• 대한지역사회영양학회지
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• 제3권3호
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• pp.454-465
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• 1998

This study was to investigate the recognition level of food contamination with residual pesticides and hazardous heavy metals from 365 male and female adults in Taejon area using questionnaires. Among the recognizing level of residual pesticides in overall foods, 69.1% were 'serious', 25.6% were 'average' and 5.3% were 'not serious'. Over 94.7% of the subjects recognized residual pesticides pollution infoods. for hazardous heavy metals in food, 47.8% responsed as 'serious', 40.5% as 'average' and 11.8 as ' not serious' . Over 88.3% of the subjects recognized contaminated pesticides seriously in fruits, 72.1% in vegetables and 51.7% in cereals, whereas 55.7% of the subjects recognized hazardous heavy metal contamination seriously in fruits, 53.4% in vegetables, 40.8% in fishes and shellfishes and 35.0% in seaweeds. The subjects recognized residual pesticides contamination more seriously in overall foods, cereal, potatoes and starches, bean, vegetables and fruits, whereas hazardous heavy metal contamination was recognized more seriously in fishes and shellfishes, and seaweeds food groups. Comparisons were shown based on individuial's occupation. Farmer, forester, iner and fisher showed the lowest recognizing level of food contamination in most food groups. The mean score of the dietary effect by mass media's information on food contamination from residual pesticides and hazardous heavy metals were 3.51±0.96 out of 5 points. By Duncan's multiple range test, sex, age, marriage, food cost per month, concerns about health and nutrition knowledge showed significant differences in the mean effect score at p<0.05. According to a pesticides contamination in several food groups were affected by food cost per month, mass media's information on food contamination, health status, and concerns about health, But a recognition level of hazardous heavy metals in food were affected by income and, food cost per month mass media's information on food contamination, health status, concern about health and nutrition knowledge. People who need to take extreme precautions of food contamination were in order of producers, government officials, homemakers, the consumer's association and consumers.

• 한국포장학회지
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• 제10권1호
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• pp.63-68
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• 2004

The regulations for migration amounts in USA, EU and Korea are investigated to compare the actual overall and specific migration date from plastic food packaging materials. Among the packaging materials regulated in above countries, printing ink solvents on packaging materials is used very widely and sometimes cause off-flavor in the food by migration of residual solvents. Even though migration of the residual solvents dose not generally cause safety problems in the contained food, it certainly can generate off-flavor and finally deteriorate quality of the finished product. Therefore regulation and development of analytical method for amount of residual ink solvents are very important issue in food industry. The headspace analytical method and tenax method for residual ink solvent on food packaging materials were evaluated from the accuracy, precise, swiftness and convenience of viewpoint. Headspace analytical method was selected and recommended for using in food industry field.

• 한국포장학회지
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• 제10권1호
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• pp.1-6
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• 2004

Amount of residual ink solvent on the packaging materials from Korea, Japan and Europe was measured and compared. The amount of packaging materials from Korea was much higher than that of Japan and Europe. To reduce the residual amounts of ink solvent, aging condition of printed packaging materials including aging time and temperature was modified and evaluated. Aging with high temperature and short time ($60^{\circ}C$ and 24 hours) was more effective for reduction of residual amount of ink solvent than that with low temperature and long time. To find out change of reduction pattern of residual amount of solvent according to plastic packaging material, several monolayer and multilayer packaging materials were selected. Among the monolayer packaging materials, the amount of EVOH and PET was lower than that of polyolefin plastic film including PE and PP. PP/EVOH/PET among the selected multilayer film showed the lowest amount of residual ink solvent on food packaging materials. Result of this research revealed that the residual amount of ink solvent can be reduced by proper selection of aging condition with and by appropriate application of mutilayer plastic film.

• 한국축산식품학회지
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• 제31권5호
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• pp.641-648
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• 2011

This study investigated the effects of high pressure with or without thermal treatment on the cured color development and residual nitrite contents of model meat systems (pork, NaCl and sodium nitrite). At low nitrite levels (${\leq}50{\mu}g/g$), 200 MPa of pressure alone (P) did not develop the cured meat color (p>0.05). Thermal treatment (T) showed curing pigmentation (higher CIE L* and CIE a*), and the impacts were more effective when pressure was combined with thermal treatment (PT). In contrast, nitrite levels did not contribute to the cured meat color when ${\geq}200{\mu}g/g$ of nitrite was added to the meat. At high nitrite levels, although the typical cured color that is induced by thermal treatment did not present by pressure alone, the PT treatment still showed a pinker color with low residual nitrite content compared to the T treatment. The higher the pressure level (300 MPa), the greater the cured meat pigmentation with lower residual nitrite. Therefore, the present study demonstrates the possible application of high pressure, both for cured pigmentation and reducing residual nitrite, respective to typical thermal treatments.

• 유기물자원화
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• 제9권4호
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• pp.81-88
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• 2001

본 연구는 유기성 폐자원의 효율적인 처리 방법의 일환인 퇴비화를 이용하여 생산된 남은 음식물 퇴비(이하 음식물 퇴비)를 고추 재배지에 시용량 별로 처리한 후 작물 생육과 토양의 이화학성 변화에 미치는 영항을 평가하기 위해 수행되었다. 처리구는 무처리구, 대조구($20Mgha^{-1}$의 돈분 퇴비), 음식물퇴비를 20, 40, 60, $80Mgha^{-1}$을 시용한 처리구 등 모두 6 개를 두었으며 3 반복, 난괴법을 이용하였다. 토양 pH는 음식물 퇴비의 시용량이 많을수록 상승하는 경향이 컸으며, 전기 전도도를 비롯한 다른 토양 특성도 비슷한 경향을 보였다. 또한 음식물 퇴비 시용량이 많을수록 용적비중은 낮아지고 공극율은 증가하는 상관관계를 보였다. 작물생육은 퇴비 시용량이 많은 처리구에서 초기 생육이 저조하였으며 1차 생육조사에서 그 차이를 뚜렷하게 확인할 수 있었다. 고추의 생중량은 초기 생육에서 저해를 받은 처리구에서 특히 적었으며 음식물 퇴비의 $20Mgha^{-1}$처리구는 대조구에 비해 낮았지만 큰 차이는 크지 않았다. 음식물 퇴비의 수용성 유기성분과 염류에 의한 초기 생육부진과 고추 수확량 감소를 감안한다면 시용량은 $30Mgha^{-1}$을 초과하지 말아야 할 것으로 판단된다. 음식물 퇴비를 연용 시험을 통해 작물 생육과 토양에 미치는 영향을 평가하여 음식물 퇴비의 시용량을 설정하는 것이 바람직할 것으로 생각된다.

• 한국축산식품학회지
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• 제24권4호
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• pp.367-372
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• 2004

Nitrite, a curing agent of meat products, is precursors of carcinogenic N-nitrosamines during processing of meat products or under human stomach conditions as well as having its own toxicity. Some researches have been conducted to evaluate the effects of ionizing radiation on the reduction of residual nitrite and N-nitrosamines in an aqueous model system and cured meat products with different packaging methods during storage. These results showed that the gamma irradiation was effective in reducing the residual nitrite and N-nitrosamines in an aqueous model system as well as meat products. Especially, irradiation combined with vacuum or modified atmosphere packaging was more effective in nitrite and N-nitrosamines reduction than aerobic packaging during storage. The objective of this review is to introduce the irradiation technology for the application of reducing the residual nitrite and N-nitrosamine contents in meat products.

• 한국환경과학회지
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• 제18권12호
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• pp.1369-1381
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• 2009

The simultaneous determination of residual pesticides was developed using a gas chromatography. In this study, a simple and reliable methodology was improved to detect 175 kinds of residual pesticides by a liquid-liquid extraction procedure, followed by chromatographic analysis by gas chromatography. The 175 kinds of residual pesticides was classified into 4 groups according to the chemical structure, column type, resolution and sensitivity. The soybean sample selected for recovery experiment was not detected any pesticides. The recovery rates were ranged from 70.6% to 119.7% in most pesticides. The relative standard deviation (RSD 0.3~5.6%) was lower than 5.6% in all cases. The limits of detection (LOD) was lower than the maximum residue levels established by Korean legislations. The method has been successfully applied to the analysis of approximately 130 real samples.

• 한국식품과학회지
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• 제42권4호
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• pp.390-397
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• 2010

Residual solvents in foods are defined as organic volatile chemicals used or produced in manufacturing of extracts or additives, or functional foods. The solvents are not completely eliminated by practical manufacturing techniques and they also may become contaminated by solvents from packing, transportation or storage in warehouses. Because residual solvents have no nutritional value but may be hazardous to human health, there is a need to remove them from the final products or reduce their amounts to below acceptable levels. The purpose of this study was to develop and evaluate an analytical method for the screening of residual solvents in health functional foods. Furthermore, the aim of this study was to constitute a reasonable management system based on the current state of the market and case studies of foreign countries. Eleven volatile solvents such as MeOH, EtOH, trichloroethylene and hexane were separated depending on their column properties, temp. and time using Gas Chromatography (GC). After determining the GC conditions, a sample preparation method using HSS (Head Space Sampling) was developed. From the results, a method for analyzing residual solvents in health functional foods was developed considering matrix effect and interference from the sample obtained from the solution of solvents-free health functional foods spiked with 11 standards solutions. Validation test using the developed GC/HSS/MS (Mass Spectrometry) method was followed by tests for precision, accuracy, recovery, linearity and adequate sensitivity. Finally, examination of 104 samples grouped in suits was performed by the developed HSS/GC/MS for screening the solvents. The 11 solvents were isolated from health functional foods based on vapor pressure difference, and followed by separation within 15 minutes in a single run. The limt of detection (LOD), limit of quantification (LOQ), recovery and coefficient of variation (C.V.) of these compounds determined by the HSS/GC/MS were found to be 0.1 pg/mL, 0.1-125 pg/g, 51.0-104.6%, and less than 15%, respectively. Using the developed HSS/GC/MS method, residual solvent from 16 out of 104 health functional products were detected as a EtOH. This method therefore seems t o be a valuable extension ofanalytical method for the identification of residual solvents in health functional food.

• 한국식품과학회지
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• 제34권4호
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• pp.741-745
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• 2002

소시지 제조시 미생물을 제어함과 동시에 잔류 아질산염함량을 감소시키기 위하여 감마선을 이용하였다. 제조된 소시지는 함기, 진공, 그리고 $CO_2$(100%) 포장하여 감마선을 0, 5, 10 kGy로 조사한 후 4주 동안 냉장저장$(4^{\circ}C)$하면서 총균수, 대장균군수, 그리고 잔류 아질산염 함량을 조사하였다. 감마선 조사시 총균수와 대장균군의 수를 유의적으로 감소시켰으며 비조사구에서는 진공과 $CO_2$, 포장이 함기포장보다 미생물 생육제어에 효과적이었으며, 잔류 아질산염의 함량은 감마선 조사에 의해 유의적으로 감소하였다(p<0.05). 또한 $CO_2$ 포장구가 잔류 아질산염 함량 감소효과에 가장 뛰어난 결과를 얻어 감마선과 $CO_2$ 포장을 병용처리한다면 소시지 제조시 미생물 제어 및 잔류 아질산염의 함량을 효과적으로 감소시켜 소비자에게 더욱 안전한 식품을 공급하게 될 수 있으리라 사료된다.

• 한국환경농학회지
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• 제34권3호
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• pp.223-229
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• 2015

소면적 재배 작물 중 연속수확작물인 높은 들깻잎의 안전성 확보를 위하여 들깻잎 중 bifenthrin 및 chlorfenapyr의 잔류양상을 연구하였다. 확립된 분석법을 이용하여 회수율시험을 실시한 결과 bifenthrin 및 chlorfenapyr의 회수율은 81.9~104.8% 범위로 만족할만하였다. 들깻잎의 생육 기간 중 bifenthrin과 chlorfenapyr의 잔류량 변화는 first order kinetics model을 적용하여 해석하였으며 이 식으로부터 산출된 감소상수는 bifenthrin에서 $0.0724-0.0535day^{-1}$, chlorfenapyr에서 $0.0948-0.0821day^{-1}$로 나타났다. 두 농약의 들깻잎 중 반감기는 bifenthrin의 경우 9.6-12.9일이었으며, chlorfenapyr는 7.3-8.4일이었다. 산출된 두 농약의 감소상수를 이용하여 pre-harvest residue limit(PHRL)을 산출한 결과 수확 10일전 들깻잎 중 bifenthrin 및 chlorfenapyr의 잔류량이 각각 17.1 및 15.9 mg/kg일 경우 수확일에는 두 농약의 잔류허용기준인 7.0 및 10.0 mg/kg 이하로 잔류하여 안전할 것으로 예상되었다.