• Title/Summary/Keyword: Powders

Search Result 4,724, Processing Time 0.028 seconds

Photocatalayst and Decomposition Properties of TiO2 and TiO2-CdS Powders Prepared by Supercritical Fluid Method (초임계 유체법으로 제조한 TiO2 및 TiO2-CdS계 광촉매의 분해물성 연구)

  • 전일수;황수현;박상준;길현식;조승범;전명석;임대영
    • Journal of the Korean Ceramic Society
    • /
    • v.41 no.6
    • /
    • pp.481-484
    • /
    • 2004
  • TiO$_2$ and TiO$_2$-CdS powders which were expected to be highly activated photocatalysts were prepared using supercritical fluid method (SCF). The prepared photocatalyst TiO$_2$ powders were crystalline of anatase and ultrafine spherical powders with large specific surface area. When photodecompositoion reaction was done with TiO$_2$ powders prepared by SCF as a photocatalyst in DCA (Dichloroactic Acid) solution, a hazardous organic compound, the photocatlyst, properties of TiO$_2$ powders prepared by SCF were better than that of commercial TiO$_2$ powders.

Synthesis and properties of $Al_2O_3-SiC$ Composites from Alkoxides III. Effect of Composite Powder Type on the Sintering Characteristics and Properties of $Al_2O_3-SiC$ Comopsites (알콕사이드로부터 $Al_2O_3-SiC$ 복합재료의 제조 및 특성 III. 복합분말의 형태에 따른 $Al_2O_3-SiC$ 복합재료의 소결 특성 및 물성)

  • 이홍림;김규영
    • Journal of the Korean Ceramic Society
    • /
    • v.30 no.4
    • /
    • pp.316-324
    • /
    • 1993
  • Three types of dispersed, coated and mechanically mixed SiC reinforced Al2O3 composite powders were used to investigate the effect of composite powder type on sintering characteristics and properties of Al2O3-SiC composites. Sinterability of coated type composite powders was superior to that of other composite powders when they were pressureless sintered at 1500~1$700^{\circ}C$ for 2h in Ar atmosphere. However, sinterabilities (>98% TD) of each type of composite powders were similar when they were hot pressed at 180$0^{\circ}C$ for 1h under 30MPa in N2 atmosphere. SiC powders were randomly distributed in the specimen prepared from dispersed type composite powders, whereas homogeneously distributed for coated type specimens. It was found that SiC powders inhibited the grain growth of Al2O3, and fracture toughness was increased by the increment of crack growth resistance due to residual stress by secondary SiC particles within Al2O3 grains.

  • PDF

Effects of Added Yam Powders on the Quality Characteristics of Yeast Leavened Pan Breads Made from Imported Wheat flour and Korean Wheat Flour (마(Dioscorea) 첨가가 우리밀과 수입밀을 이용한 식빵 품질특성에 미치는 효과)

  • 이선영;김창순
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.30 no.1
    • /
    • pp.56-63
    • /
    • 2001
  • This study investigated the quality characteristics of yeast breads with addition of hot air-dried yam powder (HDYP) and freeze-dried yam powder (FDYP), using several physical and sensory examinations. Breads were made of imported wheat flour (IWF) or Korean wheat flour (KWF). HDPY and FDYP were added to the bread formula at three levels of 3, 5, and 7%. The addition of yam powders required an increase of water absorption. As the addition of HDYP/FDYP increased, IWF dough stickiness increased and thus handling property became inferior to the control. Especially, handling property of KWF bread dough containing FDYP was most poor among the dough samples. With HDYP/FDYP, final volumes of bread made from IWF were similar to the control when 3~5% HDYPs were added whereas loaf volumes decreased significantly as the amount of added FDYP increased, indicating volume depressing effect. In bread scoring, texture scores increased when yam powders were added that hardness, chewiness, cohesiveness and guminess of KWF bread increased as the amounts of yam powders increased. The "L" value of IWF bread crumb decreased with the addition of yam powders. From sensory evaluation using acceptability scores, the results gave us that appearance, grain, texture, flavor, taste and overall acceptability of KWF bread could be more improved with the addition of yam powders than those of IWF bread.IWF bread.

  • PDF

A Study on Characteristics of Al-Pb Strips and Its Sintering Behavior (Al-Pb계 합금분말의 성형 및 소결 특성에 관한 연구)

  • Moon, Jong-Tai;Lee, Young-Kun;Lee, Yong-Ho;Cho, Sung-Suk
    • Journal of Korea Foundry Society
    • /
    • v.10 no.5
    • /
    • pp.435-443
    • /
    • 1990
  • By using the centrifugal atomization, which is one of the rapid solidification processes, Al-5,10wt%Pb alloys which are monotectic alloys were melted at 150K over two liquid phase line in the phase diagram. The melted alloy was poured on the rotating disk, being made into atomized powders, and then the solidified microstructure and morphology of the powder were investigated. This study converted the produced powders into strips by strained powder rolling. According to sintering temperature, the microstructure and hardness were investigated. The solidified structure of the powders were almost cellular dendritic structure. Pb particles ($2.0-3.0{\mu}m$) were fairl distributed in the Al matrix. Powder shapes were irregular. Rolling property and the compacting was good, respectively, because of increasing mechanical interlocking and surface area in the small size powders. With increasing temperature, the boundarys of powders were in porous form due to the diffusion. Pb particles which were surrounding the pores were inverse-segregated at the surface of the powders. With increasing of sintering temperature, the hardness of the powders and the strips decreased. In particular rolling-strip, the hardness abruptly decreased due to the release of work-hardening.

  • PDF

Sintering Characteristics of Nickel Powders for Internal Electrode of Multilayer Ceramic Capacitors (적층 세라믹 콘덴서의 내부전극용 니켈 분말의 소결 특성)

  • Lee, Sang-Geun;Choi, Eun-Young;Lee, Yoon-Bok;Park, Suong-Soo;Park, Hee-Chan;Kim, Kwang-Ho
    • Korean Journal of Materials Research
    • /
    • v.13 no.12
    • /
    • pp.779-784
    • /
    • 2003
  • Nickel powders were obtained by various preparation methods, and their sintering characteristics were investigated. Nickel powders made by wet chemical process (WCP) had a higher surface area and more narrow size distribution than that of chemical vapor deposition (CVD) method. Nickel-oxide powders by the WCP method were prepared at $200^{\circ}C$ for 3 hr. The oxidation behaviour of nickel-oxide powder is similar with that of the CVD method. Nickel powders made by the WCP method showed a higher shrinkage in the range of $600^{\circ}C$$900^{\circ}C$ than that of commercial powder made by the CVD method. The similar results were observed on the surface microstructure of sintered bodies by SEM measurements.

Spheroidization of Enamel Powders by Radio Frequency Plasma Treatment and Application to Additive Manufacturing (RF 플라즈마 처리를 이용한 칠보 유약 분말의 구상화 및 적층 제조 공정 적용)

  • Kim, Ki-Bong;Yang, Dong-Yeol;Kim, Yong-Jin;Choe, Jungho;Kwak, Ji-Na;Jung, Woo-Hyung
    • Journal of Powder Materials
    • /
    • v.27 no.5
    • /
    • pp.388-393
    • /
    • 2020
  • The enamel powders used traditionally in Korea are produced by a ball-milling process. Because of their irregular shapes, enamel powders exhibit poor flowability. Therefore, polygonal enamel powders are only used for handmade cloisonné crafts. In order to industrialize or automate the process of cloisonné crafts, it is essential to control the size and shape of the powder. In this study, the flowability of the enamel powders was improved using the spheroidization process, which employs the RF plasma treatment. In addition, a simple grid structure and logo were successfully produced using the additive manufacturing process (powder bed fusion), which utilizes spherical enamel powders. The additive manufacturing technology of spherical enamel powders is expected to be widely used in the field of cloisonné crafting in the future.

Synthesis and Photocatalytic Activity of TiO2-ZrO2 Nano-Sized Powders by Sol-Gel Process

  • Han, Jae-Kil;Saito Fumio;Park, Jong-Gu;Lee, Byong-Taek
    • Journal of the Korean Ceramic Society
    • /
    • v.42 no.1
    • /
    • pp.7-10
    • /
    • 2005
  • [ $TiO_{2}-ZrO_{2}$ ] powders were successfully synthesized by the sol-gel process using titanium iso-propoxide as a precursor. The amorphous $TiO_{2}$ particles, 70 nm in size, homogenously adhered to the surface of $ZrO_{2}$ the powders. After calcination at $450^{circ}C$, most of the $TiO_{2}$ powders appeared as an anatase type, whereas they changed to a rutile phase at $750^{circ}C$. For comparison of photocata­lytic activity, $TiO_{2}-ZrO_{2}$ nano-sized powders calcined at $450^{circ}C,\;600^{circ}C,\;and\;750^{circ}C$ were used. In the $TiO_{2}-20wt\%$ $ZrO_{2}$ powders cal­cined at $450^{circ}C$, there was excellent removal efficiency of Methyl Orange (MO). For the calcination temperature increased, $TiO_{2}­ZrO_{2}$ nano-sized powders increased $ZrO_{2}$ contents showed the good photoactivity for the photooxidation of MO.

Production and Properties of Amorphous TiCuNi Powders by Mechanical Alloying and Spark Plasma Sintering

  • Kim, J.C.;Kang, E.H.;Kwon, Y.S.;Kim, J.S.;Chang, Si-Young
    • Journal of Powder Materials
    • /
    • v.17 no.1
    • /
    • pp.36-43
    • /
    • 2010
  • In present work, amorphous TiCuNi powders were fabricated by mechanical alloying process. Amorphization and crystallization behaviors of the TiCuNi powders during high-energy ball milling and subsequent microstructure changes were studied by X-ray diffraction and transmission electron microscope. TEM samples were prepared by the focused ion beam technique. The morphology of powders prepared with different milling times was observed by field-emission scanning electron microscope and optical microscope. The powders developed a fine, layered, homogeneous structure with milling times. The crystallization behavior showed that glass transition, $T_g$, onset crystallization, $T_x$, and super cooled liquid range ${\Delta}T=T_x-T_g$ were 628, 755 and 127K, respectively. The as-prepared amorphous TiCuNi powders were consolidated by spark plasma sintering process. Full densified TiCuNi samples were successfully produced by the spark plasma sintering process. Crystallization of the MA powders happened during sintering at 733K.

Physicochemical Characteristic of Concentrate Prepared by Puffer Muscle and Skin (복어 육과 껍질 농축물의 이화학적 특성에 관한 연구)

  • Kim, Rae-Young;Sung, Nak-Ju;Kim, Won-Tae;Park, Jae-Hee;Kim, Youn-Ju;Ju, Jong-Chan
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.39 no.2
    • /
    • pp.267-273
    • /
    • 2010
  • The objective of this study was about physicochemical characteristic of puffer muscle and skin to promote the utilization of puffer as fish protein. In proximate composition, crude protein of dried puffer muscle and skin powders were 89.5% and 82.7%, respectively. Skin powders had higher lipid contents than muscle powders. Ash contents of muscle powders were higher than those of skin powders. In nucleotides and their related compounds, the contents of nucleotides were in order of IMP and ADP. The contents of saturated fatty acid in puffer muscle (83.9%) was higher than skin powders (66.3%). Oleic acid, mono-unsaturated fatty acid, in skin powder (25.9%) was higher than in muscle powders. Seventeen kinds of composition amino acids were detected in muscle powders, while 16 kinds of amino acids were found in skin powders. Total contents of amino acid in muscle powders (83,739 mg/100 g) were higher than those of skin powders (75,361 mg/100 g). In the muscle powders of puffer, glutamic acid was the highest amino acid with the concentration of 13,707 mg/100 g, and was in order of aspartic acid, lysine, leucine, arginine, alanine, valine and glycine. In skin powders, glutamic acid was the highest content with 14,843 mg/100 g followed by proline, alanine and arginine. Twenty five kinds of free amino acids were detected in dried muscle powders, while 22 kinds of free amino acids were found in dried skin powders. Taurine of dried puffer muscle and skin powders was the highest free amino acid with the concentration of 554.4 mg/100 g and 153.6 mg/100 g, respectively. The contents of total free amino acids of dried muscle powders were higher than those of dried skin powders. Especially, cysteine was only detected in dried muscle with the content of $159.3\pm1.8$ mg/100 g.

Synthesis of Sinter-active $Y_2O_3$ Powders Using Urea (요소를 이용한 활성 이트리아 분말의 합성)

  • 한주환
    • Journal of the Korean Ceramic Society
    • /
    • v.34 no.12
    • /
    • pp.1247-1253
    • /
    • 1997
  • Sinter-active yttria powders were prepared by a solution precipitation with using a self-decomposing precipitation agent NH2CONH2(urea). The cold-pressed powders can be sintered to full density and the microstructure of grains less than 200 nm at a temperature as low as 120$0^{\circ}C$. The activity of the yttria powder has been controlled by varying nucleation conditions during precipitation and by minimizing formation of aggregates. The type of precursor is decisive in preparation of a sinter-active oxide powder, and urea is desirable as a precipitation agent for an active yttrium oxide powder.

  • PDF