• Title/Summary/Keyword: Powder blending

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Study on Mixing Characteristic and Rheology of Polymer/Graphite Composites for a Bipolar Plate of Polymer Electrolyte Membrane Fuel Cell (고분자 전해질막 수소 연료 전지 분리판 용 고분자/흑연 복합 재료의 혼합 및 유변학적 특성에 관한 연구)

  • Yoo, Tae-Hyun;Kim, Dong-Hak;Son, Young-Gon
    • Journal of the Korea Academia-Industrial cooperation Society
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    • v.12 no.10
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    • pp.4673-4678
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    • 2011
  • In this paper, studies on a mixing characteristic and viscosity measurement of polymer/graphite composites for a bipolar plate of the polymer electrolyte membrane fuel cell were presented. Since the materials for the bipolar plate should be electrically conductive, contents of solid graphite in the composite are very high. As a consequence, a viscosity of the polymer/graphite composite used for the bipolar plate is very high and the measurement of the viscosity is difficult. Viscosity measurements of the polymer/graphite composites were not possible because pressure drops were continuously fluctuated during the viscosity measurements when a conventional capillary die was used. After the die design was optimized, the steady state pressure drop could be achieved, but the viscosity thus measured was not reproducible. After many trials with different experimental techniques, it was found that melt blending of the grinded powder mixtures of both PET and graphite provides reproducible viscosity measurements and electric conductivities of the polymer/graphite composites.

Comparing the Effect of Three Processing Methods for Modification of Filament Yarns with Inorganic Nanocomposite Filler and their Bioactivity against Staphylococcus aureus

  • Dastjerdi, Roya;Mojtahedi, M.R.M.;Shoshtari, A.M.
    • Macromolecular Research
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    • v.17 no.6
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    • pp.378-387
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    • 2009
  • This research compared three methods for producing and processing nanocomposite polypropylene filament yarns with permanent antimicrobial efficiency. The three methods used to mix antimicrobial agents based on silver nano particles with PP were as follows: 1) mixing of PP powder and inorganic nanocomposite filler with the appropriate concentration using a twin-screw extruder and preparing granules, 2) method 1 with a singlerather than twin-screw extruder, and 3) producing the masterbatch by a twin-screw extruder and blending it with PP in the melt spinning process. All pure polypropylene samples and other combined samples had an acceptable spinnability at the spinning temperature of $240^{\circ}C$ and take-up speed of 2,000 m/min. After producing as-spun filament yarns by a pilot plant, melt spinning machine, the samples were drawn, textured and finally weft knitted. The physical and structural properties (e.g., linear density, tenacity, breaking elongation, initial modulus, rupture work, shrinkage and crystallinity) of the as-spun and drawn yarns with constant and variable draw ratios (the variable draw ratio was used to gain a constant breaking elongation of 50%) were investigated and compared, while DSC, SEM and FTIR techniques were used to characterize the samples. Finally, the antibacterial efficiency of the knitted samples was evaluated. The experimental results revealed that the crystallinity reduction of the as-spun yarn obtained from method 1 (5%) was more than that of method 2 (3%), while the crystallinity of the modified as-spun yarns obtained with method 3 remained unchanged compared to pure yarn. However, the drawing procedure compensated for this difference. By applying methods 2 and 3, the drawing generally improved the tenacity and modulus of the modified fibers, whereas method 1 degraded the constant draw ratio. Although the biostatic efficiency of the nanocomposite yarns was excellent with all three methods, the modified fabrics obtained from methods 1 and 2 showed a higher bioactivity.

Characterization of Ni/YSZ Anode Coating for Solid Oxide Fuel Cells by Atmospheric Plasma Spray Method (고체산화물 연료전지를 위한 플라즈마 용사코팅 Ni/YSZ 음극 복합체의 특성평가)

  • Park, Soo-Dong;Yoon, Sang-Hoon;Kang, Ki-Cheol;Lee, Chang-Hee
    • Journal of Welding and Joining
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    • v.26 no.4
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    • pp.50-54
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    • 2008
  • In this research, anode for SOFC has been manufactured from two different kinds of feedstock materials through thermal spraying process and the properties of the coatings were characterized and compared. One kind of feedstock was manufactured from spray drying method which includes nano-components of NiO, YSZ (300 nm) and graphite. And the other is manufactured by blending the micron size NiO coated graphite, YSZ and graphite powders as feedstock materials. Microstructure, mechanical properties and electrical conductivity of the coatings as-sprayed, after oxidation and after hydrogen reduction containing nano composite which is prepared from spray-dried powders were evaluated and compared with the same properties of the coatings prepared from blended powder feedstock. The coatings prepared from the spray dried powders has better properties as they provide larger triple phase boundaries for hydrogen oxidation reaction and is expected to have lower polarization loss for SOFC anode applications than that of the coatings prepared from blended feedstock. A maximum electrical conductivity of 651 S/cm at $800^{\circ}C$ was achieved for the coatings from spray dried powders which much more than that of the average value.

Microbial Community Structure of Korean Cabbage Kimchi and Ingredients with Denaturing Gradient Gel Electrophoresis

  • Hong, Sung Wook;Choi, Yun-Jeong;Lee, Hae-Won;Yang, Ji-Hee;Lee, Mi-Ai
    • Journal of Microbiology and Biotechnology
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    • v.26 no.6
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    • pp.1057-1062
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    • 2016
  • Kimchi is a traditional Korean fermented vegetable food, the production of which involves brining of Korean cabbage, blending with various other ingredients (red pepper powder, garlic, ginger, salt-pickled seafood, etc.), and fermentation. Recently, kimchi has also become popular in the Western world because of its unique taste and beneficial properties such as antioxidant and antimutagenic activities, which are derived from the various raw materials and secondary metabolites of the fermentative microorganisms used during production. Despite these useful activities, analysis of the microbial community present in kimchi has received relatively little attention. The objective of this study was to evaluate the bacterial community structure from the raw materials, additives, and final kimchi product using the culture-independent method. Specifically, polymerase chain reaction-denaturing gradient gel electrophoresis (PCR-DGGE) was used to analyze the 16S rRNA partial sequences of the microflora. One primer set for bacteria, 341FGC-518R, reliably produced amplicons from kimchi and its raw materials, and these bands were clearly separated on a 35-65% denaturing gradient gel. Overall, 117 16S rRNA fragments were identified by PCR-DGGE analysis. Pediococcus pentosaceus, Leuconostoc citreum, Leuconostoc gelidum, and Leuconostoc mesenteroides were the dominant bacteria in kimchi. The other strains identified were Tetragenococcus, Pseudomonas, Weissella, and uncultured bacterium. Comprehensive analysis of these microorganisms could provide a more detailed understanding of the biologically active components of kimchi and help improve its quality. PCR-DGGE analysis can be successfully applied to a fermented food to detect unculturable or other species.

Bio-applicable Ti-based Composites with Reduced Image Distortion Under High Magnetic Field (높은 자장하에서 자기공명 영상 왜곡이 완화된 생체용 Ti 복합재료)

  • Kim, Sung-Chul;Kim, Yu-Chan;Seok, Hyun-Kwang;Yang, Seok-Jo;Shon, In-Jin;Lee, Kang-Sik;Lee, Jae-Chul
    • Korean Journal of Metals and Materials
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    • v.50 no.5
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    • pp.401-406
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    • 2012
  • When viewed using a magnetic resonance imaging (MRI) system, invasive materials inside the human body, in many cases, severely distort the MR image of human tissues. The degree of the MR image distortion increases in proportion not only to the difference in the susceptibility between the invasive material and the human tissue, but also to the intensity of the magnetic field induced by the MRI system. In this study, by blending paramagnetic Ti particles with diamagnetic graphite, we synthesized $Ti_{100-x}C_x$ composites that can reduce the artifact in the MR image under the high-strength magnetic field. Of the developed composites, $Ti_{70}C_{30}$ showed the magnetic susceptibility of ${\chi}=67.6{\times}10^{-6}$, which corresponds to 30% of those of commercially available Ti alloys, the lowest reported in the literature. The level of the MR image distortion in the vicinity of the $Ti_{70}C_{30}$ composite insert was nearly negligible even under the high magnetic field of 4.7 T. In this paper, we reported on a methodology of designing new structural materials for bio-applications, their synthesis, experimental confirmation and measurement of MR images.

Optimal Mix Design of High-Performance, Low-Heat Self-Compacting Concrete (고성능 저발열 자기충전 콘크리트의 최적 배합설계)

  • Kim, Young-Bong;Lee, Jun-Hae;Park, Dong-Cheon
    • Journal of the Korea Institute of Building Construction
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    • v.22 no.4
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    • pp.337-345
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    • 2022
  • The foundation of high-rise concrete building in coastal areas generally must be installed in an integrated manner, not separately, in order to prevent defects caused by stress on the upper and lower parts of the mounting surface and to manage the process smoothly. However, when performing integrated punching, there is a concern that temperature stress cracks may occur due to hydration heat. Due to the large member size, it is difficult to make a sufficient commitment, so it is necessary to mix concrete with high self-charging properties to ensure workability. In this research, the amount of high-performance spray and admixture used was adjusted as experimental variables to satisfy this required performance. Through the analysis of the results for each blending variable, it was found that the unit quantity was 155kg/m3 and the cement ratio in the binder was 18%, and the target values of the pre-concrete properties and compressive strength were satisfied. A four-component binder(18% cement, 50% slag fine powder, 27% fly ash, 5% silica fume) was used.

Quality of Mozzarella Cheese Analogues Prepared from Soy Milk with WP, WPC 34, WPC 80, DWP, or LP during the Storage Period (다양한 유청제품인 WP, WPC 34, WPC 80, DWP, LP를 Soymilk에 첨가하여 제조된 Mozzarella Cheese Analogue의 저장 중 품질 변화에 관한 연구)

  • Jin, Woo-Seung;Song, Kwang-Young;Seo, Kun-Ho;Yoon, Yoh-Chang
    • Journal of Dairy Science and Biotechnology
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    • v.31 no.1
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    • pp.35-49
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    • 2013
  • The purpose of this study was to develop Mozzarella cheese analogues by using dairy products in the form of WPC 34, WPC 80, whey protein, demineralized whey powder, and lactose powder along with soy milk. Soy milk was separately blended with 5% WPC 34 (A), WPC 80 (B), DWP (C), WP (D), and LP (E) and also with 10% WPC 34 (F), WPC 80 (G), DWP (H), WP (I), and LP (J). Blending of soy milk and whey products showed that increase in the proportions of whey products (WPC 34, WPC 80, DWP, WP, and LP) led to increase in the protein, lactose, and SNF levels of the admixture. A decrease in fat content was observed for all cheeses prepared from mixtures, relative to those for the control cheese. The nitrogen content within analogue samples was higher than that in the control cheese and increased with increase in the proportions of whey products within soy milk. Higher water soluble nitrogen levels were observed in cheese prepared from whey-product-blended soy milk than in the control cheese. The non-protein nitrogen level within the control Mozzarella cheese was significantly lower than that in the Mozzarella analogues, and, in the case of cheese analogues, it increased with increase in the proportion of whey products in soy milk. With regard to the physicochemical and sensory qualities of the Mozzarella cheese analogues and control cheese, the pH of all analogue samples, with the exception of the cheese prepared from group G, was lower than that of the control Mozzarella cheese. Rheological studies showed that the hardness of Mozzarella cheese analogues was lower than that of the control Mozzarella, while the elasticity, cohesiveness, and brittleness of the analogues was higher. The control sample had a higher meltability level than any of the Mozzarella analogues. Mozzarella cheese prepared with the traditional method had higher browning and stretching levels than all the cheese analogues, but a lower oiling-off level.

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Preparation and Characterization of Biomass-based Polymer Blend Films(2) (Biomass-based 고분자 블렌드 필름의 제조 및 특성 연구(2))

  • Lee, Soo;Park, Myung-Ho
    • Journal of the Korean Applied Science and Technology
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    • v.30 no.2
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    • pp.305-311
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    • 2013
  • PLA(polylactic acid), one of biodegradable polymers was blended with various amounts of wood pulp powder through solution blending technic to verify the effect of reinforcing pulp amount on the mechanical properties of blend films. Also these blend films were further modified with TDI(toluene diisocyanate) as crosslinking agent to introduce urethane functions by reaction of pulp hydroxyl groups and isocyanate. As a result, the tensile strength of blend film with 0.25 wt% pulp was increased from $565.25kg_f/cm^2$ for PLA film itself to $624.20kg_f/cm^2$. However, elongation of this film was decreased by 50% of that of PLA film itself. Only PLA/pulp blend film further modified with 500% of TDI/0.25 wt% pulp showed the slightly increased tensile strength but decreased elongation. Melting point and glass transition temperature of PLA/pulp blend films were confirmed by using Differential Scanning Calorimeter(DSC). Thermal stability of these blend films measured by TGA showed only a slight increase at temperature lower than $300^{\circ}C$.

Study on Optimum Mixture of Industrial By-Products for Lightweight Foamed Filler Production by Mixture Experimental Design (혼합물 실험계획법에 의한 경량기포 충전재 제조를 위한 산업부산물의 최적 배합 검토)

  • Woo, Yang-Yi;Park, Keun-Bae
    • Journal of the Korean Recycled Construction Resources Institute
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    • v.7 no.1
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    • pp.37-43
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    • 2019
  • This research studied production of lightweight filling production for sink hole restoration utilizing various industrial by-products(2kinds of fly ash, petro-cokes CFBC ash, blast furnace slag fine particle). For this purpose, the mixed raw material properties(compressive strength) behaviors according to the blending ratio of industrial by-products were examined by applying the experimental design method and statistical analysis was performed using the commercial program MINITAB. Compressive strengths of industrial by-products were strongly dependent on blast furnace slag powder. Compressive strength(3days aging) was 3~11MPa depending on the amount of blast furnace slag powder used. The use of CFBC fly ash was evaluated to have the least effect on compressive strength. In addition, the compressive strength and the coefficient of permeability were measured by preparing foamed concrete for the experimental batch 1 condition in the mixture experimental design. In this case, the bulk density is 0.9 to 1.0, the apparent porosity is 30 to 50%, the compressive strength(3days old) is 1 to 2MPa, and the permeability coefficient is $10^{-2}$ to $10^{-3}cm/sec$.

Physicochemical Properties of Mixtures with Mixed Organic Fertilizer and Various Organic Sources and Their Influences on Growth of Two Leaf Vegetables (유기성 자원과 혼합유기질비료 혼합물의 특성 및 처리 후 엽채류의 생육 효과)

  • Kim, Young-Sun
    • Journal of the Korea Organic Resources Recycling Association
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    • v.29 no.1
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    • pp.47-57
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    • 2021
  • This study was conducted to evaluate the properties of mixtures of mixed organic fertilizer (MOF) and various organic sources such as livestock manure compost (LMC), dried compost of poultry manure (CPM), dried food waste powder (FWP) and amino acid by-product fertilizer (ABF) and their influences on growth of lettuce and Chinese cabbage. The content of N, P2O5 and K2O of mixture of MOF, LMC and FWP (MLF) was 3.6~3.9%, 2.1~2.2% and 1.3~1.4%, respectively. Lettuce dry weight of MLF3 treatment blending with MOF (60%), LMC (10%) and FWP (30%) was increased by about 29% than that of MOF. The content of N, P2O5 and K2O of mixture of MOF, CPM, FWP and ABF (MCFA) was 4.5~4.7%, 1.7~1.9% and 1.3~1.4%, respectively. Compared to MOF, growth factors of lettuce and Chinese cabbage in the MCFA treatments were not significantly deferent. These results indicated that MLFs and MCFAs, the mixtures of respectively organic sources and MOF, could be applied as orgnic fertilizer in the cultivation of lettuce and Chinese cabbage, and were expected that LMC and ABF might be used as another sources of organic fertilizer.