• Bulletin of the Korean Chemical Society
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• 제26권3호
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• pp.467-469
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• 2005

• 대한화학회지
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• 제19권1호
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• pp.38-42
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• 1975

2-Acetothienone과 chloral을 축합시켜 chloral-2-acetothienone을 생성하였으며 이것을 탈수하여 trichloroethylidene-2-acetohienone을 합성하였다. Trichloroethylidene-2-acetothienone과 phenylhydrazine 또는 치환된 phenylhydrazine들과의 반응으로 2-aryl-6-(2-thienyl)-3(2H)-pyridazinone들을 얻었으며 hydrazine과의 반응에서는 3-(2-thienyl)-5-trichloromethyl-2-pyrazoline이 합성되었다.

• 대한화학회지
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• 제67권4호
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• pp.306-310
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• 2023

• Bulletin of the Korean Chemical Society
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• 제27권7호
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• pp.1083-1085
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• 2006

• 대한화학회지
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• 제61권5호
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• pp.291-295
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• 2017

• Bulletin of the Korean Chemical Society
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• 제23권12호
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• pp.1715-1718
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• 2002

Treatment of ethyl 5-hydroxy-3,4-diphenylthieno[2,3-c]pyridazine-6-carboxylate (1a) with hydrazine hydrate in ethanol gave the carbohydrazide 2,. Some derivatives of the latter compound have been synthesized. Also, 6-acetyl-3,4-diphenyl-5-hydroxythieno[2.3-c]pyridazine (1b) was subjected to some reactions to produce other new thienopyridazine derivatives.

• 대한화학회지
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• 제48권3호
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• pp.331-334
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• 2004

• 대한화학회지
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• 제17권1호
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• pp.25-30
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• 1973

$\gamma$,$\gamma$,$\gamma$-Trichloroethylidene-m-Nitroacetophenone과 phenylhydrazine및 치환된 phenylhydrazine들과의 반응으로 2,6-disubstituted-3-pyridazinone들을 합성하였으며 2,4-dinitrophenylhydrazine과의 반응에서는 hydrazone을 중간체로 분리하였다. hydrazinehydrate와의 반응에서는 3-(mnitrophenyl)-5-trichloromethyl-2-pyrazoline이 좋은 수득률로 얻어졌다. 또한$\gamma$,$\gamma$,$\gamma$-trichloroethylidene-m-nitroacetophenone과 치환된 phenylhydrazine과의 반응에서 phenyl기에 결합된 치환기의 효과를 검토하였다.

• 한국인쇄학회지
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• 제21권2호
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• pp.101-108
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• 2003

We synthesised 1,3-Diphenyl-5-pyren-2-yl-4,5-dihydro-1H-pyrazole(DPP) and investigated its optical properties. The structure of DPP was confirmed by GC-Mass and elemental analysis. The absorption and photoluminescent spectra of DPP were measured at both hydrophobic and hydrophilic solvents and by the stokes shifts of DPP Lippert's equation could be applied. The results showed linear relation between $[{\varepsilon}-1/2{\varepsilon}+1)-(n^2-1/2n^2+1)]$ and $({\mu}_g\;-\;{\mu}_2)^2$.

• Bulletin of the Korean Chemical Society
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• 제28권9호
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• pp.1539-1544
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• 2007

1-Phenyl-3-p-fluorophenyl-5-p-chlorophenyl-2-pyrazoline has been synthesized and characterized by elemental analysis, IR, UV-Vis and X-ray single crystal diffraction. Density functional calculations show that B3LYP/6-311G** method can reproduce the structural parameters. The electronic absorption spectra have been predicted based on the optimized structure by using 6-311G** and 6-311++G** basis sets and compared with the experimental values. The results indicate that TD-DFT method can only predict the electronic absorption spectra of the system studied here approximately. On the basis of vibrational analyses, the thermodynamic properties of the title compound at different temperatures have been calculated, revealing the correlations between ,C0p,m,S0m,H0m and temperature.