• Title/Summary/Keyword: Pre-treatment process

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Study of cotton linter pre-treatment process for producing high quality regenerated fibers for fabrics (방직용 고품질 재생섬유 제조를 위한 면린터 전처리공정에 관한 연구)

  • Park, Hee Jeong;Han, Jung Su;Son, Ha Neul;Seo, Yung Bum
    • Journal of Korea Technical Association of The Pulp and Paper Industry
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    • v.45 no.3
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    • pp.27-35
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    • 2013
  • Cotton linter pre-treatment methods using electron beam and sulfuric acid were investigated to prepare high quality regenerated fibers for fabrics. So far, NaOH was used to reduce the degree of polymerization (DP) of the cotton linter for ease of dissolving by cellulose solvent. Two pre-treatment methods were developed to reduce the consumption of the chemicals (NaOH) and to control the DP of cellulose more precisely. Changes in ${\alpha}$-cellulose contents and brightness by the pre-treatments were also important concerns. Both electron beam irradiation and sulfuric acid were shown to be effective on controlling the DP of cellulose and to reduce the chemical consumption, but reduced ${\alpha}$-cellulose contents as well in this study. Sulfuric acid pre-treatment, which needed additional washing process after the pre-treatment when comparing to the electron beam irradiation method, gave the highest brightness and the highest reduction of ${\alpha}$-cellulose content.

Effects of Ultrasonic Cleaning and Chemical Pre-treatment on the Characteristics of Fast-stabilized Rayon Fabrics (빠르게 안정화된 레이온직물의 특성에 미치는 초음파세척 및 화학전처리 영향)

  • Cho, Chae Wook;Cho, Donghwan
    • Journal of Adhesion and Interface
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    • v.14 no.3
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    • pp.146-159
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    • 2013
  • In the present study, stabilized rayon fabrics were prepared from fast isothermal stabilization processes, which were carried out within four minutes at $350^{\circ}C$. The effects of ultrasonic cleaning and chemical pre-treatment on the chemical composition, physical characteristics, X-ray diffraction pattern, thermal stability and shape of the stabilized rayon fabrics were investigated extensively. In order to reduce the weight loss and thermal shrinkage of rayon fabrics occurring during the stabilization process, ultrasonic cleaning was first conducted and then chemical pre-treatments using $NH_4Cl$, $Na_3PO_4$, $H_3PO_4$, and $ZnCl_2$ were performed, respectively. The results indicated that both ultrasonic cleaning and chemical pre-treatment influenced the weight loss, thermal shrinkage, microstructure, carbon content, thermal stability and fabric shape of stabilized rayon fabrics. Also the results depended on the fast-stabilization time and the type of chemical pre-treatment agents used.

Microstructure properties of internal tin processed Nb3Sn superconducting wires with pre-heating condition (내부확산법에 의한 Nb3Sn 초전도 선재의 예비 열처리 조건에 따른 미세조직 변화)

  • 하동우;오상수;하홍수;이남진;류강식;한일용;이준석
    • Proceedings of the Korea Institute of Applied Superconductivity and Cryogenics Conference
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    • 1999.02a
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    • pp.14-17
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    • 1999
  • Four designed $Nb_{3}$Sn superconductors have been fabricated in order to investigate the effect of pre-heat treatment for internal tin process. 3 types of sub-elements and 2 types of Sn reservers were fabricated. Diffusion of Sn is better in the strand divided Sn equally than in the strand had one large Sn reserver during pre heat-treatment.

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Preparation and Adhesion Characteristics of Binary Blended Waterborne Polyurethane (이성분계 혼합 폴리우레탄 수분산체의 제조 및 접착 특성 연구)

  • Kim, Eun Ji;Park, In Kyu;Park, Jae Hyung
    • Journal of Adhesion and Interface
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    • v.19 no.1
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    • pp.5-12
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    • 2018
  • The purpose of this study is to evaluate the adhesive properties of polyurethane mixed aqueous dispersions by omitting the primer, dealing with the preparation of skins for synthetic leather with excellent adhesion by omitting the pre-treatment process. The two-component mixed polyurethane water dispersion was prepared by synthesizing an ester-based polyurethane resin (PU-T) and a carbonate-based polyurethane resin (PU-C) to obtain the final resin. As a result of measuring the peel strength of the adhesive specimens omitting the pre-treatment agent, it was confirmed that the state adhesive strength (ethylene vinyl acetate (middle): $4.2kg_f/cm$ and rubber (outsole): $4.4kg_f/cm$) there was. This makes it possible to omit the pre-treatment process which has been indispensably used in the shoe manufacturing process, thereby reducing the process time and reducing the amount of volatile organic compounds (VOCs) generated in the pre-treatment product, resulting in environmentally advantageous.

Ozone-Activated Carbon Treatment in Middle Keum River containing Ammonia-Nitrogen (암모니아성질소를 함유한 금강중류 하천수의 오존-활성탄처리)

  • Kim, Chung-Hwan;Jung, Sang-Gi;Kim, Hag-Seong
    • Journal of Korean Society on Water Environment
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    • v.18 no.4
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    • pp.355-363
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    • 2002
  • A demonstration plant was carried out to investigate the removal efficiency of $NH_3-N$ and $KMnO_4$ consumption depending on the existence of pre-chlorination for the ozonation and activated carbon process in the S water treatment plant which is located at the middle of Keum River. The averge removal efficiency of $KMnO_4$ consumption for $O_3/GAC$ processes with pre-chlorination and $O_3/BAC$ processes without pre-chlorination were 48.6% and 50% respectively. It is similar to removal effect of $KMnO_4$ consumption for GAC and BAC process depending on the existence of pre-chlorination. Otherwise, the removal of THMFP for GAC and BAC process was 58% and 68% respectively. $NH_3-N$ was not almost removed by sand filter and ozonation, but the average removal efficiency in the BAC process was about 31%. Especially, $NH_3-N$ was not almost removed by $O_3/BAC$ processes at the low temperature (below $$10^{\circ}C$$) in the winter season, $O_3/BAC$ processes have the advantage of removal of organic substance when it is compared to pre -chlorination followed by $O_3/GAC$ processes. Pre-chlorination followed by $O_3/GAC$ processes were required to remove $NH_3-N$ in the winter season because the removal of $NH_3-N$ was almost ineffective by $O_3/BAC$ process.

Demonstration of Low-carbon Pre-oxidation Technology for Algae Using Sodium Permanganate (과망간산나트륨을 활용한 조류 대응 저탄소 전산화기술 실증화 연구)

  • Junsoo, Ha;Daniel Sangdu, Hur;Chaieon, Im;Donghee, Jung;Youngseong, Lim;Jinkyong, Ju
    • Journal of Korean Society on Water Environment
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    • v.38 no.6
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    • pp.267-274
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    • 2022
  • This paper is a result of research conducted on the 800,000 m3/d capacity of A Water Treatment Plant (WTP) and 400,000 m3/d capacity of B WTP plant in operation in the Nakdong River region. We evaluated the effect of algae broom on the WTP operation based on the running data of both WTP and the data on the pre-oxidation process field test for algae control using sodium permanganate (SPM) at the B WTP. The study results showed that during the algal bloom period, the coagulant dose increased by 102% in A WTP and 58% in B WTP, respectively, and the chlorine dose also increased by 38% and 29%, respectively, which may affect Total trihalomethane (THM) production. Data such as algal populations and Chl-a, residual chlorine and THM, algal populations, and ozone dose appeared also highly correlated, confirming that algal broom affects WTP operations, including water quality and chemical dosage. As a result of the field test of B WTP, THMs appeared lower than that of the control, suggesting the possibility of the SPM pre-oxidation process as an alternative to algae-related water quality management. Furthermore, in terms of GHG emissions due to energy consumption, it was observed that the pre-oxidation process using SPM was approximately 10.8%, which is a very low ratio compared to the pre-ozonation process. Therefore, these results suggest that the SPM pre-oxidation process can be recommended as an alternative to low-carbon water purification technology.

Study on the Improvement of Adhesion between Cu Laminate and PSR (동박과 PSR간의 접합력 향상에 관한 연구)

  • 김경섭;정승부;신영의
    • Journal of Welding and Joining
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    • v.17 no.2
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    • pp.61-65
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    • 1999
  • Because of the need for packages which accommodate high pin count, high density and high speed device, PBGA(plastic ball grid array) package gets more spotlight. But the substrate material which is used for PBGA package is in nature susceptible to moisture penetration. The objective of the study is to find out the path of delamination in the stacked structure of substrate. To increase the adhesion between the cooper laminate and PSR(photo solder resist) which is the weakest part, experiments were performed by changing parameters of printing pre-treatment and post-treatment process. As a result of experiments, the factor effects on the adhesion between the cooper laminate and PSR is caused by all of the pre-treatment and post-treatment condition. A considerable change was observed depending on the amount of UV irradiation after thermal cure which is typical of printing post-treatment condition rather than pre-treatment condition.

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The Effect of Pre-Treatment Methods for the Life Time of the Insoluble Electrodes (불용성 전극의 전처리 방법이 전극의 수명에 미치는 영향)

  • Park, Mi-Jung;Lee, Taek-Soon;Kang, Meea;Han, Chi-Bok
    • Journal of Korean Society of Environmental Engineers
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    • v.38 no.6
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    • pp.291-298
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    • 2016
  • Electrochemical water treatment process as a useful treatment method for the removal of non-degradable matter has been consistently studied for several decades. Key process of electrochemical water treatment are oxidation reaction from an anode and reduction from a cathode. In this study, the effect of pre-treatment methods in the insoluble electrode manufacturing process for the water treatment has been evaluated for the life time of electrode The results of this study showed that pre-treatment methods of a base metal such as surface roughness, clean method and interlayer formation influenced to life time of electrode when the same condition (catalyst electrode layer coating method and material system) was applied for pre-treatment methods. This study was conducted by using $IrO_2/Ti$ electrode In the test of sand-blasting process, an electrode manufactured by using sanding media of different sizes resulted in the most effective electrode life time when the size of alumina was used for $212{\sim}180{\mu}m$ praticle size (#80). The most effective method was considered using arc plasma in the additional roughness control and cleaning process, sputtering method to form Ta type interlayer formation process.

A Study for Natural Dyeing Textiles with Bean-Juice Treatment Method (콩즙 처리 방법에 따른 천연염색포의 염색성 연구)

  • Park, Kyeon-Soon;Choi, In-Ryu;Bae, Kye-In
    • Journal of the Korea Fashion and Costume Design Association
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    • v.9 no.2
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    • pp.85-92
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    • 2007
  • This study focused on bean-juice treatment method which have dyeing property to indigo, yellow soil, sappan wood, cochineal and also on the possibility of applying to mordanting. This is different from the active mordanting using chemicals. Natural mordants with development of dyeing are not harmful, also are the medicines for disease. Limestone and ash neutralize the acidic soil. bean-juice protein adhere to cellulose surface and change the physical properties of protein so that coloring of dye is better than before and film non-soluble in water is made. Therefore the color made from bean-juice process lasts after washing. This study try to show one of the ways to improve the current method using the heavy metal which can have bad effects for environment and human being. Bean-juice(raw bean, heated bean) treatment method can be the way to fix the natural dyeing problem of bad dyeing. Bean-juice had been treated under various condition with pre-treatment, post-treatment and raw bean, heated bean. Following results are obtained in this study. In the case of Indigo dyeing, pre-treatment of heated bean shows the biggest difference of color. In the case of yellow soil dyeing, pre-treatment of raw bean-juice shows the biggest gap of color. Pre-treatment of heated bean in sappan wood dyeing case and post-treatment of raw bean show bigger color difference than pre-treatment of raw bean. In cochineal dyeing, raw bean pre-treatment shows the biggest color difference.

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Pre-Coagulation and Pre-Ozonation for Ozone Resisting Microfiltration Membrane Filtration System of a High Humic Contained Surface Water (고농도 휴믹성분이 포함된 강 원수에서 응집-침전 및 오존 공정을 전처리로 적용한 오존 내성막 pilot plant에서의 운전성 및 투과수 수질변화에 관한 연구)

  • Lee, Sanghyup;Yoshimasa, Watanabe;Lee, Seockheun;Ahn, Kyuhong
    • Journal of Korean Society of Water and Wastewater
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    • v.18 no.5
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    • pp.598-607
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    • 2004
  • In this study, the effects of two pre-treatment processes were observed prior to membrane filtration: pre-coagulation and pre-ozonation. To compare the effect of two above-mentioned pre-treatments, we adopted the four schemes: first one is direct membrane filtration of river surface water, second one is membrane filtration after pre-coagulation, third one is membrane filtration after pre-ozonation and fourth one is membrane filtration after pre-coagulation and pre-ozonation. There are two exceptional characteristics in applied processes. One is the usage of the MF membrane which has high ozone resisting characteristic. Therefore, ozone resides in membrane module during filtration. The other is adoption of Jet Mixed Separator (JMS) as coagulation-sedimentation process. The change in transmembrane pressure and permeate water quality were also examined. As a result, considering the filtration performance efficiency and permeate water quality, the process composed of filtration with combination of both pre-coagulation and pre-ozonation was proved most effective. The improved efficiency was due to the reduction of loading rate of fouling inducing materials to membrane module by coagulation process as well as variable reactions, such as degradation, particle destabilization and coagulation, occurred by residual ozone in membrane module. The additional effect of pre-coagulation before pre-ozonation is suppression of AOC, one of the by-products induced by ozonation. Therefore, combination of pre-coagulation and pre-ozonation is the effective process to overcome the major de-merit of ozonation i.e. by-products formation.