• 동력기계공학회지
• /
• 제18권1호
• /
• pp.106-111
• /
• 2014

This article describes effect of post heat treatment on wear characteristics of thermally sprayed Co-based self-flux alloy coating. Co-based self-flux alloy coatings were deposited on steel substrates using a flame spray process. Post heat treatments were carried out at 800, 900, 1000 and $1100^{\circ}C$ for 30min in a vacuum chamber. For analysis of effect of post heat treatment on mechanical properties, wear test and hardness test were performed for post heat-treated coating specimen. Microstructures of heat treated coating layer and wear track were examined using SEM and EDS. Wear loss and hardness became lower with increasing post heat treatment temperature.

• 플랜트 저널
• /
• 제6권4호
• /
• pp.56-62
• /
• 2010

This study investigated characteristics of the post-weld heat treatment of SA213-T23, which was developed for water wall of the ultra super critical power boiler. The temperature of post weld heat treatment should be $730^{\circ}C$ or higher to reduce hardness of the deposit metal and heat affected zone. Coincidently, the temperature should remain $760^{\circ}C$ or lower to prevent hardness of the base metal from dropping. Hardness decline of deposit metal was trivial according to time when the holding time of heat treatment at $740^{\circ}C$ of post-weld heat treatment gradually increased from initial 15 minutes.

• 열처리공학회지
• /
• 제16권3호
• /
• pp.141-147
• /
• 2003

The effects of heat treatment on the fatigue life and welding residual stress of welded plates were investigated in this study. The plates were welded by flux cored arc welding process, and post weld heat treated at $600^{\circ}C$ for 1 hour. The residual stresses of welded plates before and after post weld heat treatment were measured by hole drilling method. To measure the fatigue life of welded plates, low cycle fatigue tests under strain control and high cycle fatigue tests under load control were performed respectively, by using cylindrical specimens containing weld metal and heat affected zone. The obtained result shows that the post weld heat treatment reduces the residual stress, and resultantly changes the fatigue life of welded plate. Goodman diagrammatic analysis has also been performed to study the effect of post weld heat treatment on the high cycle fatigue life.

• 한국표면공학회지
• /
• 제52권5호
• /
• pp.275-281
• /
• 2019

Anodization is widely used to enhance the properties of aluminum, such as hardness, electric resistance, abrasion resistance, corrosion resistance etc. But these properties can be enhanced with additional process. According to the partial crystallization of oxide layer with post heat treatment, enhanced hardness can be expected with partial crystallization. In this study, post heat treatments were applied to the anodized aluminum alloys of Al6061 to achieve the partial crystallization, and crystallizations were evaluated with the reduced breakdown voltages. Interestingly, remarkable enhanced hardness (21~29%), abrasion resistance (26~62%), and reduced breakdown voltage (24~44%) were observed for the sulfuric acid anodized samples when we annealed the anodized samples with 1hour post heat treatment at $360^{\circ}C$. For the Al5052 alloys, a lot of cracks were observed when we applied the post heat treatment.

• 소성∙가공
• /
• 제20권2호
• /
• pp.140-145
• /
• 2011

The aim of the present study is to derive optimized post heat treatment temperatures to get a proper formability for Ti/STS409L/Ti clad materials. These clad materials were fabricated by cold rolling followed by a post heat treatment process for 10 minutes at temperatures ranging from $500^{\circ}C$ to $850^{\circ}C$. The microstructure of the interface was observed using a Scanning Electron Microscope(SEM) and an Energy Dispersive X-ray Analyser(EDX) in order to investigate the effects of post heat treatment on the bonding properties of the Ti/STS409L/Ti clad materials. Diffusion bonding was observed at the interfaces with a diffusion layer thickness increasing with the post heat treatment temperature. The diffusion layer was composed of a type of(${\varepsilon}+{\zeta}$) intermetallic compound containing additional elements, namely, Fe, Ti and Ni. The micro Knoop hardness of the Ti/STS409L interfaces was found to increase with heat treatment up to $800^{\circ}C$ and then decrease for temperatures rising up to $850^{\circ}C$. The tensile strength was shown to decrease for heat treatment temperature increasing to $750^{\circ}C$ and then increase rapidly for temperature rising up to $850^{\circ}C$. A post heat treatment temperature range of $700{\sim}750^{\circ}C$ was found to optimize the formability of Ti/STS409L/Ti clad materials.

• Carbon letters
• /
• 제8권2호
• /
• pp.127-133
• /
• 2007

In this study, commercially available pitch-based carbon fibers of general grade were post-heat-treated using a boxtype high temperature furnace at $1800^{\circ}C$, $2000^{\circ}$, $2200^{\circ}C$, and $2400^{\circ}C$, respectively. The fundamental characteristics of each heat-treated carbon fibers were investigated in terms of chemical composition, morphology, thermal stability, X-ray diffraction, single filament tensile test, and electrical resistivity. The result showed that the fiber properties were significantly influenced by the post-heat-treatment, indicating the greater effect with increasing treatment temperature. The carbon contents, thermal stability, and tensile properties of the carbon fibers used here were further increased by the post-heat-treatment, whereas the d-spacing between graphene layers and the electrical resistivity were reduced with increasing post-heat-treatment temperature.

• 열처리공학회지
• /
• 제36권2호
• /
• pp.61-68
• /
• 2023

Ti and Ti alloys are used in the automobile and aerospace industries due to their high specific strength and excellent corrosion resistance. However their application is limited due to poor formability at room temperature and high unit cost. In order to overcome these issues, dissimilarly jointed materials, such as cladding materials, are widely investigated to utilize them in each industrial field because of an enhanced plasticity and relatively low cost. Among various dissimilar bonding processes, the rolled cladding process is widely used in Ti alloys, but has a disadvantage of low bonding strength. Although this problem can be solved through post-heat treatment, the mechanical properties at the bonded interface are deteriorated due to residual stress generated during post-heat treatment. Therefore, in this study, the microstructure change and residual stress trends at the interfaces of Ti/Al cladding materials were studied with increasing post-heat treatment temperature. As a result, compared to the as-rolled specimens, no difference in microstructure was observed in the specimens after postheat treatment at 300, 400, and 500℃. However, a new intermetallic compound layer was formed between Ti and Al when post-heat treatment was performed at a temperature of 600℃ or higher. Then, it was also confirmed that compressive residual stress with a large deviation was formed in Ti due to the difference in thermal expansion coefficient and modulus of elasticity between Ti Grade II and Al 1050.

• 대한치과보철학회지
• /
• 제34권4호
• /
• pp.869-902
• /
• 1996

Flexion of a metal/ceramic fixed partial denture(EPD) frameworks under function can cause fracture of porcelain or deterioration of the cement seal. This study evaluated the flexion characteristics of three-unit mandibular FPD frameworks, repacing the second pre-molar under compressive load(200g, 400g). Testing was accompished with real-time holographic interferometry, using 6 porcelain fused-to metal frameworks. Tested alloys were non-precious alloy(Heracles, Holland), semi-precious alloy(Degudent U, Germany) and precious alloy(Degudent H, Germany). Changes of the fringe patterns according to the heat treatment(porcelain firing cycle), various loads(200g, 400g), occlusal forms(occlusal porcelain veneering, facial porcelain veneering), various alloys and post-soldering units were compared. Dental study model(Nissan dental products, Inc. D51DP-500A, Japan) and six 3-unit metal/ceramic fixed partial denture frameworks were used as experimental materials. 36 holograms were taken on fixed dental study model by using the 10mW He-Ne laser and real-time holographic interferometry. On the basis of this study, the following conclusions can be drawn : 1. In the frameworks for facial porcelain veneering, the semi-precious alloy framework was least deformed and precious alloy framework, non-precious alloy framework orderly before heat treatment, and the deformation was not shown great difference among three alloys after heat treatment and post-soldering. 2. In the frameworks for occlusal porcelain veneering, the precious alloy framework was greatest deformed and the deformation was not difference between semi-precious alloy framework and non-precious alloy framework before, after heat treatment, and the deformation was not shown great difference among three alloys after post soldering. 3. In the non-precious alloy frameworks for facial porcelain veneering and occlusal porcelain veneering, the deformation was greatly decreased after heat treatment and conversely increased after post-soldering. 4. In the semi-precious alloy framework for facial porcelain veneering, the deformation was not detectable after heat treatment and increased after post-solder. And in the frame-work for occlusal porcelain veneering, the deformation was slightly decreased after heat treatment and increased after post-soldering. 5. In the precious alloy framework for facial porcelain veneering, the deformation was greatly decreased after heat treatment and increased after post-soldering, And in the framework for occlusal porcelain veneering, the deformation was greatly decreased after heat treatment and decreased after post-soldering.

• 대한치과재료학회지
• /
• 제42권2호
• /
• pp.95-106
• /
• 2015

Hardening mechanism associated with post-firing heat treatment of softening heat treated and then firing simulated Pd-Ag-Au alloy for bonding porcelain was examined by observing the change in hardness, crystal structure and microstructure. By post-firing heat treatment of as-cast, solution treated and pre-firing heat treated specimens at $650^{\circ}C$ after casting, the hardness value increased within 10 minutes. Then, hardness consistently increased until 30 minutes, and gap of hardness value among the specimens was reduced. The increase in hardness after post-firing heat treatment was caused by grain interior precipitation in the matrix. The softening heat treatment did not affect the increase in hardness by post-firing heat treatment. The precipitated phase from the parent Pd-Ag-Au-rich ${\alpha}$ phase with face-centered cubic structure by post-firing heat treatment was $Pd_3$(Sn, In) phase with face-centered tetragonal structure, which has lattice parameters of $a_{200}=4.0907{\AA}$, $c_{002}=3.745{\AA}$. From above results, appropriate post-firing heat treatment in order to support the hardness of Pd-Ag-Au metal substructure was expected to bring positive effects to durability of the prosthesis.

• Journal of Welding and Joining
• /
• 제32권2호
• /
• pp.29-36
• /
• 2014

Recently, in order to enhance the function and usefulness of products, cladding of dissimilar materials that maximizes the performance of the material is being widely used in all areas of industry as an important process. Clad steel plate, produced by cladding stainless steel plate, an anticorrosive material, on carbon steel plate, is being used to produce pressure vessels. Stainless steel plate has good corrosion resistance, and carbon steel plate has good rigidity and strength; clad steel can satisfy all of these qualities at once. This study aims to find the ${\delta}$-ferrite behavior, mechanical properties, structure change, integrity and reliability of clad steel weld on hot rolled steel plates. For this purpose, multi-layer welding, repair welding and post weld heat treatment were implemented according to welding procedure specifications (WPS). In order to observe the mechanical properties and toughness of clad steel weld zone, post weld heat treatment was carried out according to ASME Sec. VIII Div.1 UW-40 procedure for post weld heat treatment. With heat treatment at $625^{\circ}C$, the hold time was used as the process variable, increased by intervals that were doubled each time, from 80 to 1,280 min. The structure of weld part was typical cast structure; localized primary austenite areas appeared near central vermicular ferrite and fusion line. The heat affected zone showed rough austenite structure created by the weld heat input. Due to annealing effects of heat treatment, the mechanical properties (tensile strength, hardness, impact value) of the heat affected area tended to decrease. From the results of this study, it is possible to conclude the integrity of clad steel welds is not affected much in field welding, repair welding, multi-layer welding, post weld heat treatment, etc.