cryogenic vessels, various insulation methods have been employed. To reduce heat conduction loss, the epoxy resin-based insulation supports G-10 were used. To minimize radiation heat loss, vapor cooled radiation shield, multi-layer insulation, and high vacuum were adopted. Mass flow meter was used to measure boil-off rate of the 5 L cryogenic vessel. A series of performance tests were done for liquid nitrogen and liquid hydrogen to compare with design parameters, resulting in the boil-off rate of 1.7%/day for liquid nitrogen and 16.8%/day for liquid hydrogen at maximum.

Fine structure of Laminaria religiosa Miyabe (Laminariales, Phaeophyta) 1 . Composition of Fixatives. (애기다시마 식물의 미세구조 연구 1. 고정액 조성)

  • CHUNG Ik-Kyo
    • Korean Journal of Fisheries and Aquatic Sciences
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    • v.23 no.2
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    • pp.155-166
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    • 1990
  • There have been many problems like plasmolysis in the ultrastructural studies with kelps. The present study was conducted with series of different fixatives and buffer solutions and several resins to solve the plasmolysis phenomena. The fixative of 1470 mosmol($3\%$ glutaraldehyde, $2.4\%$ paraformaldehyde in 0.05M cacodylate buffer with 0.2M sucrose and $0.5\%$ caffeine at pH of 7.2) showed the least frequency of plasmolysis. The relationship between the concentration of primary fixatives and the frequency of plasmolysis was not found. With above fixative the possibility of plasmolysis during infiltration period was not identified using ultra-low viscosity resin. Generally, the kelp(Laminaria religiosa) contains a lot of mucilage, which interupts the infiltration of fixative. The possible physiological mechanisms related with mucilage secretion may be unable to fix the region of plasmalemma properly.

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A Study on Low Velocity Impact and Residual Compressive Strength for Carbon/Epoxy Composite Laminate (탄소섬유/에폭시 복합적층판의 저속 충격 및 잔류 압축강도에 관한 연구)

  • Lee, S.Y.;Park, B.J.;Kim, J.H.;Lee, Y.S.;Jeon, J.C.
    • Proceedings of the KSME Conference
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    • 2000.11a
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    • pp.250-255
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    • 2000
  • Damage induced by low velocity impact loading in aircraft composite laminates is the form of failure which is occurred frequently in aircraft. Low velocity impact can be caused either by maintenance accidents with tool drops or by in-flight impacts with debris. As the consequences of impact loading in composite laminates, matrix cracking, delamination and eventually fiber breakage for higher impact energies can be occurred. Even when no visible impact damage is observed, damage can exist inside of composite laminates and the carrying load of the composite laminates is considerably reduced. The reduction of strength and stiffness by impact loading occurs in compressive loading due to laminate buckling in the delaminated areas. The objective of this study is to determine inside damage of composite laminates by impact loading and to determine residual compressive strength and the damage growth mechanisms of impacted composite laminates. For this purpose a series of impact and compression after impact tests are carried out on composite laminates made of carbon fiber reinforced epoxy resin matrix with lay up pattern of $[({\pm}45)(0/90)_2]s$ and $[({\pm}45)(0)_3(90)(0)_3({\pm}45)]$. UT-C scan is used to determine impact damage characteristics and CAI(Compression After Impact) tests are carried out to evaluate quantitatively reduction of compressive strength by impact loading.

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Quantitative Evaluation of Geotextile Void Structures Using Digital Image Analysis (디지털 이미지 분석을 이용한 지오텍스타일 공극 분포의 정량화)

  • Kim, Duhwan
    • Journal of the Korean Geosynthetics Society
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    • v.12 no.1
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    • pp.51-61
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    • 2013
  • This paper presents results from a study undertaken to quantitatively evaluate the geotextile pore sizes using optical image analysis. The evaluation was conducted by observing surfaces of coupons cut from resin-impregnated specimens of geotextile-geomembrane layered under various load conditions. Stereological concepts were applied to collect representative specimens from a series of laboratory tests. The sizes of voids enclosed by filaments were expressed in terms of the largest inscribing opening size (LIOS) distribution. The opening diameter corresponding to the 50% cumulative frequency decreased by about 45mm as the load increased from 10 to 300kPa and recovered to about 90% of its initial state on unloading back to 10kPa. The average void size was reduced by 32 and 16.5% as the geotextile was sheared against a textured geomembrane under normal stresses of 100 and 300kPa, respectively. The results showed how the LIOS distribution varied as a function of normal stress and interface shear displacement against a smooth and a textured geomembrane surfaces.

Micromechanics-based Analysis on Tensile Behavior of the Sprayed FRP Composites with Chopped Glass Fibers (유리단섬유로 보강된 분사식 섬유보강 복합재료의 인장거동에 관한 미세역학 기반 해석)

  • Yang, Beom-Joo;Ha, Seong-Kook;Lee, Haeng-Ki
    • Journal of the Computational Structural Engineering Institute of Korea
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    • v.25 no.3
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    • pp.211-217
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    • 2012
  • In this paper, experimental tests and theoretical studies were carried out to evaluate the tensile behavior of the sprayed FRP composite with chopped glass fiber. For this, a series of tensile strength tests with various strain rates were conducted on the specimens of the matrix and sprayed FRP composite. Sprayed FRP composite contained chopped glass fibers with fiber length of 15mm and a specific volume fraction of fibers of 25 %. An inverse simulation was conducted to simulate the strain rate sensitivity based on the present experimental data of the epoxy resin. The simulated viscosity value is adapted to the micromechanics-based viscoelastic damage model(Yang et al., 2012), and the overall tensile behavior of sprayed FRP composites is predicted. It was seen from the comparative study between present experimental data and predication results that the proposed methodology can be used to predict the viscoelastic behavior of the sprayed FRP composite.

Comparison of shaping ability using LightSpeed, ProTaper and Hybrid technique in simulated root canals (모조 레진블락 근관에서 LightSpeed, ProTaper 및 Hybrid technique의 성형 효율 비교)

  • Kang, Soon-Il;Kwak, Sang-Won;Park, Jeong-Kil;Hur, Bock;Kim, Hyeon-Cheol
    • The Journal of the Korean dental association
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    • v.47 no.7
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    • pp.444-454
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    • 2009
  • The purpose of this study was to compare the shaping abilities of LightSpeed, ProTaper-Universal, and hybrid technique using S-series of ProTaper-Universal and LigthSpeed. The 72 simulated root canals of J-shape were used and classified as flowing 3 groups according to the instrumentation methods; Group P of 24 canal blocks were prepared with ProTaper-Universal, Group L was prepared with LightSpeed, and Group H was prepared with hybrid technique (initial shaping with ProTaper-Universal SI and S2 and apical shaping with LightSpeed from #25 to #50). A second-year resident of Endodontic department prepared the resin block canals to apical size #50 (F5 in Group P). The time lapses for instrumentation and the reduction of root canal curvature after shaping were measured. The pre- and post-instrumented root canals were scanned and superimposed to evaluate and calculate the increased canal width and apical centering ratio. The results were as followings: Group Land H showed significant less instrumentation time than Group P (p < 0.05). The ProTaper system showed greater reduction of root canal curvature and working length diminishment than other methods (p < 0.05). LightSpeed system showed best canal curvature preserving characteristics. The Group P had greater instrumented widths at all levels examined (p < 0.05). Group L and Group H showed lower centering ratio (ability to preserve the canal center; the lower ratio means the better canal center preservation) than Group P (p < 0.05). Group H had the lowest centering ratio at the 1 mm level.

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Experimental study on propagation behavior of three-dimensional cracks influenced by intermediate principal stress

  • Sun, Xi Z.;Shen, B.;Zhang, Bao L.
    • Geomechanics and Engineering
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    • v.14 no.2
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    • pp.195-202
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    • 2018
  • Many laboratory experiments on crack propagation under uniaxial loading and biaxial loading have been conducted in the past using transparent materials such as resin, polymethyl methacrylate (PMMA), etc. However, propagation behaviors of three-dimensional (3D) cracks in rock or rock-like materials under tri-axial loading are often considerably different. In this study, a series of true tri-axial loading tests on the rock-like material with two semi-ellipse pre-existing cracks were performed in laboratory to investigate the acoustic emission (AE) characteristics and propagation characteristics of 3D crack groups influenced by intermediate principal stress. Compared with previous experiments under uniaxial loading and biaxial loading, the tests under true tri-axial loading showed that shear cracks, anti-wing cracks and secondary cracks were the main failure mechanisms, and the initiation and propagation of tensile cracks were limited. Shear cracks propagated in the direction parallel to pre-existing crack plane. With the increase of intermediate principal stress, the critical stress of crack initiation increased gradually, and secondary shear cracks may no longer coalesce in the rock bridge. Crack aperture decreased with the increase of intermediate principal stress, and the failure is dominated by shear fracturing. There are two stages of fracture development: stable propagation stage and unstable failure stage. The AE events occurred in a zone parallel to pre-existing crack plane, and the AE zone increased gradually with the increase of intermediate principal stress, eventually forming obvious shear rupture planes. This shows that shear cracks initiated and propagated in the pre-existing crack direction, forming a shear rupture plane inside the specimens. The paths of fracturing inside the specimens were observed using the Computerized Tomography (CT) scanning and reconstruction.

Study on Effect of the printing direction and layer thickness for micro-fluidic chip fabrication via SLA 3D printing (적층 방식 3차원 프린팅에 의한 미세유로 칩 제작 공정에서 프린팅 방향 및 적층 두께의 영향에 관한 연구)

  • Jin, Jae-Ho;Kwon, Da-in;Oh, Jae-Hwan;Kang, Do-Hyun;Kim, Kwanoh;Yoon, Jae-Sung;Yoo, Yeong-Eun
    • Design & Manufacturing
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    • v.16 no.3
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    • pp.58-65
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    • 2022
  • Micro-fluidic chip has been fabricated by lithography process on silicon or glass wafer, casting using PDMS, injection molding of thermoplastics or 3D printing, etc. Among these processes, 3D printing can fabricate micro-fluidic chip directly from the design without master or template for fluidic channel fabricated previously. Due to this direct printing, 3D printing provides very fast and economical method for prototyping micro-fluidic chip comparing to conventional fabrication process such as lithography, PDMS casting or injection molding. Although 3D printing is now used more extensively due to this fast and cheap process done automatically by single printing machine, there are some issues on accuracy or surface characteristics, etc. The accuracy of the shape and size of the micro-channel is limited by the resolution of the printing and printing direction or layering direction in case of SLM type of 3D printing using UV curable resin. In this study, the printing direction and thickness of each printing layer are investigated to see the effect on the size, shape and surface of the micro-channel. A set of micro-channels with different size was designed and arrayed orthogonal. Micro-fluidic chips are 3D printed in different directions to the micro-channel, orthogonal, parallel, or skewed. The shape of the cross-section of the micro-channel and the surface of the micro-channel are photographed using optical microscopy. From a series of experiments, an optimal printing direction and process conditions are investigated for 3D printing of micro-fluidic chip.

The Study and Conservation of Woven Cigarette Inserts (담배 사은품 실크 인서트(Silk Inserts)에 관한 연구와 보존처리)

  • Lee, Young-Joo
    • Journal of the Korean Society of Clothing and Textiles
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    • v.30 no.3 s.151
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    • pp.447-457
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    • 2006
  • The purpose of this study is to document and preserve an unidentified textile purchased at a flea market. This study object is important because it is one of the very rare silk insert series from 1930s which were created for commercial use(as inclusion in cigarette packages). The investigation was conducted by researching the limited publications that discuss silk inserts, visiting many sites on the internet that offer such inserts for sale or catering to the collectors of these silk inserts, and especially visiting the collection of silk inserts, named the J.R. Burdick Collection, at the Metropolitan Museum of Art, New York. Several pieces matched the patches used in the study piece. But Buidick's description on time frame(1912-1915) did not indicate the full range of production of silk inserts. After the identification of object, the conservation treatment was carefully done using adhesives. The results of this study can be summarized as follows; 1. The silk inserts of the study object were included as promotions by some company owned by the American Tobacco Company, probably at some time between 1934 and 1939. 2. The initial stage in the conservation treatment was mechanical surface cleaning using a vacuum cleaner. After vacuuming, humidification was conducted to reduce creases in the top of the object. The damaged areas were backed with stabiltax coated with a solution of Elvace 45675 since the fiber of this object was too deteriorated. 3. Adhesive treatments using Elvace showed satisfactory results: flexibility, strength, no damaging effects on the study object, removability without damaging the object.