• Title/Summary/Keyword: Residue test

검색결과 279건 처리시간 0.03초

사과쥬스박과 두유박으로부터 제조한 식이섬유원을 보강한 면류 제조 (Preparation of noodle supplemented with treated apple pomace and soymilk residue as a source of dietary fiber)

  • 홍재식;김명곤;윤숙;유남수;김용규
    • Applied Biological Chemistry
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    • 제36권2호
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    • pp.80-85
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    • 1993
  • 가공적성을 떨어뜨리지 않으면서 우수한 기능특성을 보이는 식이섬유원은 제조할 목적으로 대량 수급이 용이한 사과쥬스박과 두유박에 작종 이화학적 처리하여 식이성유의 함량과 기능성을 향상시킨 식이섬유원을 이용하여 이들을 직접 식품에 응용하여 그 이용 가능성을 모색하였다. 식이섬유질원을 밀가루와 혼합한 복합분의 호화양상을 Amylograph로 측정한 결과 식이섬유질원의 첨가량이 증가될수록 점도가 감소하였다. 식이섬유질원을 첨가하여 면을 제조하여본 결과 식이섬유질원의 첨가량이 증가할수록 조리면의 중량과 부피는 증가하였으나 인장강도는 감소하였는데 처리 사과육이 처리 두유박보다 인장강도의 감소가 심하였다. 관능검사에서는 처리 두유박 5% 첨가시 밀가루면보다 우수한 관능성을 보였으며 처리 두유박 10%와 처리 사과육 5% 첨가시 향기, 색도, 조직감 및 전체적인 맛에서 밀가루면과 유의차를 보이지 않았다.

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Effect of fermented biogas residue on growth performance, serum biochemical parameters, and meat quality in pigs

  • Xu, Xiang;Li, Lv-mu;Li, Bin;Guo, Wen-jie;Ding, Xiao-ling;Xu, Fa-zhi
    • Asian-Australasian Journal of Animal Sciences
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    • 제30권10호
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    • pp.1464-1470
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    • 2017
  • Objective: This study investigated the effect of fermented biogas residue (FBR) of wheat on the performance, serum biochemical parameters, and meat quality in pigs. Methods: We selected 128 pigs (the mean initial body weight was $40.24{\pm}3.08kg$) and randomly allocated them to 4 groups (1 control group and 3 treatment groups) with 4 replicates per group and 8 pigs per pen in a randomized complete block design based on initial body weight and sex. The control group received a corn-soybean meal-based diet, the treatment group fed diets containing 5%, 10%, and 15% FBR, respectively (abbreviated as FBR5, FBR10, and FBR15, respectively). Every group received equivalent-energy and nitrogen diets. The test lasted 60 days and was divided into early and late stages. Blood and carcass samples were obtained on 60 d. Meat quality was collected from two pigs per pen. Results: During the late stage, the average daily feed intake and average daily gain of the treatment groups was greater than that of the control group (p<0.05). During the entire experiment, the average daily gain of the treatment groups was higher than that of the control group (p<0.05). Fermented biomass residue did not significantly affect serum biochemical parameters or meat quality, but did affect amino acid profiles in pork. The contents of Asp, Arg, Tyr, Phe, Leu, Thr, Ser, Lys, Pro, Ala, essential amino acids, non-essential amino acids, and total amino acids in pork of FBR5 and FBR10 were greater than those of the control group (p<0.05). Conclusion: These combined results suggest that feeding FBR could increase the average daily gain and average daily feed intake in pigs and the content of several flavor-promoting amino acids.

액체크로마토그래피를 이용한 벌꿀 중 테트라싸이클린계 항생물질의 정량분석 및 잔류조사 (Determination and survey of tetracyclines residue in honey by high performance liquid chromatography)

  • 이성모;박은정;홍지영;김정임;이정구;황현순;김용희
    • 한국동물위생학회지
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    • 제28권3호
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    • pp.203-213
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    • 2005
  • Oxytetracycline, tetracycline, chlortetracycline and doxycycline in honey were separated by solid phase extraction (SPE) and determined with high performance liquid chromatography (HPLC) with UV/Visible detector. Analysis was carried out using following conditions: XTerra $C_8$ column $(3.9\times150mm\;i.d. 5{\mu}m)$, mobile phase composed of 0.01M oxalic acid : methanol : acetonitrile (820 : 80 : 100, v/v/v), isocratic pump at a flow rate of 0.9 ml/min. and $50{\mu}l$ of injection volume, UV/Visible detector with wavelength of 360nm. The calibration curves of four tetracyclines showed linearity $(\gamma^2>0.999)$ at concentration range of $100\~1,000 ng/ml$. The recoveries in fortified honey represented more than $70\%$ with low coefficient of variation $(<10\%)$ for concentration range of four tetracyclines. The detection limits for oxytetracycline, tetracycline, chlortetracycline and doxycycline were 13.8, 14.6, 26.2 and 24.9ng/g in acacia honey. respectively. We also monitored tetracyclines residue in domestic honey [n : 38, acacia (20), wild flower (18) ] and foreign honey [n=22, legally distributed (13), illegally distributed (9)] using modified Charm II screening and HPLC confirmation methods. Seven of the 60 samples $(11.7\%)$ were suspect positive using modified Charm II screening test. Chlortetracycline residue was found in one foreign honey (illegally distributed) tested at concentrations of 0.22 ppm. Conclusively, for more effective control of tetracyclines used in beekeeping should be further survey for residues in honey and also national guidelines (maximum residue limit : MRL) and methods should be obligatory.

수출용 단감에 대한 Difenoconazole과 Thiamethoxam의 잔류특성 연구 (Residue Studies of Difenoconazole and Thiamethoxam during Cultivation of Sweet Persimmon for Export)

  • 장희라;강혜림;도정아;오재호;황인균;권기성;임무혁;김균
    • 한국환경농학회지
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    • 제31권3호
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    • pp.248-254
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    • 2012
  • 국내 유망 수출 식품 중 잔류농약으로 인하여 수출 장애가 있는 식품을 대상으로 문제가 되는 농약에 대해 CAC 및 수출국의 농약잔류 허용기준 제안을 위한 작물잔류 시험을 수행하였다. 대상 작물은 수출용 단감이었고, difenoconazole과 thiamethoxam을 대상으로 시험을 수행하였다. Difenoconazole의 잔류량 범위는 0.2~0.56 mg/kg였고, thiamethoxam의 잔류량 범위는 0.08~0.28 mg/kg으로 두 약제 모두 수확 1일차 시료부터 MRL 농도 이하로 잔류량이 감소하였다. 따라서 안전사용기준에 따라 약제를 살포하고 수확한다면 국내에 설정된 MRL 기준을 충분히 만족시키는 것으로 확인되었다. Difenoconazole의 각 포장별 반감기는 각각 13.6, 19.4, 16.3일 이었고, thiamethoxam의 각 포장별 반감기는 각각 10.0, 15.3, 14.0일 이었다. Clothianidin의 잔류농도는 1개 지역에서 14, 28일 시료에서 검출되었으나, 농도는 0.03 mg/kg 이하였다.

인삼박(人蔘粕) 및 인삼엽(人蔘葉)으로 제조(製造)한 Mosquito Coil Powder가 Rat 및 Mouse에 미치는 독성(毒性)에 관한 연구(硏究) (Toxicity Test of Mosquito Coil Powder Made of Ginseng Leaf and Ginseng Residue after Extraction with Ethanol- Water System)

  • 허재두;심순주;김용주;오정균;김재백
    • Journal of Pharmaceutical Investigation
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    • 제9권3호
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    • pp.22-26
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    • 1979
  • This report was carried out toxicity test for the mosquito coil made of Ginseng leaf and the residue after extraction of Ginseng root. This results are as follows: In the first group, was not shown any special difference on the body weight, the motion and dissection. In the second group, was not shown any Special difference on the body weight, considerable difference on the motion and considerable loss of appetite besides very slight loss, but came cack soon again to normal state by change of air after a moment. In the third group, the body weight and appetite was depressed very slightly and the motion was shown very slightly difference, but came back soon again to normal state by chenge of air after a moment too. No one was died, and all the animal were the normal state on the reslt of dessection, Therefore, we have positive evidence that this mosquito coil powder is applied to animals without any toxicity.

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골프장 농약 검사를 위한 다성분동시시험방법 확립에 관한 연구

  • 이민효;노회정;박종겸;윤정기;김찬섭
    • 한국지하수토양환경학회:학술대회논문집
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    • 한국지하수토양환경학회 2002년도 추계학술발표회
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    • pp.81-85
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    • 2002
  • The possibility of simultaneous analysis of 24 pesticides out of 30 residual pesticides which are subjected to test in the golf courses was examined. The utility of the simultaneous analysis of multi-residue pesticides was evaluated by recovery test through a standard addition method of pesticides in water, soil, and lawn grass. The experimental results of the recovery rates for individual pesticides are as follows : The number of pesticide of which average recovery was over 70% regardless of medium was 16 pesticides. These pesticides were composed of 8 organophosphorus pesticides(Chlorpyrifos, Chlorpyrifos-methyl, Diazinon, EPN, Fenitrothion, Phenthoate, Phosalone, and Toclofos-methyl). 4 organochlorinated pesticides(Daconil, Captan, Endosulfan, and Tetradifon), 2 pyrethroid pesticides(Fepropathrin, Lambda-cyhalothrin) and 2 other pesticides(Bromopropylate, Pendimethalin). On the other hand, in case of Dicofol, average recovery by medium was over 70% for water and lawn grass but was only 53.3% for soil. Therefore, the simultaneous analytical method applied in this experiment is not appropriate for analysis of Dicofol in soil. Furthermore, among 7 pesticides, 2 pesticides(Amitraz and Pyraclofos) showed that theirs average recovery rates deviated from criteria(70~130%) at almost all media, while 5 pesticides(Bensulide, Deltamethrin, Iprodione, Phosphamidon and Tralomethlin) were not detected from all media by selected GC detector(NPD or ECD).

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세종지역 유통 식육 중 벤지미다졸계 구충제 잔류실태 조사 (Investigation of benzimidazole residues in the meat in Sejong area)

  • 김태평;김태원;이종훈;김문배
    • 한국동물위생학회지
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    • 제44권3호
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    • pp.125-131
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    • 2021
  • Benzimidazole is an widely used anthelmintics in livestock clinics. The aim of present study was to investigate benzimidazole residues in the meat in Sejong City. A total of 338 samples of meat(beef 287, pork 37, chicken 14) were selected from the laboratory meat(Korean beef genetic test, hygiene test) supplied to school in Sejong City. Representative benzimidazole class drug such as thiabendazole, 2-amino albendazole sulfone, fenbendazole, oxfendazole, and oxfendazole sulfone were monitored in samples by using lc-ms/ms and the analysis was preformed based on the Korea Food Code guideline. Limit of quantitation (LOQ) was ranged from 0.56 to 3.02 ppb for target drugs and the accuracy was within the acceptance criteria. Among the sample analyzed only one case, the pork meat was found to have drug levels that exceed LOQ. However, the overall residue concentration was 2.17 ppb, which was lower than the maximum residue levels (100 ppb).

USING AN ABSTRACTION OF AMINO ACID TYPES TO IMPROVE THE QUALITY OF STATISTICAL POTENTIALS FOR PROTEIN STRUCTURE PREDICTION

  • Lee, Jin-Woo
    • Journal of the Korean Society for Industrial and Applied Mathematics
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    • 제15권3호
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    • pp.191-199
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    • 2011
  • In this paper, we adopt a position specific scoring matrix as an abstraction of amino acid type to derive two new statistical potentials for protein structure prediction, and investigated its effect on the quality of the potentials compared to that derived using residue specific amino acid identity. For stringent test of the potential quality, we carried out folding simulations of 91 residue A chain of protein 2gpi, and found unexpectedly that the abstract amino acid type improved the quality of the one-body type statistical potential, but not for the two-body type statistical potential which describes long range interactions. This observation could be effectively used when one develops more accurate potentials for structure prediction, which are usually involved in merging various one-body and many-body potentials.

A QUADRATIC APPROXIMATION FOR PROTEIN SEQUENCE TO STRUCTURE MAPPING

  • Oh, Se-Young;Yun, Jae-Heon;Chung, Sei-Young
    • Journal of applied mathematics & informatics
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    • 제12권1_2호
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    • pp.155-164
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    • 2003
  • A method is proposed to predict the distances between given residue pairs (between C$\sub$${\alpha}$/ atoms) of a protein using a sequence to structure mapping by indefinite quadratic approximation. The prediction technique requires a data fitting in three dimensional space with coordinates of the residues of known structured proteins and leads to a numerical ref resentation of 20 amino acids by minimizing a large least norm iteratively. These approximations are used in distance prediction for given residue pairs. Some computational experience on a test set of small proteins from Brookhaven Protein Data Bank are given.

W CMP 세정 공정에서 DHF에 적용에 관한 연구 (A Study of DHF application at W CMP Cleaning Process)

  • 김상용;서용진;이우선;김창일;장의구
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2002년도 추계학술대회 논문집 Vol.15
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    • pp.147-150
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    • 2002
  • In this study, we evaluated the dilute HF Cleaning to reduce residual defects made by W CMP process. But, One point we should focus is It should not effect to metal thin film reliability. The purpose of this test is to verify barrier metal damage during HF cleaning and based on this result we get rid of slurry residue defect which is main defect of W CMP process for the better yield.

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