• 제목/요약/키워드: Recovery percentage

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Development of a Simultaneous Analysis Method for Disapproved Coloring Agents in Foods Using HPLC (HPLC를 이용한 식품중 허용 외 색소의 동시분석에 관한 연구)

  • Kim, Cheon-Hoe;Lee, Min-Jae;Kim, Keoung-Ok;Lee, Hyoun-Young;Yang, Joo-Hong;Heo, Seok;Park, Jong-Seok;Jang, Yeong-Mi;Kim, Hee-Yun
    • Korean Journal of Food Science and Technology
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    • v.40 no.4
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    • pp.375-381
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    • 2008
  • This study developed the simultaneous analysis method for efficient safety controls of import food of Orange II, Rhodamine B, Para Red, and Sudan dye I-IV among disapproved coloring agents that use is prohibited in foods. The analysis method was developed according to the sample pre-treatment and HPLC conditions, and a documentary survey was used to establish the detection limit of the method, followed by effectiveness verification and recovery percentage examinations. Recovery percentage examination for 26 products resulted Orange II displayed recovery percentage of 96.46-121.26%, Rhodamine B displayed recovery percentage of 70.86-106.53%, Para Red displayed recovery percentage of 97.00-116.86%, Sudan I displayed recovery percentage of 92.93-112.44%, Sudan II displayed recovery percentage of 96.63-115.10%, Sudan III displayed recovery percentage of 92.21-114.73%, Sudan IV displayed recovery percentage of 93.22-122.91%. Correlation coefficient of gradient of this analysis method exhibited more than 0.999, RSD exhibited fewer than 2 as 0.8-1.39%, exactitude exhibited more than 90%. At this time, detection limit and fixed quantity limit decided by each 0.1 mg/L, 0.3 mg/L.

Recovery of Nitric Acid from Waste Solder Stripper by Diffusion Dialysis (폐솔더 박리액으로부터 확산투석법에 의한 질산의 회수)

  • Ryu, Seong-Hyung;Kim, Tae-Young;Ahn, Nak-Kyoon;Gang, Myeong-Sik;Ahn, Jae-Woo;Ahn, Jong-Gwan
    • Resources Recycling
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    • v.24 no.5
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    • pp.33-39
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    • 2015
  • A basic study was conducted to effectively recover nitric acid from a waste solder stripper by diffusion dialysis using anion exchange membranes. The effects of flow rate, flux ratio, nitrate concentration, and metallic ion types and concentration on the recovery percentage of nitric acid were investigated. The recovery percentage of nitric acid was decreased with the increase of flow velocity. But the recovery percentage of nitric acid was increased as the increase of flux ratio(W/F) and showing a recovery percentage of nitric acid of about 99% at a flux ratio of 1.5 or more. As the increase of nitric acid concentration in feed solution, the recovery percentage of nitric acid was increased up to 3.0M, but in case of greater than 3.0M, the recovery percentage gradually was decreased. Leakage percentage of metallic ions through the membrane were in the order of Pb, Na and Cu but Fe and Sn did not leakaged. As a result of diffusion dialysis using real waste solder stripper at a flow rate of $0.9L/hr-m^2$, W/F = 1.3, a recovery percentage of nitric acid of approximately 94% was gained.

Recycling of Aluminum Alloy from Al-Cu Metal Matrix Composite Reinforced with SiC Particulates

  • Sharma, Ashutosh;Ahn, Byungmin
    • Korean Journal of Materials Research
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    • v.28 no.12
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    • pp.691-695
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    • 2018
  • In this study, we investigate the recycling of aluminum-based metal matrix composites(AMCs) embedded with SiC particulates. The microstructure of the AMCs is characterized by X-ray diffraction and scanning electron microscopy. The possibility of recycling the composite scrap is attempted from the melted alloy and SiC particulates by re-melting, holding and solidification in crucibles. The recovery percentage of the matrix alloy is calculated after a number of holding times, 0, 5, 10, 15, 20, 25 and 30 minutes and for different particulate sizes and weight fractions in the Al matrix. The results show that the recovery percentage of the matrix alloy, as well as the time required for maximum recovery of the matrix, is dependent on the size and weight fraction of SiC particulates. In addition, the percentage recovery increases with particulate size but drops with the particulate fraction in the matrix. The time to reach maximum recovery falls rapidly with an increase in particulate size and fraction.

Milling Condition and Harvesting Time for Improving Milling Recovery of Head Foxtail Millet Grain (완전미도정수율 향상을 위한 조(Setaria italica Beauvois) 도정방법 및 수확시기)

  • Lee, Jae-Saeng;Ko, Jee-Yeon;Song, Seuk-Bo;Woo, Koan-Sik;Kim, Jung-In;Kim, Hyun-Young;Jung, Tae-Wook;Kwak, Do-Yeon;Oh, In-Seok;Kim, Ki-Young
    • KOREAN JOURNAL OF CROP SCIENCE
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    • v.57 no.3
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    • pp.280-285
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    • 2012
  • This study was conducted to establish proper milling condition and harvesting time for improving the milling recovery of head foxtail millet grain. Brown foxtail millet recovery and the percentage of head foxtail millet recovery were significantly different according to the number of hulling and milling time. Also, the interaction of these factors had influence on brown foxtail millet recovery and the percentage of head foxtail millet recovery. To improve the percentage of head foxtail millet recovery, it was effective to hull grain twice and mill for 1.30 minute. 1000-grain weight of brown foxtail millet, brown foxtail millet recovery, hardness of brown foxtail millet, milling recovery, and the percentage of milling recovery of head foxtail millet grain were significantly different according to harvesting day after heading. For improving the ratio of ripened grain and the percentage of recovery of head foxtail millet, it is recommended to harvest 45 days (accumulated temperature : $1,148^{\circ}C$) after heading (DAH) in early maturing Hwangkeumjo, 50 DAH (accumulated temperature : $1,150^{\circ}C$) in mid-late maturing Samdamae and Kyeongkwan1, and 55 DAH (accumulated temperature : $1,168^{\circ}C$) in late maturing Samdachal.

An experimental study on the myocardial protection effect of the steroid mixed cardioplegic solution (Steroid를 첨가한 Cardioplegic solution의 심근보호효과에 관한 실험적 연구)

  • 유시원
    • Journal of Chest Surgery
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    • v.17 no.4
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    • pp.565-573
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    • 1984
  • The increasing use of cardioplegic solution for the reduction of ischemic tissue injury requires that all cardioplegic solution be carefully assessed for any protective or damaging properties. This study describes functional assessment of the efficiency of steroid in cardioplegic solution by using a Langendorffs perfusion model. Isolated rat heart were subject to a 2 minute period of coronary infusion with the steroid mixed cold cardioplegic solution immediately before and also at the midpoint of a 60 minutes period of hypothermic [10\ulcorner\ulcorner] ischemic arrest. The result of this study were as follows: 1.Spontaneous heart beat after ischemic arrest occurred 14 second later Langendorffs reperfusion in the steroid mixed Young & GIK group and 16 second later in the control group. [Young & GIK without steroid] A good recovery state of spontaneous heart beat was shown in both groups. 2.The percentage of recoveries of heart rate during the 30 minute after postischemic Langendorffs reperfusion was; at first 5 minute 106.3\ulcorner.7% [P<0.05] in the steroid mixed Young & GIK group. This percentage of recovery of steroid mixed Young & GIK group was significantly greater than the control group during the first 5 minute course. 3.The percentage of recovery of coronary flow during the 30 minute after postischemic Langendorffs reperfusion was; at first 5 minute 101\ulcorner.2% in the steroid mixed Young & GI K group. This percentage of recovery of the steroid mixed Young & GIK group was not significantly than the control group during the first 5 minute.

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Mineral Nutrition of the Field-Grown Rice Plant -[I] Recovery of Fertilizer Nitrogen, Phosphorus and Potassium in Relation to Nutrient Uptake, Grain and Dry Matter Yield- (포장재배(圃場栽培) 수도(水稻)의 무기영양(無機營養) -[I] 삼요소이용률(三要素利用率)과 양분흡수량(養分吸收量), 수량(收量) 및 건물생산량(乾物生産量)과(乾物生産量)의 관계(關係)-)

  • Park, Hoon
    • Applied Biological Chemistry
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    • v.16 no.2
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    • pp.99-111
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    • 1973
  • Percentage recovery or fertilizer nitrogen, phosphorus and potassium by rice plant(Oriza sativa L.) were investigated at 8, 10, 12, 14 kg/10a of N, 6 kg of $P_2O_5$ and 8 kg of $K_2O$ application level in 1967 (51 places) and 1968 (32 places). Two types of nutrient contribution for the yield, that is, P type in which phosphorus firstly increases silicate uptake and secondly silicate increases nitrogen uptake, and K type in which potassium firstly increases P uptake and secondly P increases nitrogen uptake were postulated according to the following results from the correlation analyses (linear) between percentage recovery of fertilizer nutrient and grain or dry matter yields and nutrient uptake. 1. Percentage frequency of minus or zero recovery occurrence was 4% in nitrogen, 48% in phosphorus and 38% in potassium. The frequency distribution of percentage recovery appeared as a normal distribution curve with maximum at 30 to 40 recovery class in nitrogen, but appeared as a show distribution with maximum at below zero class in phosphorus and potassium. 2. Percentage recovery (including only above zero) was 33 in N (above 10kg/10a), 27 in P, 40 in K in 1967 and 40 in N, 20 in P, 46 in Kin 1968. Mean percentage recovery of two years including zero for zero or below zero was 33 in N, 13 in P and 27 in K. 3. Standard deviation of percentage recovery was greater than percentage recovery in P and K and annual variation of CV (coefficient of variation) was greatest in P. 4. The frequency of significant correlation between percentage recovery and grain or dry matter yield was highest in N and lowest in P. Percentage recovery of nitrogen at 10 kg level has significant correlation only with percentage recovery of P in 1967 and only with that of potassium in 1968. 5. The correlation between percentage recovery and dry matter yield of all treatments showed only significant in P in 1967, and only significant in K in 1968, Negative correlation coefficients between percentage recovery and grain or dry matter yield of no or minus fertilizer plots were shown only in K in 1967 and only in P in 1968 indicating that phosphorus fertilizer gave a distinct positive role in 1967 but somewhat' negative role in 1968 while potassium fertilizer worked positively in 1968 but somewhat negatively in 1967. 6. The correlation between percentage recovery of nutrient and grain yield showed similar tendency as with dry matter yield but lower coefficients. Thus the role of nutrients was more precisely expressed through dry matter yield. 7. Percentage recovery of N very frequently had significant correlation with nitrogen uptake of nitrogen applied plot, and significant negative correlation with nitrogen uptake of minus nitrogen plot, and less frequently had significant correlation with P, K and Si uptake of nitrogen applied plot. 8. Percentage recovery of P had significant correlation with Si uptake of all treatments and with N uptake of all treatments except minus phosphorus plot in 1967 indicating that phosphorus application firstly increases Si uptake and secondly silicate increases nitrogen uptake. Percentage recovery of P also frequently had significant correlation with P or K uptake of nitrogen applied plot. 9. Percentage recovery of K had significant correlation with P uptake of all treatments, N uptake of all treatments except minus phosphorus plot, and significant negative correlation with K uptake of minus K plot and with Si uptake of no fertilizer plot or the highest N applied plot in 1968, and negative correlation coefficient with P uptake of no fertilizer or minus nutrient plot in 1967. Percentage recovery of K had higher correlation coefficients with dry matter yield or grain yield than with K uptake. The above facts suggest that K application firstly increases P uptake and secondly phosphorus increases nitrogen uptake for dry matter yied. 10. Percentage recovery of N had significant higher correlation coefficient with grain yield or dry matter yield of minus K plot than with those of minus phosphorus plot, and had higher with those of fertilizer plot than with those of minus K plot. Similar tendency was observed between N uptake and percentage recovery of N among the above treatments. Percentage recovery of K had negative correlation coefficient with grain or-dry matter yield of no fertilizer plot or minus nutrient plot. These facts reveal that phosphorus increases nitrogen uptake and when phosphorus or nitrogen is insufficient potassium competatively inhibits nitrogen uptake. 11. Percentage recovery of N, Pand K had significant negative correlation with relative dry matter yield of minus phosphorus plot (yield of minus plot x 100/yield of complete plot; in 1967 and with relative grain yield of minus K plot in 1968. These results suggest that phosphorus affects tillering or vegetative phase more while potassium affects grain formation or Reproductive phase more, and that clearly show the annual difference of P and K fertilizer effect according to the weather. 12. The correlation between percentage recovery of fertilizer and the relative yield of minus nutrient plat or that of no fertilizer plot to that of minus nutrient plot indicated that nitrogen is the most effective factor for the production even in the minus P or K plot. 13. From the above facts it could be concluded that about 40 to 50 percen of paddy fields do rot require P or K fertilizer and even in the case of need the application amount should be greatly different according to field and weather of the year, especially in phosphorus.

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Recovery of Tin from Tin Oxide Resulted from Glass Manufacturing Process by Pyrometallurgy (유리생산공정 폐주석산화물에서 건식제련에 의한 주석회수기술)

  • Lee, Sang-Ro;Kim, Sang-Yeol;Lee, Man-Seung;Park, Man-Bok
    • Resources Recycling
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    • v.24 no.2
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    • pp.23-28
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    • 2015
  • Most of the domestic need for tin rely on imports. In this work, a pyrometallurgical process was investigated to recover pure tin from the tin oxides in tin bath which results from the production of flat glass and LCD panel. From the results on the effect of reaction temperature, the highest recovery percentage of tin was obtained at $1350^{\circ}C$. The recovery percentage of tin was improved to 88% by employing the first and second smelting step. Electrorefining of the crude tin thus obtained led to pure tin with purity higher than 99.9%.

The Effect of Protein and Carbohydrate on the Recovery Rate of Restricted Rats (탄수화물 및 단백질이 식이 제한을 받은 흰쥐의 회복에 미치는 영향)

  • 신동순
    • Journal of the Korean Home Economics Association
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    • v.19 no.2
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    • pp.175-182
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    • 1981
  • This study was designed to compare the effect of protein with that of calorie, both of which were supplemented by separate feeding, on the recovery rate and metabolic change of undernourished rats. During the two weeks of food restriction, the weight of body and some major internal organs was reduced, compared with normal growing rats, but the extent of reduction was various. After that, recovery food was supplemented for two weeks. The amount of body nitrogen retention and its -percentage were lower in unsupplemented and sugar supplemented groups. Among the supplemented groups, its amount was increased according as the protein intake was higher, while its percentage was decreased. Body and internal organs weight change showed a similar tendency. Interrelation between calorie intake and body fat retention (liver fat content and epididymal fat pad weight) was not found regularly. Consequently, the recovery rate from restriction was higher in protein supplemented group than calorie supplemented group. But no significant difference could be found between the groups.

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Effect of Different Ratios of Concentrate and Roughage on Lipid Synthesis by Rumen Microorganisms In Vitro

  • Sasaki, H.;Horiguchi, K.;Takahashi, T.
    • Asian-Australasian Journal of Animal Sciences
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    • v.16 no.1
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    • pp.36-38
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    • 2003
  • The effect of different feeding ratios of concentrate to roughage on ruminal lipid synthesis in vitro was examined. Three sheep fitted with a rumen fistula were fed three different ratios (8:2, 4:6 and 0:10) of concentrate and roughage, and their rumen liquor were used for incubation. $^{13}C$-labeled glucose or sodium acetate as substrate was added to cultures of rumen liquor, and they were incubated for 6 h. The total lipid in the culture of the rumen liquor was extracted, and the percentage of $^{13}C$ excess was analyzed. The percentage of $^{13}C$ excess recovered when incubated with glucose increased with increased ratio of concentrate in the diet. The values of cultures incubated with glucose were higher than those incubated with sodium acetate except the roughage-only feeding. In the roughage-only diet, the percentage of $^{13}C$ excess when incubated with sodium acetate was highest of all diets. The recovery percentage of $^{13}C$ from glucose increased with increased ratio of concentrate. The recovery percentage of $^{13}C$ from sodium acetate addition in only roughage feeding was highest among the three diets. The recovery percentage of $^{13}C$ from glucose was markedly higher than that of sodium acetate addition in all feedings. The results indicate that high concentrate feeding facilitates lipid synthesis by rumen microorganisms, and that glucose may be the precursor for lipid synthesis rather than acetic acid.

Comparison of Extraction Methods for the Analysis of Total Petroleum Hydrocarbons in Contaminated Soil (오염토양내 석유계 총탄화수소 분석을 위한 추출방법의 비교)

  • Eui-Young Hwang;Wan Namkoong;Jung-Young Choi
    • Journal of Korea Soil Environment Society
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    • v.5 no.2
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    • pp.45-53
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    • 2000
  • Two extraction methods for total petroleum hydrocarbon (TPH) from contaminated soil were evaluated. The soil used for this study was sandy loam. Diesel oil was selected as representative petroleum hydrocarbons and was spiked at 100, 10,000, 50,000mg TPH/kg dry soil. Percentage recovery of TPH by shaking method was higher compared to Soxhlet extraction. At extraction time of 2 hours and sample to solvent ratio of 1 : 5, the highest percentage recovery was obtained. In this condition, percentage recovery of TPH in soil contaminated with 100mg/kg and 50,000mg/kg as TPH was 95.9% and 95.5%, respectively The volume of solvent lost by volatilization in shaking method was relatively small compared to Soxhlet extraction.

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