• 제목/요약/키워드: Primary Si

검색결과 524건 처리시간 0.028초

Surface Defects States on a SiO2/Si Observed by REELS

  • Kim, Juhwan;Kim, Beomsik;Park, Soojeong;Park, Chanae;Denny, Yus Rama;Seo, Soonjoo;Chae, Hong Chol;Kang, Hee Jae
    • 한국진공학회:학술대회논문집
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    • 한국진공학회 2013년도 제44회 동계 정기학술대회 초록집
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    • pp.271-271
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    • 2013
  • The defect states of a Ar-sputtered SiO2 surface on Si (001) were investigated using Auger electron spectroscopy (AES) and reflection electron energy loss spectroscopy (REELS). The REELS spectra at the primary electron energy of 500 eV showedthat three peaks at 2.5, 5.1, and 7.2 eV were found within the band gap after sputtering. These peaks do not appear at the primary electron energies of 1,000 and 1,500 eV, which means that the defect states are located at the extreme surface of a SiO2/Si thin film. According to the calculations, two peaks at 7.2 and 5.1 eV are related to neutral oxygen vacancies. However, the third peak at 2.5 eV has never been previously reported and the theories proposed that this defect state may be due to Si-Si bonding. Our Auger data showed that a peak for Si-Si bonding at 89 eV appears after Ar ion sputtering on the surface of the sample, which is consistent with the theoretical models.

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Hot Top공정으로 제조한 A390합금 주조봉의 표면 돌기 생성에 관한 연구 (A Study on the Formation of the Bosses on the Surface of A390 Cast Bar with Hot Top Process)

  • 이정무;강석봉;김병조
    • 연구논문집
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    • 통권25호
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    • pp.155-161
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    • 1995
  • During casting of A390 billet by Hot Top process, bosses were formed on the surface of cast bar. The formation of boss is assumed due to a large amount of latent heat released during the formation of primary Si in A390 alloy. The low melting point elements around primary Si are locally remelted to liquid and interdendrite offers a path by which the liquid can pass through to the surface. Addition of Sr decreases the amount of latent heat by preventing the formation of primary Si near the surface and thus suppresses the formation of boss on the surface of cast bar. Therefore, the formation of boss could be reduced remarkably when the casting condition was selected to extract the latent heat outward easily.

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표면크랙 예측을 위한 결정립 제어 레오로지 소재 표면의 나노 변형특성에 관한 연구 (A Study on the Nano-Deformation Characteristics of Grain-Size Controlled Rheology Material Surfaces for Surface Crack Prediction)

  • 윤성원;김현일;강충길
    • 한국정밀공학회:학술대회논문집
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    • 한국정밀공학회 2004년도 추계학술대회 논문집
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    • pp.355-358
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    • 2004
  • In this study, the deformation characteristics of grain-size controlled rheology materials surfaces were investigated as a part of the research on the surface crack prediction in semi-solid formed automobile components. The microstructure of rheology Al-Si alloys consists of primary and eutectic regions. In eutectic regions the crack initiation begins with initial fracture of the eutectic silicon particles and inside other intermetallic phases. Nano-deformation characteristics in the eutectic and primary region of semi-solid aluminum alloys (356 alloy and 319 alloy) were investigated through the nanoindentation/scratch experiments and the AFM observation.

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Effect of Asymmetric Hot Rolling on the Texture Evolution of Fe-3%Si Steel

  • Na, Tae-Wook;Park, Hyung-Ki;Park, Chang-Soo;Joo, Hyung-Don;Park, Jong-Tae;Han, Heung Nam;Hwang, Nong-Moon
    • Metals and materials international
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    • 제24권6호
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    • pp.1369-1375
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    • 2018
  • In Fe-3%Si steel, the hot rolling process affects not only the hot rolling texture but also the primary recrystallization texture. Here, the effect of asymmetric hot rolling was studied by comparing the difference in the texture evolved between asymmetric and symmetric hot rolling. The effect of asymmetric hot rolling on the texture of primary recrystallized Fe-3%Si steel was also studied. The symmetric hot rolling of Fe-3%Si steel produces a rotated cube texture at the center but Goss and copper textures near the surface. Asymmetric hot rolling tends to produce Goss and copper textures even at the center like the texture near the surface. After primary recrystallization, the dominant texture at the center changes from {001} <210> to {111} <112> and the new texture has a higher fraction of the grains which make the low energy boundary with Goss grains than that of symmetric hot rolling.

A TRADE OFF STUDY OF LIGHTWEIGHT PRIMARY MIRROR FOR SPACEBORNE TELESCOPE

  • LEE Haeng-Bok;Choi Se-Chol
    • 한국우주과학회:학술대회논문집(한국우주과학회보)
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    • 한국우주과학회 2005년도 한국우주과학회보 제14권2호
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    • pp.149-152
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    • 2005
  • High-resolution telescope from space comprises electro-optical imagery with a ground resolution tying within the range of 1 to 5 meters. According to information documented in the literature up to now, most primary mirrors verified and flown in optical space missions have been lightweighted made from Zerodur, ULE, beryllium, SiC or aluminium. A trade off study was performed to determine as a &lightweighted& by factors like backside cell pattern, rib thickness, face thickness, mirror fixation device location and material and so on based on structural performance for primary mirror in submeter class spaceborne telescope.

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Mechanical Properties and Castabilities of Al-12Mg-5.5Zn-xSi Alloys

  • Kim, Jeong-Min;Sung, Ki-Dug;Jun, Joong-Hwan;Kim, Ki-Tae;Jung, Woon-Jae
    • 한국주조공학회지
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    • 제24권6호
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    • pp.340-346
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    • 2004
  • 초정 $Mg_2Si$와 미세한 $MgZn_2$ 석출상을 갖는 고강도 내마모 Al합금을 개발하기 이하여 Al-l2wt%Mg-5.5wt%Zn합금에 0-5wt%까지 Si을 첨가 시켰으며, 미세조직 및 기계적 성질에 미치는 영향을 조사하였다. Si의 함량이 증가함에 따라 형성되는 $Mg_2Si$상의 양이 증가하였으며, 동시에 고강선 온도가 점차적으로 증가함에 따라 효과적인 열처리가 가능해지는 것을 관찰할 수 있었다. 5wt%Si이 첨가된 합금의 경우 적절한 열처리를 통해 미세한 $MgZn_2$ 석출상이 기지에 균일하게 분포한 미세조직을 얻을 수 있었고 이를 통해 인장강도를 현저하게 증가시킬 수 있었다. 또한 Si이 첨가된 Al-Mg-Zn합금은 유동도 및 열간 균열저항성과 같은 주조성면에서도 다른 고강도 Al합금에 비하여 월등히 우수한 것으로 나타났다.

분사주조한 입자강화 알루미늄 복합재료의 미세조직 특성 (Characteristics in Microstructure of Particle Reinforced Al Matrix Composites Fabricated by Spray-Cast Forming Process)

  • 박종성;이인우;김명호
    • 한국주조공학회지
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    • 제14권6호
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    • pp.530-540
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    • 1994
  • Aluminium-silicon alloy(JIS AC8A) matrix composites reinforced with SiC particles were fabricated by spray-cast forming process, and the microstructure of powders and preforms produced were studied by using an optical and scanning electron microscopy. SiC particles were co-sprayed by mixed phase injection method during the spray casting process. Most of the composite powders formed by this mixed phase injection method exhibit morphology of particle-embedded type, and some exhibits the morphology of particle attached type due to additional attachment of the SiC particles on the surface of the powders in flight. The preforms deposited were resulted in dispersed type microstructure. The pre-solidified droplets and the deposited preform of SiC-reinforced aluminium alloy exhibit finer equiaxed grain size than that of unreinforced aluminium alloy. Eutectic silicons of granular type are crystallized at the corner of the aluminum grains in the preforms deposited, and some SiC particles seem to act as nucleation sites for primary/eutectic silicon during solidification. Such primary/eutectic silicons seem to retard grain growth during the continued spray casting process. It is envisaged from the microstructural observations for the deposited preform that the resultant distribution of SiC injected particles in the Al-Si microsturcture is affected by the amount of liquid phase in the top part of the preform and by the solidification rate of the preform deposited.

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Microstructure and Consolidation of Gas Atomized Al-Si Powder

  • Hong, S.J.;Lee, M.K.;Rhee, C.K.;Chun, B.S.
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part2
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    • pp.994-995
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    • 2006
  • The microstructure of the extruded Al-20Si bars showed a homogeneous distribution of eutectic Si and primary Si particles embedded in the Al matrix. The grain size of ${\alpha}-Al$ varied from 150 to 600 nm and the size of the eutectic Si and primary Si in the extruded bars was about 100 - 200 nm. The room temperature tensile strength of the alloy with a powder size $<26{\mu}m$ was 322 MPa, while for the coarser powder ($45-106{\mu}m$) it was 230 MPa. With decreasing powder size from $45-106{\mu}m$ to $<26{\mu}m$, the specific wear of all the alloys decreased significantly at all sliding speeds due to the higher strength achieved by ultrafine-grained constituent phases. The fracture mechanism of failure in tension testing and wear testing was also studied.

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고액 공존영역 온도 열처리에 의한 Al-Si합금의 초정 구형화 (Sphering of Primary Dendrites in Al-Si alloys by Mushy Zone Heat Treatments)

  • 안중호;송인혁;한유동
    • 한국주조공학회지
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    • 제16권6호
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    • pp.513-522
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    • 1996
  • In the present work, we have investigated the strain-induced melt activation (SIMA) process in Al-8%Si and Al-25%Si alloys. Primary dendrites were transformed into spherical microstrctures by mushy zone heat treatments of the cold-worked alloys. Various processing parameters which govern the sphering of the dendrites have been examined. The result showed that semi-solid alloys having a typically nondendritic spherical microstructure can be easily produced by this method.

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Al-Si-Cu합금에서 Fe 함량에 따른 $\beta-Al_5FeSi$ 금속간화합물의 형성 및 응고미세조직 특성 (Formation and Microstructure Characteristics of $\beta-Al_5FeSi$ Intermetallic Compound in the Al-Si-Cu Alloys with the Variation of Fe Content)

  • 김봉환;이상목
    • 한국주조공학회지
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    • 제29권5호
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    • pp.225-232
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    • 2009
  • For comprehensive understanding of the formation behavior of $\beta-Al_5FeSi$ phase in Al-Si-Cu alloys with the existence of Fe element, microstructure characterizations were performed using combined analysis of OM, SEM-EDS, XRD. Especially, experimental and predictive works on solidification events of $\beta-Al_5FeSi$ phase as well as other phases formed together with $\beta-Al_5FeSi$ have been carried out by using DSC analysis and Java-based Materials Properties software (J. Mat. Pro.). Primary and eutectic $\beta-Al_5FeSi$ phases were able to distinguish from each other on microstructures by their morphological features. Primary $\beta-Al_5FeSi$ phase was seen to have rough surface perpendicular to growth direction, indicating free attachment of solute atoms in liquid state. On the other hand, the eutectic $\beta-Al_5FeSi$ phase was formed with plain and straight surface during eutectic reaction together with $\alpha$-Al phase. The eutectic reaction of $\beta-Al_5FeSi$ and $\alpha$-Al phases was seen to be able to separate into each formation depending on cooling rate.