• Title/Summary/Keyword: Powder consolidation

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Consolidation of Bulk Metallic Glass Composites

  • Lee, Jin-Kyu;Kim, Hwi-Jun;Kim, Taek-Soo;Shin, Seung-Yong;Bae, Jung-Chan
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.848-849
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    • 2006
  • Bulk metallic glass (BMG) composites combining a $Cu_{54}Ni_6Zr_{22}Ti_{18}$ matrix with brass powders or $Zr_{62}A_{l8}Ni_{13}Cu_{17}$ metallic glass powders were fabricated by spark plasma sintering. The brass powders and Zr-based metallic glass powders added for the enhancement of plasticity are well distributed homogeneously in the Cu-based metallic glass matrix after consolidation. The BMG composites show macroscopic plasticity after yielding, and the plastic strain increased to around 2% without a decrease in strength for the composite material containing 20 vol% Zr-based amorphous powders. The proper combination of strength and plasticity in the BMG composites was obtained by introducing a second phase in the metallic glass matrix.

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Mechanical Properties of Carbon Nanotube/Cu Nanocomposites Produced by Powder Equal Channel Angular Pressing (분말 ECAP 공정으로 제조된 탄소나노튜브/Cu 나노복합재료의 기계적 성질)

  • Yoon, Seung-Chae;Jeong, Young-Gi;Kim, Hyoung-Seop
    • Transactions of Materials Processing
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    • v.15 no.5 s.86
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    • pp.360-365
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    • 2006
  • Carbon nanotubes (CNTs) have been the subject of intensive studies for applications in the fields of nano technologies in recent years due to their superior mechanical, electric, optical and electronic properties. Because of their exceptionally small diameters (${\appros}\;several\;nm$) as well as their high Young's modulus (${\appros}1\;TPa$), tensile strength (${\appros}\;200\;GPa$) and high elongation (10-30%) in addition to a high chemical stability, CNTs are attractive reinforcement materials for light weight and high strength metal matrix composites. Although extensive researches have been performed on the electrical, mechanical and functional properties of CNTs, there are not many successful results on the mechanical properties of CNT dispersed nanocomposites. In this paper, we applied equal channel angular pressing for consolidation of CNT/Cu powder mixtures. We also investigated the hardness and microstructures of CNT/Cu nanocomposites used experimental for metal matrix composites.

Synthesis of Ni-based Bulk Metallic Glass Composites (Ni계 벌크 비정질 복합재의 제조)

  • Lee, Jin-Kyu
    • Journal of Powder Materials
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    • v.15 no.4
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    • pp.297-301
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    • 2008
  • The Ni-based bulk metallic glass matrix composites were fabricated by spark plasma sintering of mixture of gas-atomized metallic glass powders and ductile brass powders. The successful consolidation of metallic glass matrix composite was achieved by strong bonding between metallic glass powders due to viscous flow deformation and lower stress of ductile brass powders in the supercooled liquid state during spark plasma sintering. The composite shows some macroscopic plasticity after yielding, which was obtained by introducing a ductile second brass phase in the Ni-based metallic glass matrix.

Microstructure and Mechanical Properties of P/M Processed 2XXX Al-${SiC}_{p}$ Composites (분말야금방법으로 제조된 2XXX Al-${SiC}_{p}$ 복합재료의 미세조직과 기계적 성질)

  • 심기삼
    • Journal of Powder Materials
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    • v.4 no.1
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    • pp.26-41
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    • 1997
  • The powder metallurgy (P/M) processed 2009 and 2124 Al composites reinforced with SiC particulates were studied by focusing on the effect of consolidation temperature on the microstructural and mechanical Properties. The mechanical properties such as tensile properties and microhardness of the second phases were analysed in relation to the microstructures observed by a SEM and an optical microscope. The in situ fracture process study using SEM showed that the grain refinement and the removal of manganese-containing particles often observed in the 2124 Al-${SiC}_{p}$ composites were important for the improvement of the mechanical properties. This study offers an optimum consolidation temperature for the control of the manganese-containing particles in the 2124 Al-${SiC}_{p}$ composites that yields mechanical properties higher than those of the 2009 Al-${SiC}_{p}$ composites.

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Fabrication of Metallic Glass/metallic Glass Composites by Spark Plasma Sintering (방전플라즈마 소결법에 의한 비정질/비정질 복합재의 제조)

  • Lee, Jin-Kyu
    • Journal of Powder Materials
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    • v.14 no.6
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    • pp.405-409
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    • 2007
  • The Cu-based bulk metallic glass (BMG) composites containing Zr-based metallic glass phase have been consolidated by spark plasma sintering using the mixture of Cu-based and Zr-based metallic glass powders in their overlapped supercooled liquid region. The Zr-based metallic glass phases are well distributed homogeneously in the Cu-based metallic glass matrix after consolidation process. The successful consolidation of BMG composites with dual amorphous phases was corresponding to the sound viscous flow of the two kinds of metallic glass powders in their overlapped supercooled liquid region.

The Effect of Pre-compaction on Density and Mechanical Properties of Magnetic Pulsed and Sintered $Al_2O_3$ Bulk

  • Hong, S.J.;Lee, J.K.;Lee, M.K.;Kim, W.W.;Rhee, C.K.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.967-968
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    • 2006
  • This research reports for the successful consolidation of $Al_2O_3$ powder with retained ultra-fine structure using MPC and sintering. Measurements in the consolidated $Al_2O_3$ bulk indicated that hardness, fracture toughenss, and breakdown voltage have been much improved relative to the conventional polycrystalline materials. Finally, optimization of the compaction parameters and sintering conditions will lead to the consolidation of $Al_2O_3$ nanopowder with higher density and even further enhanced mechanical properties.

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Mg-Y-Cu Bulk Metallic Glass Obtained by Mechanical Alloying and Powder Consolidation

  • Lee, P.Y.;Hsu, C.F.;Wang, C.C.
    • Proceedings of the Korean Powder Metallurgy Institute Conference
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    • 2006.09b
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    • pp.950-951
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    • 2006
  • [ $Mg_{55}Y_{15}Cu_{30}$ ] metallic glass powders were prepared by the mechanical alloying of pure Mg, Y, and Cu after 10 h of milling. The thermal stability of these $Mg_{55}Y_{15}Cu_{30}$ amorphous powders was investigated using the differential scanning calorimeter (DSC). $T_g$, $T_x$, and ${\Delta}T_x$ are 442 K, 478 K, and 36 K, respectively. The as-milled $Mg_{55}Y_{15}Cu_{30}$ powders were then consolidated by vacuum hot pressing into disk compacts with a diameter and thickness of 10 mm and 1 mm, respectively. This yielded bulk $Mg_{55}Y_{15}Cu_{30}$ metallic glass with nanocrystalline precipitates homogeneously embedded in a highly dense glassy matrix. The pressure applied during consolidation can enhance thermal stability and prolong the existence of amorphous phase within $Mg_{55}Y_{15}Cu_{30}$ powders.

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Binderless Consolidation of Fine Poly-Si Powders for the Application as Photovoltaic Feedstock (태양전지(太陽電池) 원재료(原材料)로 사용(使用)하기 위한 폴리실리콘 미세분말(微細粉末)의 무점결제(無粘結劑) 성형(成形))

  • Shin, Je-Sik;Kim, Dae-Suk;Kim, Ki-Young;Shon, In-Jin;Moon, Byung-Moon
    • Resources Recycling
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    • v.18 no.1
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    • pp.38-43
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    • 2009
  • In this study, binderless consolidation processes of ultra foe Si powder, by-products of making high purity poly-Si in the current method, were systematically investigated for use as economical solar-grade feedstock. The average diameter of the silicon powder was $7.8{\mu}m$. The main contaminants of the fine silicon powder were $SiO_2$ type oxide and humidity. The chemical pretreatment using the HF solution was observed to be effective for the improvement of the compactability of the silicon powder and the density ratio and the strength of the silicon powder compacts. The yield of the binder-free consolidation process increased by 20% under a vacuum condition. In as-received state, the silicon powder were not pure enough to be used as solar grade feed-stock material. After the dry chemical treatments, a sufficiently high purity above solar-grade was able to be achieved.