• 제목/요약/키워드: Pressureless infiltration

검색결과 21건 처리시간 0.02초

무가압함침법으로 제조된 입자강화 금속복합재료의 마모특성 (Wear Characteristics of Particulate Reinforced Metal Matrix Composites Fabricated by a Pressureless Metal Infiltration Process)

  • 김재동;정순억;김형진
    • 한국해양공학회지
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    • 제17권1호
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    • pp.55-60
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    • 2003
  • The effect of size and volume fraction of ceramic particles, with sliding velocity on the wear properties were investigated for the metal matrix composites fabricated by the pressureless infiltration process. The metal matrix composites exhibited about 5.5 - 6 times the wear resistance compared with AC8A alloy at high sliding velocity, and by increasing the particle size and decreasing the volume fraction, the wear resistance was improved. The wear resistance of metal matrix composites and AC8A alloy exhibited different aspects. Wear loss of AC8A alloy increased with sliding velocity, linearly : whereas, metal matrix composites indicated more wear loss than AC8A alloy at the slow velocity region. However, a transition point of wear loss was found at the middle velocity region, which shows the minimum wear loss. Further, wear loss at the high velocity region exhibited nearly the same value as the slow velocity region. In terms of wear mechanism, the metal matrix composites generally exhibited abrasive wear at slow to high sliding velocity; however, AC8A alloy showed abrasive wear at low sliding velocity and adhesive and melt wear at high sliding velocity.

알루미늄 기지 금속복합재료의 기계적 성질에 미치는 제조변수의 영향 (Effects of Processing Parameters on the Mechanical Properties of Aluminium Matrix Composites)

  • 김재동;고성위;김형진
    • 동력기계공학회지
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    • 제9권4호
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    • pp.130-136
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    • 2005
  • The effects of additional Mg content, the size and volume fraction of reinforcement phase on the mechanical properties of ceramic particle reinforced aluminium matrix composites fabricated by pressureless metal infiltration process were investigated. The hardness of $SiC_p/AC8A$ composites increased gradually with an increase in the additive Mg content, while the bending strength of $SiC_p/AC8A$ composites increased with an increase in additive Mg content up to 5%. However, this decreased when the level of additive Mg content was greater than 5% due to the formation of coarse precipitates by excessive Mg reaction and an increase in the porosity level. The hardness and strength of the composites increased with decreasing the size of SiC particle. It was found that the composites with smaller particles enhanced the interfacial bonding than those with bigger particles from fractography of the composites. The hardness of $Al_2O_{3p}/AC8A$ composites increased gradually with an increase in the volume fraction, however, the bending strength of $Al_2O_{3p}/AC8A$ composites decreased when the volume fraction of alumina particle was greater than 40% owing to the high porosity level.

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무가압함침법으로 제조된 입자강화 금속복합재료의 마모특성 (Wear Characteristics of Particulate Reinforced Metal Matrix Composites Fabricated by Pressureless Metal Infiltration Process)

  • 김재동;정순억;김형진
    • 한국해양공학회:학술대회논문집
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    • 한국해양공학회 2002년도 추계학술대회 논문집
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    • pp.379-384
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    • 2002
  • The effect of size and volume fraction of ceramic particles with sliding velocity on the wear properties were investigated for the metal matrix composites fabricated by pressureless infiltration process. The particulate metal matrix composites exhibited about 5.5 - 6 times of excellent wear resistance compared with AC8A alloy at high sliding velocity, and as increasing the particle size and decreasing the volume fraction the wear resistance was improved. The wear resistance of metal matrix composites and AC8A alloy exhibited different aspects. Wear loss of AC8A alloy increased with sliding velocity linearly. whereas metal matrix composites indicated more wear loss than AC8A alloy at slow velocity region, however a transition point of wear loss was found at middle velocity region which show the minimum wear loss, and wear loss at high velocity region exhibited nearly same value with slow velocity region. In terms of wear mechanism, the metal matrix composites exhibited the abrasive wear at slow to high sliding velocity generally, however AC8A alloy showed abrasive wear at low sliding velocity and adhesive and melt wear at high sliding velocity.

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Thermomechanical Properties of Functionally Graded $Al-SiC_p$ Composites

  • Song, Dae-Hyun;Park, Yong-Ha;Park, Yong-Ho;Park, Ik-Min;Cho, Kyung-Mox
    • 한국분말야금학회:학술대회논문집
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    • 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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    • pp.85-86
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    • 2006
  • A theoretical model is applied to the analysis of thermomechanical properties of $Al-SiC_p$ FGMs in this study. Functionally graded $Al-SiC_p$ composites ($Al-SiC_p$ FGMs) consisted with 10 layers gradually changing volume fractions of Al and $SiC_p$ were fabricated using the pressureless infiltration technique. $Al-SiC_p$ FGMs plates of total thickness of 3mm, 5mm and 7mm with fairly uniform distribution and compositional gradient of $SiC_p$ reinforcement in the Al matrix throughout the thickness was successfully fabricated. The curvature of $Al-SiC_p$ FGM plates was measured to check the internal stress distribution predicted via a theoretical model for the analysis of thermo-mechanical deformation. The evolution of curvature and also internal stresses in response to temperature variations could be predicted for the different combinations of geometric thickness of FGM plates. Theoretical prediction of thermally induced stress distribution makes it possible to design FGM structures without any critical failure during the usage of them.

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무가압 침투에 의하여 제조된 Al-5Mg-X(Si, Cu, Ti)/SiCp 복합재료의 시효 및 마멸특성에 관한 연구 (A Study on Aging and Wear Behaviors of Al-5Mg-X(Si, Cu, Ti)/SiCp Composites Fabricated by Pressureless Infiltration Method)

  • 우기도;김석원;나홍석;문호정
    • 한국주조공학회지
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    • 제20권5호
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    • pp.300-306
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    • 2000
  • The objective of this work was to investigate the effects of SiC particle size(50, 100 ${\mu}m$) and additional elements such as Si, Cu and Ti on aging behavior in Al-5Mg-X(Si,Cu,Ti)/SiCp composites fabricated by pressureless infiltration method using hardness and wear test, scanning electron microscopy(SEM) and differential scanning calorimetry(DSC). The peak aging time in Al-5Mg-X(Si, Cu, Ti)/SiCp(50, 100 ${\mu}m$) composites is shorter than Al-5Mg-0.3Si alloy.The peak aging time of 50 ${\mu}m$ SiC particle reinforced Al-5Mg-X(Si,Cu,Ti) composites is shorter than those of 100 ${\mu}m$ SiC particle reinforced of Al-5Mg-X(Si,Cu,Ti) composites. The Al-5Mg-0.3Si-0.1Cu-0.1Ti/SiCp(50 ${\mu}m$) composites aged at $180^{\circ}C$ has higher hardness and better wear resistance than any other aged composite.The aging effect is promoted by the addition of Si and Cu in Al-5Mg/SiCp composites, so the wear resistance of Al-5Mg/SiCp composites with Si and Cu elements is enhanced by the aging treatment.

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무가압함침법으로 제조한 SiCp/AC8A 복합재료의 기계적 성질 (Mechanical Properties of SiCp/AC8A Composites Fabricated by Pressureless Metal Infiltration Process)

  • 김재동;고성위;김형진
    • Composites Research
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    • 제15권3호
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    • pp.1-10
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    • 2002
  • 무가압함침법에 의해 제조된 SiCp/AC8A복합재료에 대하여 SiC 입자 크기와 부가적인 Mg의 첨가가 복합재료의 기계적 성질과 마모특성에 미치는 영향을 조사하였다. SiCp/AC8A복합재료의 경도와 굽힘강도는 입자의 크기가 작아짐에 따라 증가하였다. Mg 첨가량이 증가함에 따라 SiCP/AC8A복합재료의 경도는 경질의 반응생성물에 의해 상승하였으나 굽힘강도는 석출물의 조대화와 기공율의 증대에 의해 저하하였다. SiCp/AC8A복합재료는 AC8A 기지재에 비하여 고속의 마찰속도에서 6배의 내마모성을 나타냈으며 강화입자의 크기가 작아짐에 따라 내마모성은 향상되는 것으로 나타났다. 마모기구에 있어서 SiCp/AC8A복합재료는 마찰속도에 관계없이 연삭마모를 나타냈으나 AC8A 기지재는 마찰속도가 고속화됨에 따라 응착 및 용융마모의 마모면을 나타냈다.

Processing and properties of $Al_{2}O_{3}/SiC$ nanocomposites by polycarbosilane infiltration

  • Jung-Soo Ha;Chang-Sung Lim;Chang-Sam Kim
    • 한국결정성장학회지
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    • 제12권2호
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    • pp.80-86
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    • 2002
  • $Al_{2}O_{3}/SiC$ nanocomposites were made by infiltrating partially sintered alumina bodies with polycarbosilane (PCS) solutions, which is a SiC polymer precursor, with pressureless sintering. The SiC content, densification, phases, strength, and microstructure were investigated with the processing parameters such as PCS solution concentration and heat treatment condition for PCS pyrolysis and sintering. The results were compared with those for pure alumina and nanocomposite samples made by the existing polymer precursor route (i.e. the PCS addition process). The SiC contents of up to 1.5 vol% were obtained by the PCS infiltration. PCS pyrolysis, followed by air heat treatment, was needed before sintering to avoid a cracking problem and to attain a densification as high as 98 % of theoretical. The nanocomposites exhibited significantly higher strength than pure alumina and those prepared by the PCS addition process despite larger grain size. Besides $\alpha-Al_{2}O_{3}/SiC$ and $\beta-SiC$ phases, mullite was present a little in the nanocomposites, which resulted from the reaction of $SiO_{2}$ in the pyrolysis product of PCS with the $Al_{2}O_{3}$ matrix during sintering. The nanocomposites had intagranular particles believed to be SiC, which is a typical feature of $Al_{2}O_{3}/SiC$ nanocomposites.

무가압 분말충전 알루미나에 이트리아를 함유한 붕규산염 유리를 침투시킨 코아 도재의 물성 (THE PHYSCIAL PORPERTIES OFY Y2O3-CONTAINING GLASS INFILTRATED ALUMINA CORE MADE BY PRESSURELESS POWDER PACKING METHOD)

  • 황승우;이근우
    • 대한치과보철학회지
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    • 제35권1호
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    • pp.221-243
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    • 1997
  • The objective of this study was to characterize the mechanical properties of $Y_{2}O_{3}$-containing glass infiltrated ceramic core material, which was made by pressureless powder packing method. A pure alumina powder with a grain size of about $4{\mu}m$ was packed without pressure is silicon mold to form a bar shaped sample, and applied PVA solution as a binder. Samples were sinterd at $1350^{\circ}C$ for 1 hour. After cooling, $Y_{2}O_{3}$-containing glass($SiO_{2},\;Y_{2}O_{3},\;B_{2}O_{3},\;Al_{2}O_{3}$, ect) was infiltrated to the sinterd samples at $1300^{\circ}C$ for 2 hours and cooled. Six different proportions $Y_{2}O_{3}$ of were used to know the effect of the mismatch of the thermal expansion coefficient between alumina powder and glass. The samples were ground to $3{\times}3{\times}30$ mm size and polished with $1{\mu}m$ diamond paste. Flexural strength, fracture toughness, hardness and other physical properties were obtained, and the fractured surface was examined with SEM and EPMA. Ten samples of each group were tested and compared with In-Ceram(tm) core materials of same size made in dental laboratory. The results were as follows : 1. The flexural strengths of group 1 and 3 were significantly not different with that of In-Ceram, but other experimental groups were lower than In-Ceram. 2. The shrinkage rate of samples was 0.42% after first firing, and 0.45% after glass infiltration. Total shrinkage rate was 0.87%. 3. After first firing, porosity rate of experimental groups was 50%, compared with 22.25% of In-Ceram. After glass infiltration, porosity rate of experimental groups was 2%, and 1% in In-Ceram. 4. There was no statistical difference in hardness between two materials tested, but in fracture toughness, group 2 and 3 were higher than In-Ceram. 5. The thermal expansion coefficients of experimental groups were varied to $4.51-5.35{\times}10^{-6}/^{\circ}C$ according to glass composition, also the flexural strengths of samples were varied. 6. In a view of SEM, many microparticles about $0.5{\mu}m$ diameter and $4{\mu}m$ diameter were observed in In-Ceram. But in experimental group, the size of most particles was about $4{\mu}m$, and a little microparticles was observed. The results obtained in this study showed that the mismatch of the thermal expansion coefficients between alumina powder and infiltrated glass affect the flexural strength of alumin/glass composite. The $Y_{2}O_{3}$-containing glass infiltrated ceramic core made by powder packing method will takes less time and cost with sufficient flexural strength similar to all ceramic crown made with slip casting technique.

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Fabrication of Porous Al2O3-(m-ZrO2) Composites and Al2O3-(m-ZrO2)/PMMA Hybrid Composites by Infiltration Process

  • Lee, Byong-Taek;Quang, Do Van;Song, Ho-Yeon
    • 한국세라믹학회지
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    • 제44권6호
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    • pp.291-296
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    • 2007
  • Porous $Al_2O_3-(m-ZrO_2)$ composites were fabricated by pressureless sintering, using different volume percentages (40% - 60%) of poly methyl methacrylate (PMMA) powders as a pore-forming agent. The pore-forming agent was successfully removed, and the pore size and shape were well-controlled during the burn-out and sintering processes. The average pore size in the porous $Al_2O_3-(m-ZrO_2)$ bodies was about $200\;{\mu}m$ in diameter. The values of relative density, bending strength, hardness, and elastic modulus decreased as the PMMA content increased; i.e., in the porous body (sintered at $1500^{\circ}C$) using 55 vol % PMMA, their values were about 50.8%, 29.8 MPa, 266.4 Hv, and 6.4 GPa, respectively. To make the $Al_2O_3-(m-ZrO_2)$/polymer hybrid composites, a bioactive polymer, such as PMMA, was infiltrated into the porous $Al_2O_3-(m-ZrO_2)$ composites. After infiltration, most of the pores in the porous $Al_2O_3-(m-ZrO_2)$ composites, which were made using 60 vol % PMMA additions, were infiltrated with PMMA, and their values of relative density, bending strength, hardness, and elastic modulus remarkably increased.

BN 입자 강화 Al-5wt% Mg 기지 복합재료의 고온 크립 변형에서의 임계응력 해석 (A Study of Threshold stress during High Temperature Creep of $\textrm{BN}_f$/Al-5, wt% Mg Metal Matrix Composite)

  • 송명훈;권훈;김용석
    • 한국소성가공학회:학술대회논문집
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    • 한국소성가공학회 2000년도 춘계학술대회논문집
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    • pp.187-191
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    • 2000
  • High temperature creep behaviour of Al-5 wt% Mg alloy reinforced with 7.5% BN flakes was studied. The composite specimens showed two main creep characteristics : (1) the value of the apparent stress exponent of the composite was high and varied with applied stress (2) the apparent activation energy for creep was much larger than that for self-diffusion in aluminum The true stress exponent of the composite was set equal to 5. Temperature dependence of the threshold stress of the composite was very strong. Which could not be rationalized by allowing for the temperature dependence of the elastic modulus change. AIN particles which were incorporated into the Al matrix during fabrication of the composite by the PRIMEXTM method were found to be effective barriers to dislocation motion and to give rise the threshold stress during creep of the composite

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