• Bulletin of the Korean Chemical Society
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• v.34 no.6
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• pp.1698-1702
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• 2013

Glucose is a common medical analyte measuring in human serum or blood samples. The development of a primary method is necessary for the establishment of traceability in measurements. We have developed an isotope dilution liquid chromatography tandem mass spectrometry as a primary method for the measurement of glucose in human serum. Glucose and glucose-$^{13}C_6$ in sample were ionized in ESI negative mode and monitored at mass transfers of m/z 179/89 and 185/92 in MRM, respectively. Glucose was separated on $NH_2P$-50 2D column, and the mobile phase was 20 mM $NH_4OAc$ in 30% acetonitrile/70% water. Verification of this method was performed by the comparison with NIST SRMs. Our results agreed well with the SRM values. We have developed two levels of glucose serum certified reference material using this method and distributed them to the clinical laboratories in Korea as samples for proficiency testings. The expended uncertainty was about 1.2% on 95% confidence level. In proficiency testings, the results obtained from the clinical laboratories showed about 3.6% and 3.9% RSD to the certified values. Primary method can provide the traceability to the field laboratories through proficiency testings or certified reference materials.

• Steel and Composite Structures
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• v.48 no.3
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• pp.335-351
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• 2023

This research studies the primary resonance and nonlinear vibratory responses of multilayer functionally graded shallow (MFGS) shells under external excitations. The shells considered with functionally graded porous (FGP) core and resting on two types of nonlinear viscoelastic foundations (NVEF) governed by either a linear model with two parameters of Winkler and Pasternak foundations or a nonlinear model of hardening/softening cubic stiffness augmented by a Kelvin-Voigt viscoelastic model. The shells considered have three layers, sandwiched by functionally graded (FG), FGP, and FG materials. To investigate the influence of various porosity distributions, two types of FGP middle layer cores are considered. With the first-order shear deformation theory (FSDT), Hooke's law, and von-Kármán equation, the stress-strain relations for the MFGS shells with FGP core are developed. The governing equations of the shells are consequently derived. For the sake of higher accuracy and reliability, the P-T method is implemented in numerically analyzing the vibration, and the method of multiple scales (MMS) as one of the perturbation methods is used to investigate the primary resonance. The results of the present research are verified with the results available in the literature. The analytical results are compared with the P-T method. The influences of material, geometry, and nonlinear viscoelastic foundation parameters on the responses of the shells are illustrated.

• Transactions of the Korean Society of Automotive Engineers
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• v.7 no.9
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• pp.10-19
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• 1999

In this study , a simple method has been developed to detect the required spark voltage by using the primary spark voltage instead of the secondary spark voltage. Through engine motoring experiments, this method testified to be quite satisfactory. Though the required spark voltage is affected by many in-cylinder conditions, temperature is one of the most important factors. The temperature increases significantly by combustion and the required spark voltage also changes by the temperature during the expansion stroke. On the basis of this fact, misfire can be monitored by comparing the required spark voltage between compression stroke and expansion stroke. So, in this study, two step ignition method is introduced to monitor combustion at expansion stroke. The test result shows that this method can be used to detect complex misfire pattern.

• International Journal of Advanced Culture Technology
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• v.10 no.4
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• pp.102-109
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• 2022

In order to explore the characteristics that are more suitable for the physical and mental development of young people, enrich the existing martial arts teaching material system. Through the literature method, experimental method, questionnaire method and other research methods, the teaching comparison experiment of martial arts textbooks in primary and secondary schools was carried out, and the attitudes of martial arts courses at different ages in primary and secondary schools were analyzed. For different types of martial arts teaching materials, primary school students are more fond of them than junior high school students, and students of different ages also have different degrees of love for the four types of martial arts teaching materials, pointing out that it is necessary to carry out the reform of martial arts teaching materials as soon as possible, improve the difficulty, teach martial arts skills and knowledge in the combination of attack and defense, and reduce the trend of gymnastics; adjust and improve the periodicity, pertinence and diversity of martial arts teaching materials; mobilize students' enthusiasm for learning, cultivate students' interest in martial arts, and promote the inheritance of martial arts In the process of martial arts teaching, students' sense of identification with traditional Chinese culture is enhanced, and cultural self-confidence is enhanced.

• Geomechanics and Engineering
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• v.36 no.6
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• pp.575-587
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• 2024

The contact pressure between the surrounding rock and the support is an important indicator of the surrounding rock pressure. There has been a bottleneck in the prediction of contact loads between surrounding rock and primary support in deep-buried mountain tunnels. The main reason is that a reliable method wasn't existed to quantify the contact loads. This study had been taken into account the flexible support role of the primary support, and the fitting curve of surrounding rock deformation for dynamic tunnel construction was proposed. New formulas for the calculation of contact loads between surrounding rock and primary support were obtained by inversion. Comparative analysis of the calculation results with numerical simulation verified the reliability of the calculation method in this study. It can be seen from the analyses that the contact load between surrounding rock and primary support increases, remains unchanged and decreases during acceleration, uniform velocity and deceleration, respectively, and the deformation of the surrounding rock in the acceleration and deceleration stages cannot completely converted into contact loads. The contact loads between surrounding rock and primary support of medium-strength and weak surrounding rock tunnels are generally within 150 kPa and 1 MPa, respectively. For tunnels with weak surrounding rock, advanced support can be installed to reduce the unique release coefficient λ₀ and the value of the constant D, with the purpose of reducing the contact loads between surrounding rock and primary support. Changes in support parameters have a small effect on the contact loads between surrounding rock and primary support, but increase or decrease the safety factor, resulting in a waste of resources or a situation that threatens the safety of the support. The results of this research provide guidance for the prediction of contact loads between surrounding rock and primary support for dynamic tunnel construction.

• Journal of the Korean Graphic Arts Communication Society
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• v.30 no.2
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• pp.35-45
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• 2012

Need color separation process to appear number of minimum printing plate waterway maximum printing color at printing process. This time, printing plate is separated three primary colors of C(cyan), M(magenta), Y(yellow). Appear all colors of printing such three primary colors. But, three primary color ink appears 100% dark gray that is not clean as chroma is neared color to 0 because is not pure. As well as, the ink area rate that is whole by over print amount increase of three primary is expanded. As a result, influence in secondary printablity set-off growth by inaccurate color reproduction and ink dry badness, trapping efficiency decline etc.. Apply ink saving method that is replaced as K ink in consisted dark color constituent because three primary colors are over print each other adding one more K(black) plate by method to improve these problem. Therefore, can reduce extension of the total ink area rate, and help in correct color appearance control. As well as, eco-friendly printing process attains improving printablity at the same time curtailment of printing expense by reducing requirement of total ink. Usually, there are UCR(under color removal) and GCR(gray component replacement) to ink saving application method. But, the practical use limit is insufficient state to tribe of technological investigation or field application about these method in domestic printing field. Therefore, in this research, ink saving been bringing by one method of eco-friendly printing confirmed that is applicable in usual domestic printing environment. Also, searched result getting in printablity by ink saving application.

• The Journal of Korean Institute of Communications and Information Sciences
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• v.33 no.11A
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• pp.1105-1116
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• 2008

Cognitive radio is one of the most effective techniques to improve the spectrum utilization efficiency. To implement the cognitive radio, spectrum sensing is considered as the key functionality because only counting on it, can the secondary users identify the spectrum holes and utilize them efficiently without causing interference to primary users. Generally, there are several spectrum sensing methods; the most common and simplest method is energy detection. However, the conventional energy detection has some disadvantages, which are caused by noise, especially, uncertain noise power leads to degradation of energy detector. In this paper, to solve this problem, we proposed sliding window-based energy detection method which can devide the frequency band of primary signal and noise using sliding window to estimate the power of primary user without the noise effect and achieve the better performance. It can calculate the energy of primary user only and can detect the primary signal. The simulation result shows that our proposed method outperforms conventional one.

• Transactions of the Korean Society of Mechanical Engineers A
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• v.26 no.6
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• pp.1194-1202
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• 2002

A study on the topology optimization of a multi-spectral camera for space-use is presented. The optimization is carried out under self-weight and polishing pressure loading. A multi-spectral camera for space-use experiences degradation of optical image in the space, which can not be detected on the optical test bench on the earth. An optical surface deformation of a primary mirror, which is a principal component of the camera system, is an important factor affecting the optical performance of the whole camera system. In this study, topology optimization of the primary mirror of the camera is presented. As an objective function, a measure of Strehl ratio is used. Total mass of the primary mirror is given as a constraint to the optimization problem. The sensitivities of the objective function and constraint are calculated by direct differentiation method. Optimization procedure is carried out by an optimality criteria method. For the light-weight primary mirror design, a three dimensional model is treated. As a preliminary example, topology optimization considering a self-weight loading is treated. In the second example, the polishing pressure is also included as a loading in the topology optimization of the mirror. Results of the optimized design topology for the mirror with various mass constraints are presented.

• Proceedings of the KAIS Fall Conference
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• 2007.11a
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• pp.74-77
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• 2007

Primary charging roller rotated with contacting surface of OPC drum and take charge OPC drum. Owing to this reason, primary charging roller made by elasticity substance with electric conduction. Properties of charging and image changed by class of coating, method of coating and environment. This study developed about coating method to make print image of good quality.

• Journal of Biosystems Engineering
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• v.23 no.4
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• pp.373-380
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• 1998

The contribution of this paper is to provide the methods for the production automation of potato microtuber using the vision process in growth monitoring. The first method deals with computation for the growth density in the primary growth process. The second method addresses cognition process to identify the number and the volume of potato microtuber in secondary growth process. The third is to decide whether potato microtubers are infected by a virus or bacteria in growth process. The computation for the growth density in the primary growth process uses the method of Labeling. The second and third methods use template matching based on color patterns. With the developed method using vision process, this experiment is capable of discriminating weekly growth-rate in primary growth process, 85% cognition rate in secondary process and identifying whether there are infections. Therefore, we conclude that our experimental results are capable of growth monitoring for mass production of potato microtubers.