• Title/Summary/Keyword: Powder Injection Molding

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Mechanical and Antibacterial Properties of Copper-added Austenitic Stainless Steel (304L) by MIM

  • Nishiyabu, Kazuaki;Masai, Yoshikaze;Ishida, Masashi;Tanaka, Shigeo
    • Journal of Powder Materials
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    • v.9 no.4
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    • pp.227-234
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    • 2002
  • For the austenitic stainless steel (304L) manufactured by metal injection molding(MIM), the effects of copper content and sintering temperature on the mechanical properties, antibacterial activities, corrosion resistance, and electric resistances were investigated. The specimens were prepared by injection molding of the premixed powders of water-atomized 304 L and Cu with poly-acetyl binders. The green compacts were prepared with various copper contents from 0 to 10 wt.% Cu, which were debound thermally at 873 K for 7.2 ks in $N_2$gas atmosphere and subsequently sintered at various temperatures from 1323 K to 1623 K for 7.2 ks in Ar gas atmosphere. The relative density and tensile strength of the sintered compacts showed the minimum values at 5 and 8 wt.% Cu, respectively. Both the relative density and the tensile strength of the specimen with 10 wt.% Cu sintered at 1373 K showed the highest values, higher than those of copper-free specimen. Antibacterial activities investigated by the plastic film contact printing method for bacilli and the quantitative analysis of copper ion dissolved in water increased as the increase of the copper content to stainless steels. It was also verified by the measurement of pitting potential that the copper addition in 304 L could improve the corrosion resistance. Furthermore the electric conductivity increased with the increase of copper content.

Metal Injection Molding of Nanostructured W-Cu Composite Powders Prepared by Mechanical Alloying (기계적 합금방법으로 제조한 극초미세 조직의 W-Cu 복합분말의 금속사출성형 연구)

  • 김진천
    • Journal of Powder Materials
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    • v.5 no.2
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    • pp.145-153
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    • 1998
  • W-Cu alloy is attractive to thermal managing materials in microelectronic devices because of its good thermal properties. The metal injection molding (MIM) of W-Cu systems can satisfy the need for mass production of the complex shaped W-Cu parts in semiconductor devices. In this study, the application of MIM process of the mechanically alloyed (MA) W-Cu composite powders, which had higher sinterability were investigated. The MA W-Cu powders and reduction treated (RT) powders were injected by using of the multicomponent binder system. The multi-stage debinding cycles were adopted in $N_2$ and $H_2$ atmosphere. The isostatic repressing treatment was carried out in order to improve the relative density of brown parts. The brown part of RT W-Cu composite powder sintered at 110$0^{\circ}C$ had shown the higher sinterability compared to that of MA powder. The relative sintered density of all specimens increased to 96% by sintering at 120$0^{\circ}C$ for 1 hour. The relationship between green density and the sintering behavior of MA W-Cu composite powder was analyzed and discussed on the basis of the nanostructured characteristics of the MA W-Cu composite powder.

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Investigation of Micro Cutting Characteristics for Tungsten-Carbide Green Part (초경 그린파트 마이크로 절삭가공 특성 분석)

  • Kim, G.H.;Jung, W.C.;Yoon, G.S.;Heo, Y.M.;Kwon, Y.S.;Cho, M.W.
    • Transactions of Materials Processing
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    • v.19 no.3
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    • pp.191-196
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    • 2010
  • Tungsten-carbide as typical difficult-to-cut material has excellent mechanical properties such as high thermal resistivity, mechanical strength and chemical durability. However, it is next to impossible for tungsten-carbide to be fabricated the needed parts by cutting process. In this study, for establishing the micro fabrication method of tungsten-carbide for micro injection or compression molding core, the investigation on micro cutting characteristics of tungsten-carbide green part which is made by powder injection molding process and easy to cut relatively was performed. For this, micro endmilling experiments of tungsten-carbide green part were performed according to various cutting conditions. Finally, the wear trend of micro endmill and the appearance of micro rib according to feed-rate and cutting depth per step were analyzed through SEM images of micro cutting feature and microscope images of micro tools.

Fabrication of Equiatomic CoCrFeMnNi High-Entropy Alloy by Metal Injection Molding Process Using Coarse-Sized Powders

  • Eun Seong Kim;Jae Man Park;Ji Sun Lee;Jungho Choe;Soung Yeoul Ahn;Sang Guk Jeong;Do Won Lee;Seong Jin Park;Hyoung Seop Kim
    • Journal of Powder Materials
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    • v.30 no.1
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    • pp.1-6
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    • 2023
  • High-entropy alloys (HEAs) are attracting attention because of their excellent properties and functions; however, they are relatively expensive compared with commercial alloys. Therefore, various efforts have been made to reduce the cost of raw materials. In this study, MIM is attempted using coarse equiatomic CoCrFeMnNi HEA powders. The mixing ratio (powder:binder) for HEA feedstock preparation is explored using torque rheometer. The block-shaped green parts are fabricated through a metal injection molding process using feedstock. The thermal debinding conditions are explored by thermogravimetric analysis, and solvent and thermal debinding are performed. It is densified under various sintering conditions considering the melting point of the HEA. The final product, which contains a small amount of non-FCC phase, is manufactured at a sintering temperature of 1250℃.

Microstructure and Sintering Behavior of Injection Molded Fe Sintered Body Using Rapid Thermal Heating Process (급속승온공정을 이용한 사출성헝된 Fe 소결체의 미세조직 및 소결거동)

  • Kim Ki-Hyun;Han Jae-Kil;Yu Ji-Hun;Choi Chul-Jin;Lee Byong-Taek
    • Journal of Powder Materials
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    • v.11 no.6 s.47
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    • pp.528-534
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    • 2004
  • Using the nano Fe powders having 50 nm in diameter, Fe compact bodies were fabricated by injec-tion molding process. The relationship between microstructure and material properties depending on the volume ratio of powder/binder and sintering temperature were characterized by SEM, TEM techniques. In the compact body with the volume percentage ratio of 45(Fe powder) : 55(binder), which was sintered at $700^{\circ}C,$ the relative density was about $97{\%},$ and the values of volume shrinkage and hardness were about $66.3{\%}$ and 242.0 Hv, respec-tively. Using the composition of 50(Fe powder) : 50(binder) and sintered at $700^{\circ}C,$ the values of relative density, volume shrinkage and hardness of Fe sintered bodies were $73.3{\%},\;47.6{\%}$ and 152.8 Hv, respectively. They showed brittle fracture mode due to the porous and fine microstructure.

Fabrication of Injection Molded Fe-50%Ni Sintered Bodies (사출성형된 Fe-50%Ni 소결체의 제조)

  • Kim Ki-Hyun;Yoon Hyeong-Chul;Choi Chul-Jin;Lee Byong-Taek
    • Journal of Powder Materials
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    • v.11 no.6 s.47
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    • pp.472-476
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    • 2004
  • The Fe-Ni compact bodies were fabricated using Fe-Ni mixed powders with 50 nm in diameter by injection molding process. The relationship between microstructure and material properties was characterized with respect to the volume ratio of powder/binder and sintering temperature with SEM and TEM. In the compact body having the volume percent ratio of 45(Fe-Ni) : 55(binder), which was sintered at $900^{\circ}C$ the values of relative density and hardness were low about 97.7% and 277.1 Hv, respectively. Using the composition of 50(Fe Ni) : 50(binder) and sintered at $900^{\circ}C$, the values of relative density and hardness were 98.5%, 294.4 Hv, respec-tively. The grain size of sintered bodies strongly depended on the sintering temperature. In both samples sintered at $600^{\circ}C$ and $900^{\circ}C$, the average grain sizes were about 150 nm and 500 nm in diameter, respectively.