• Title/Summary/Keyword: Rapid quenching

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Investigation of Residual Stress Characteristics of Specimen Fabricated by DED and Quenching Processes Using Thermo-mechanical Analysis (열-기계 연계 해석을 이용한 에너지 제어 용착 및 담금질 공정으로 제작된 시편의 잔류응력 특성 분석)

  • Hwang, An-Jae;Lee, Kwang-Kyu;Ahn, Dong-Gyu
    • Journal of the Korean Society of Manufacturing Process Engineers
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    • v.20 no.12
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    • pp.113-122
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    • 2021
  • Complicated residual stress distributions occur in the vicinity of a deposited region via directed energy deposition (DED) process owing to the rapid heating and cooling cycle of the deposited region and the substrate. The residual stress can cause defects and premature failure in the vicinity of the deposited region. Several heat treatment technologies have been extensively researched and applied on the part deposited by the DED process to relieve the residual stress. The aim of this study was to investigate the residual stress characteristics of a specimen fabricated by DED and a quenching process using thermomechanical analyses. A coupled thermomechanical analysis technique was adopted to predict the residual stress distribution in the vicinity of the deposited region subsequent to the quenching step. The results of the finite element (FE) analyses for the deposition and the cooling measures show that the residual stress in the vicinity of the deposited region significantly increases after the completion of the elastic recovery. The results of the FE analyses for the heating and quenching stages further indicate that the residual stress in the vicinity of the deposited region remarkably increases at the initial stage of quenching. In addition, it is observed that the residual stress for quenching is lesser than that after the elastic recovery, irrespective of the deposited material.

A Study on the Film Boiling-Quenching Process of the Hot Surface for the Heat Treatment of Metals (1st Report, Cooling Curves and Transient Boiling Heat Transfer during the Quenching Process of Carbon Steel) (金屬熱處理를 위한 高溫面의 膜沸騰急冷却에 관한 硏究 (第1報, 炭素鋼 켄칭 過程의 冷却曲線과 過渡沸騰熱傳達))

  • Yun, Seok-Hun;Hong, Yeong-Pyo;Kim, Gyeong-Geun;Jeong, Dae-In
    • Journal of Advanced Marine Engineering and Technology
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    • v.15 no.3
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    • pp.57-65
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    • 1991
  • The quenching of steels by water is one of the important problems in engineering for the applications of heat treatment or continuous casting process, but the fundamental researches by the theoretical approaches have not been satisfactorily improved yet. The very rapid cooling problems by the thermal conduction including the latent heat of phase transformation in steel and the transient boiling heat transfer of water on the surface of the steel covering from $850^{\circ}C$ to $20^{\circ}C$ are the key problems of heat treatment. The present quenching experiments are performed for the cylindrical specimens of carbon steel, S45C of diameters (12-30). Nonlinear transient heat conduction and transient boiling heat transfer problem of water on the surface of specimens is analyzed by the numerical method of inverse heat conduction problem. The conditions for the calculation are that the initial temperature of specimens is $820^{\circ}C$ and the cooling water in bath are $20^{\circ}C$,$40^{\circ}C$,$60^{\circ}C$,$80^{\circ}C$,$95^{\circ}C$ with no agitation.

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CHILLING SENSITIVITY OF CUCUMBER PLANTS MONITORED IN TERMS OF CHLOROPHYLL FLUORESCENCE

  • Kang, In-Soon;Moon, Byoung-Yong;Seo, Kye-Hong;Chun, Hyun-Sik;Lee, Chin-Bum
    • Journal of Photoscience
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    • v.3 no.1
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    • pp.9-14
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    • 1996
  • For three cultivars of chilling-sensitive cucumber plants, chilling sensitivity was evaluated in terms of photosynthetic activity using Chl fluorescence techniques. Low-temperature treatment caused a decrease in photosynthetic activities of cucumber leaves, measured as CO$_2$ exchange, as well as the decrease in the stomatal conductance. FR of the three cultivars decreased after chilling for 24 h in light and the extent of decline of F$_R$ was the greatest in 'Chosaeng' cultivar. When these plants were recovered from light-chilling, 'Chosaeng' and 'Samchuk' cultivars did not fully restore the original value of F$_R$ after 24 h of recovery, in contrast to 'Ilmi' cultivar which showed a rather efficient recovery. The results of FR study showed that 'Chosaeng' was most susceptible, whereas Ilmi was most resistant, to chilling among the three cultivars of cucumber plants. When quenching coefficients for chlorophyll fluorescence was analyzed after chilling the cucumber plants for 24 h in light, 'Chosaeng' elicited more rapid declines in the coefficients for photochemical quenching (qQ), non-photochemical quenching (qNP) and energy-dependent quenching (qE) than 'Ilmi' and 'Samchuk'. The implications of these observations are discussed in relation to the growth habits of the respective cultivars in the field. The results showed that measurement of chlorophyll fluorescence was an effective means of screening chilling tolerance of cucumber plants. Furthermore, the study on the chlorophyll fluorescence induction and fluorescence quenching charactersitics showed that low temperature could accelerate inhibition of photosynthesis in chilling-sensitive plants, by limiting Calvin cycle activity and disrupting, in part, the energy dissipation mechanims of the photosystem II.

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Analysis of Phase Transformation and Temperature History during Hot Stamping Using the Finite Element Method (유한요소해석을 이용한 핫스탬핑 공정시 발생하는 온도 이력 및 상변태 해석)

  • Yoon, S.C.;Kim, D.H.
    • Transactions of Materials Processing
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    • v.22 no.3
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    • pp.123-132
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    • 2013
  • Hot stamping, which is the hot pressing of special steel sheet using a cold die, can combine ease of shaping with high strength mechanical properties due to the hardening effect of rapid quenching. In this paper, a thermo-mechanical analysis of hot stamping using the finite element method in conjunction with phase transformations was performed in order to investigate the plastic deformation behavior, temperature history, and mechanical properties of the stamped car part. We also conducted a fully coupled thermo-mechanical analysis during the stamping and rapid quenching process to obtain the mechanical properties with the consideration of the effects of plastic deformation and phase transformation on the temperature histories at each point in the part. The finite element analysis could provide key information concerning the temperature histories and the sheet mechanical properties when the phase transformation is properly considered. Such an analysis can also be used to determine the effect of cyclic cooling on the tooling.

The Effect of Hot Stamping Operation Condition on the Mechanical Properties (핫스탬핑 공정조건에 따른 기계적 특성)

  • Kim, H.D.;Moon, M.B.;Lee, S.H.;Yoon, K.W.;Yoo, J.H.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2008.10a
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    • pp.317-320
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    • 2008
  • The Hot Stamping process, which is the hot pressing of steel parts using cold dies. can utilize both case of shaping and high strength due to the hardening effect of rapid quenching during the pressing. We carried out experiments of quenching rate and tempering treatments at temperatures of $200^{\circ}C$ and $300^{\circ}C$ and different soaking times. Tn this study, the mechanical properties and microstructure of micro boron alloyed steels after heat treatments are compared.

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Try out and Analytical Researches on Quenching Process of Coupled Torsion Beam Axle using Boron Steel Tube (보론강을 이용한 CTBA의 후열처리 공정 실험 및 해석)

  • Yoon, S.J.;Park, J.K.;Kim, Y.S.;Suh, C.H.;Lee, K.H.;Kim, R.Y.
    • Proceedings of the Korean Society for Technology of Plasticity Conference
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    • 2009.10a
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    • pp.181-184
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    • 2009
  • The hot press farming process, which is the press hardening of steel parts using cold dies, can utilize both ease of shaping and high strength due to the hardening effect of rapid quenching during the pressing. In this study, a thermo-elastoplastic analysis of the hot press forming process using the finite element method was performed in order to investigate the deformation behavior and temperature history during the process and the mechanical properties of the pressed parts.

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Detection of Nitroaromatic Compounds Based on Fluorescent Silafluorene Chemosensors

  • Kim, Bumseok
    • Journal of Integrative Natural Science
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    • v.3 no.1
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    • pp.19-23
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    • 2010
  • A simple and rapid method is described for detecting nitroaromatic explosives in air or seawater with the use of photoluminescent organosilicon compounds. The synthesis, spectroscopic characterization, and fluorescence quenching efficiency of silafluorenes are reported. Silafluorenes were synthesized from the reduction of dilithiobiphenyl with dichlorosilanes. Two silafluorenes were used for the detection of nitroaromatic compounds. Detection of nitroaromatic molecules, such as 2,4-dinitrotoluene (DNT), 2,4,6-trinitrotoluene (TNT), and picric acid (PA), has been explored. A linear Stern-Volmer relationship was observed for the first three analytes. Fluorescence spectra of silafluorenes obtained in either toluene solutions or thin films displayed no shift in the maximum of the emission wavelength. The photoluminescence quenching occurs by a static mechanism.

Novel green Sr4ScAl3O10:Eu2+ phosphor prepared by the melt quenching technique

  • Toda, Kenji;Iwaki, Masato;Katsu, Minenori;Kamei, Shin-nosuke;Kim, Sun-Woog;Hasegawa, Takuya;Muto, Masaru;Yamanashi, Ryota;Sakamoto, Tatsuya;Ishigaki, Tadashi;Uematsu, Kazuyoshi;Sato, Mineo;Yoon, Dae-Ho
    • Journal of Ceramic Processing Research
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    • v.20 no.3
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    • pp.276-279
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    • 2019
  • New green-emitting Sr4ScAl3O10:Eu2+ phosphor was prepared using a novel melt quenching synthesis method. The temperature of raw materials irradiated with the strong light of the Xe arc-lamp was rose up to about 2273 K, followed by a sharp drop in the temperature after turn off the lamp. This method is a useful tool for rapid screening of novel phosphor materials.

A Study on the Synthesis and Characteristics of Carbon Nanomaterials by Thermal Plasma (열플라즈마를 이용한 탄소 나노 물질의 합성 및 특성에 관한 연구)

  • Seong-Pyo Kang;Tae-Hee Kim
    • Journal of the Korean institute of surface engineering
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    • v.57 no.3
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    • pp.155-164
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    • 2024
  • Physical properties of carbon nanomaterials are dependent on their nanostructures and they are modified by diverse synthesis methods. Among them, thermal plasma method stands out for synthesizing carbon nanomaterials by controlling chemical and physical reactions through various design and operating conditions such as plasma torch type, plasma gas composition, power capacity, raw material injection rate, quenching rate, kinds of precursors, and so on. The method enables the production of carbon nanomaterials with various nanostructures and characteristics. The high-energy integration at high-temperature region thermal plasma to the precursor is possible to completely vaporize precursors, and the vaporized materials are rapidly condensed to the nanomaterials due to the rapid quenching rate by sharp temperature gradient. The synthesized nanomaterials are averagely in several nanometers to 100 nm scale. Especially, the thermal plasma was validated to synthesize low-dimensional carbon nanomaterials, carbon nanotubes and graphene, which hold immense promise for future applications.