• Title/Summary/Keyword: Pretreatment techniques

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An Experimental study on the bond strength according to the surface treatment of metal alloy for porcelain fused metal crown (-금속(金屬) 표면처리방법(表面處理方法)에 따른 비귀금속합금(非貴金屬合金)과 도재(陶材)와의 결합강도(結合强度)에 관(關)한 실험적(實驗的) 연구(硏究)-)

  • Chung, In-Sung
    • Journal of Technologic Dentistry
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    • v.11 no.1
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    • pp.83-88
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    • 1989
  • This investigation was performed to evaluate the effect of four different preteatment techniques on the bond strength of porcelain to non-precious metal alloy. Samples of total of 40 were divided into 4 groups according to the 4 variables which included the 50$\mu$alumina oxide air abrasion, method, the as retention bead method, the L-retention bead method, the Etching method. The completed metal-porcelain samples were compressed in Instron loading machine until gross fracture occured to examine the effect of the complex variables on the bond strength of porcelain to non precious metal alloy. The result obtained were as follows : 1. The difference of bond strength according to four different pretreatment techniques was statistically significant(p<0.01). 2. The difference of bond strength between the ss-retention bead method and the L-retention bead method was not significant statistically(p>0.05) 3. The difference of bond strength between the retention bead method and the etching method was statistically significant(p<0.01). 4. The difference of bond strength between the retention bead method and the 50$\mu$alumina oxide air abrasion method was statistically significant(p<0.01). 5. The difference of bond strength between the etching method and the 50$\mu$alumina oxide air abrasion method was statistically significant(p<0.01).

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Fault Current Discrimination of Power Line using FCM allowing self-organization (FCM에 기반한 자가생성 지도학습알고리즘을 이용한 전력선의 고장전류 판별)

  • Jeong, Jong-Won;Won, Tae-Hyun;Lee, Joon-Tark
    • Proceedings of the KIEE Conference
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    • 2011.07a
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    • pp.368-369
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    • 2011
  • This article suggests an online-based remote fault current mode discrimination method in order to identify the causes of the power line faults with various causes. For that, it refers to existing cause identification methods and categorizes modes by fault causes based on statistical techniques beforehand and performs the pretreatment process of fault currents by each cause acquired from the fault recorder into a topological plane in order to extract the characteristics of fault currents by each cause. After that, for the fault mode categorization, it discriminates modes by each cause using data by each cause as leaning data through utilizing RBF network based on FCM allowing self-organization in deciding the middle layer. And then it tests the validity of the suggested method as applying it to the data of the actual fault currents acquired from the fault recorder in the electric power transmission center.

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The Effect on HRT and Hydraulic Characteristics of Biological Activated Carbon Fluidized Bed. (생물활성탄 유동상의 수리학적 특성과 체류시간의 영향)

  • 우달식;김선일;남상호
    • Journal of environmental and Sanitary engineering
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    • v.12 no.3
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    • pp.103-109
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    • 1997
  • As the quality of raw water deteriorates, a number of additional treatment techniques have been developed and adapted to water treatment for producing a safe and aesthetically satisfactory drinking water. So, BACFB process as pretreatment in water supply is to be effective to remove dissolved organics. This study performed to find out the effects of HRT and hydraulic characteristics on BACFB reactors in water supply. The flow type in reactor was a high dispersion with complete mixing. As superficial velocity was increased, bed expansion was closed to theoretical values. It was considered that below 30 min HRT could operated to ensure the removal of dissolved organics.

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Analytical Methodology of Stable Isotopes Ratios: Sample Pretreatment, Analysis and Application (안정동위원소비 분석 기법의 이해: 시료의 전처리, 분석 및 자료의 해석과 적용)

  • Kim, Min-Seob;Hwang, Jong-Yeon;Kwon, Oh-Sang;Lee, Won-Seok
    • Korean Journal of Ecology and Environment
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    • v.46 no.4
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    • pp.471-487
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    • 2013
  • This review paper was written to provide background information as well as future application for aquatic ecologists interested in using stable isotope. Stable isotope techniques has proved to be an extremely useful to elucidate a lot of environmental and ecological problems. Stable isotopes have been used as possible tracers to identify sources, to quantify relative inputs in a system. When utilized carefully, stable isotope tools provides apparent advantages for the scientists to find out the processes of material cycles in various environments and energy flows in natural ecosystems.

Shear bond strength of a new self-adhering flowable composite resin for lithium disilicate-reinforced CAD/CAM ceramic material

  • Erdemir, Ugur;Sancakli, Hande Sar;Sancakli, Erkan;Eren, Meltem Mert;Ozel, Sevda;Yucel, Taner;Yildiz, Esra
    • The Journal of Advanced Prosthodontics
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    • v.6 no.6
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    • pp.434-443
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    • 2014
  • PURPOSE. The purpose of this study was to evaluate and compare the effects of different surface pretreatment techniques on the surface roughness and shear bond strength of a new self-adhering flowable composite resin for use with lithium disilicate-reinforced CAD/CAM ceramic material. MATERIALS AND METHODS. A total of one hundred thirty lithium disilicate CAD/CAM ceramic plates with dimensions of $6mm{\times}4mm$ and 3 mm thick were prepared. Specimens were then assigned into five groups (n=26) as follows: untreated control, coating with $30{\mu}m$ silica oxide particles ($Cojet^{TM}$ Sand), 9.6% hydrofluoric acid etching, Er:YAG laser irradiation, and grinding with a high-speed fine diamond bur. A self-adhering flowable composite resin (Vertise Flow) was applied onto the pre-treated ceramic plates using the Ultradent shear bond Teflon mold system. Surface roughness was measured by atomic force microscopy. Shear bond strength test were performed using a universal testing machine at a crosshead speed of 1 mm/min. Surface roughness data were analyzed by one-way ANOVA and the Tukey HSD tests. Shear bond strength test values were analyzed by Kruskal-Wallis and Mann-Whitney U tests at ${\alpha}=.05$. RESULTS. Hydrofluoric acid etching and grinding with high-speed fine diamond bur produced significantly higher surface roughness than the other pretreatment groups (P<.05). Hydrofluoric acid etching and silica coating yielded the highest shear bond strength values (P<.001). CONCLUSION. Self-adhering flowable composite resin used as repair composite resin exhibited very low bond strength irrespective of the surface pretreatments used.

Bioethanol Production from Macroalgal Biomass (해조류 바이오매스를 이용한 바이오에탄올 생산기술)

  • Ra, Chae Hun;Sunwoo, In Young;Kim, Sung-Koo
    • Journal of Life Science
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    • v.26 no.8
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    • pp.976-982
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    • 2016
  • Seaweed has high growth rate, low land usage, high CO2 absorption and no competition for food resources. Therefore, the use of lignin-free seaweed as a raw material is arising as a third generation biomass for bioethanol production. Various pretreatment techniques have been introduced to enhance the overall hydrolysis yield, and can be categorized into physical, chemical, biological, enzymatic or a combination. Thermal acid hydrolysis pretreatment is one of the most popular methods to attain high sugar yields from seaweed biomass for economic reasons. At thermal acid hydrolysis conditions, the 3,6-anhydro-galactose (AHG) from biomass could be converted to 5-hydroxymethylfurfural (HMF), which might inhibit the cell growth and decrease ethanol production. AHG is prone to decomposition into HMF, due to its acid-labile character, and subsequently into weak acids such as levulinic acid and formic acid. These inhibitors can retard yeast growth and reduce ethanol productivity during fermentation. Thus, the carbohydrates in seaweed require effective treatment methods to obtain a high concentration of monosaccharides and a low concentration of inhibitor HMF for ethanol fermentation. The efficiency of bioethanol production from the seaweed biomass hydrolysate is assessed by separate hydrolysis and fermentation (SHF). To improve the efficiency of the ethanol fermentation of mixed monosaccharides, the adaptation of yeast to high concentration of sugar could make simultaneous utilization of mixed monosaccharides for the production of ethanol from seaweed.

The experiment of process efficiency and salt elimination in food waste compost using triple salt (삼중염을 이용한 음식물 쓰레기 퇴비 중 염분제거 및 공정효율화 실험)

  • Kim, Nam-Cheon;Jang, Byung-Man
    • Journal of the Korea Organic Resources Recycling Association
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    • v.14 no.2
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    • pp.83-90
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    • 2006
  • The NaCl contents of food waste composts made by various techniques known up to now were under the level of 1% by fresh weight basis. But these techniques has some problem that is environment pollution from treated water and high equipment cost. The application to agricultural land of food waste compost that is not sufficiently removed NaCl was considered to be improper due to salt accumulation in soils and plant growth inhibition by salt stress. The purpose of this study is to decompose NaCl in food waste compost using triple salt and this method is differ from existing chemical method. Also, reaction of NaCl with triple salt produced KCl that is basic material of potassium fertilizer. Moreover Also, there was temperature rise of average $5^{\circ}C$ as result that apply triple salt in food waste 600 ton in food wast composting productive capacity. Obvious odious smell reduction effect appeared pretreatment process and fermentation process with temperature rise and this is because triple salt activation of aerobe and removes odious smell cause material by salt content decrease effectively.

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Treatment Characteristics of Japanese Larch Heartwood with CCA or CCFZ and Improving its CCA Treatability by Incising Techniques (낙엽송(落葉松) 심재(心材)의 CCA와 CCFZ 처리특성(處理特性) 및 자상처리(刺傷處理)에 의(依)한 CCA 처리도(處理度) 개선(改善))

  • Kang, Sung-Mo;Kim, Gyu-Hyeok;Paik, Ki-Hyon
    • Journal of the Korean Wood Science and Technology
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    • v.23 no.4
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    • pp.60-66
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    • 1995
  • The treatability of Japanese larch heartwood was assessed by pressure treatment of non-incised dimension material with CCA or CCFZ. The effectiveness of incising(conventional, high density, and needle incising) for improving CCA treatability on refractory Japanese larch heartwood was also investigated. Preservative retention and penetration were somewhat greater with CCFZ treatment, although those was generally poor in both preservatives. The retention gradients for both CCA and CCFZ-treated stock were essentially the same shape. Treatment of non-incised material with CCA acheived the recommended treatability for using treated wood at the regions of hazard class H2 in the Japanese Agricultural Standards. However, Japanese larch heartwood would require incising as a pretreatment for enhancing treatability, if CCA-treated larch is intended to be used at the regions of hazard class H3 and H4. As expected, incising resulted in a considerable improvement of preservative treatability, particularly penetration, and the effect of incising on the improvement of treatability was excellent at the sequence of needle incising, high density incising, and conventional incising. Among incising techniques investigated in this study, high density and needle incising enhanced CCA treatability beyond the point where it did meet a minimum requirements specified by the Japanese Agricultural Standards for using CCA-treated Japanese larch at the regions of hazard class H3 and even H4.

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Bioseparations in Lab-On-A-Chip (랩온어칩에서의 생물분리기술)

  • Chang Woo-Jin;Koo Yoon-Mo
    • KSBB Journal
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    • v.20 no.3
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    • pp.197-204
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    • 2005
  • Lab-on-a-chip is a miniaturized analytical device in which all of the procedures for the analysis of molecules are carried out, such as pretreatment, reaction, separation, detection, etc. Lab-on-a-chip has increasing concern as a device not only for rapid detection of molecules but also for high throughput screening and point of care, because conventional laborious and time consuming analytical procedures can be substituted. Thus, a lot of microfabrication and analytical techniques for lab-on-a-chip have been developed with microstructures smaller than a few hundreds of micrometers. Separation of the molecules is one of the most important components of lab-on-a-chip, because effective separation method can simplify the design and can provide better sensitivity. The electrokinetic separation based on capillary electrophoresis is most widely employed technique in lab-on-a-chip for the control of fluids and the separation of molecules. In this article, bioseparation techniques and its applications realized in lab-on-a-chip are reviewed.

Chemical Derivatization of Catecholamines for Gas Chromatography-Mass Spectrometry

  • Park, Sun-Young;Kang, Bo-Xin;Li, Quing;Kim, Hoon-Sik;Lee, Jun-Gae;Hong, Jong-Ki
    • Bulletin of the Korean Chemical Society
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    • v.30 no.7
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    • pp.1497-1504
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    • 2009
  • GC/MS analysis of catecholamines (CAs) in biological sample may produce poor reproducible quantitaion when chemical derivatization is used as the technique to form a volatile derivative. Significant quantities of the side products can be formed from CAs with primary amine during the derivatization reaction under un-optimized conditions. We have tested various chemical derivatization techniques in an attempt to find an optimum derivatization method that will reduce side product formation, enable to separate several catecholamine derivatives in GC chromatogram, and obtain significant improvement of detection sensitivity in GC/MS analysis. Whereas several derivatization techniques such as trimethylsilylation (TMS), trifluoroacylation (TFA), and two step derivatization methods were active, selective derivatization to form O-TMS, N-heptafluorobutylacyl (HFBA) derivative using N-methyl-N-(trimethylsilyl)-trifluoroacetamide (MSTFA) and N-methyl-bis(heptafluorobutyramide) (MBHFBA) reagents was found to be the most effective method. Moreover, this derivative formed by selective derivatization could provide sufficient sensitivity and peak separation as well as produce higher mass ion as base peak to use selected ion in SIM mode. Calibration curves based on the use of an isotopically labeled internal standard show good linearity over the range assayed, 1 ~ 5000 ng/mL, with correlation coefficients of > 0.996. The detection limits of the method ranged from 0.2 to 5.0 ppb for the different CAs studied. The developed method will be applied to the analysis of various CAs in biological sample, combined with appropriate sample pretreatment.