• Title/Summary/Keyword: Porosities

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High Temperature Oxidation Behaviour of Fe-XAl-0.1Y(X = 5, 10, 14 wt.%) Alloys (Fe-XAl-0.1Y(X =5, 10, 14 wt.%) 합금의 고온 산화거동)

  • Lee, Byung-Woo;Seo, Won-Chan;Park, Chan
    • Korean Journal of Materials Research
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    • v.13 no.12
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    • pp.791-795
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    • 2003
  • The oxidation behaviour of Fe-XAl-0.1Y(X= 5, 10, 14 wt.%) alloys were investigated at 1073, 1173 and 1273 K in oxygen/ nitrogen gas atmosphere for 1∼24 hrs using SEM/EDX, XRD and EPMA. The weight changes of Fe-XAl-0.1Y alloys followed the parabolic rate law. Oxidation rates of 10Al and 14Al alloys were ten times lower than that of 5Al alloys. This is attributed to the formations of protective $A1_2$$O_3$oxides on the surface of 10Al and 14Al alloys. The oxidation product scales of the 5Al alloy showed that thick iron oxide scales($Fe_2$$O_3$, $Fe_3$$O_4$) containing porosities formed during early stages of oxidation. With continued oxidation, aluminum oxide was formed at the alloy/scale interface.

Experience in Visual Testing of the Main Feed Water Piping Weld for Hanul Unit 3 (한울 3호기 주급수 배관 용접부 육안검사 경험)

  • Yoon, Byung Sik;Moon, Gyoon Young;Kim, Yong Sik
    • Transactions of the Korean Society of Pressure Vessels and Piping
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    • v.11 no.1
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    • pp.74-78
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    • 2015
  • Nuclear power plant steam generator that is one of the main component has several thousands of thin tubes. And the steam generator tube is subject to damage because of the severe operation conditions such as the high temperature and pressure. Therefore periodic inspections are conducted to ensure the integrity of steam generator component. Hanul unit 3 also has been inspected in accordance with in-service inspection program and is scheduled to be replaced for exceeding the plugging rate which was recommended by manufacturer. During the steam generator replacement activity, we found several clustered porosity on inner surface of main feed water pipe. Additionally crack-like indications were found at weld interface between base material and weld of main feed water pipe. This paper describes the field experience and visual testing results for inner surface of main feed water pipes. The destructive test result had shown that these indications were porosities which were caused by manufacturing process not by operation service.

Electrodeposited Porous Tungsten Oxides as Anode Materials for Lithium Secondary Batteries

  • Lee, Du-Young;Choi, Woo-Sung;Shin, Heon-Cheol
    • Journal of Electrochemical Science and Technology
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    • v.7 no.2
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    • pp.161-169
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    • 2016
  • Porous tungsten oxide thin films were prepared by electrodeposition and tested as anodes of lithium secondary batteries. The synthesized films were composed of nanoparticles of 60-140 nm size, with porosities of 30-40 %. Increasing the temperature turned out to be a more effective approach to introduce porosity in the structure than increasing the electrolyte viscosity. The assessment of the synthesized films as anodes of lithium secondary batteries revealed a much higher initial discharge capacity for the porous than the dense samples. The discharge capacity retention significantly increased with increasing porosity and was further enhanced by heat treatment. In particular, a thin film composed of particles of about 140 nm in size and with a porosity of 40 % exhibited an initial discharge capacity higher than 600 mAh/g and a remaining capacity above 300 mAh/g after 30 cycles. Following heat treatment, the remaining capacity of this sample after 30 cycles increased to about 500 mA h/g.

Fermentation Characteristics of Kochujang in Onggis with Different Porosities (통기성이 다른 옹기에서의 고추장 발효 특성)

  • Chung, Sun-Kyung;Lee, Kwang-Soo;An, Duck-Soon
    • KOREAN JOURNAL OF PACKAGING SCIENCE & TECHNOLOGY
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    • v.14 no.1
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    • pp.9-14
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    • 2008
  • The effect of different porosity of onggis, Korean earthenware, on the fermentation of kochujang was investigated. The porosity was controlled with glazing treatment. Three kinds of onggis were made: one with no glazing treatment, one with outside glazing treatment, and one with both inside and outside glazing treatment. During 4 month fermentation of kochujang in porosity-controlled earthenwares, physical, chemical, microbiological, and sensory quality attributes were monitored. Higher protease activity and higher contents of amino nitrogen, free amino acids, and total neucleotide were observed in kochujang fermented in the onggi with outside glazing treatment, which might have resulted in better sensory quality. Onggi with medium porosity could be effective for fermentation of kochujang.

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Blade Development and Test of WinDS$3000^{TM}$ System (WinDS$3000^{TM}$ 시스템의 블레이드 개발 및 시험)

  • Lee, Sang-Il;Lee, Kyeong-Woo;Joo, Wan-Don;Lee, Ki-Hak;Park, Jong-Po
    • 한국신재생에너지학회:학술대회논문집
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    • 2009.11a
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    • pp.448-448
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    • 2009
  • A new blade has been developed to apply to Doosan 3MW offshore wind turbine named as WinDS3000TM. The 3MW blade has been designed by the concept of slim external shape and optimized structure. High-performance glass fiber reinforced epoxy composites were used as the main material of the blade. The blade was manufactured using vacuum infusion process in order to increase the fiber volume fraction and to reduce micro-porosities. The blade has successfully passed the full-scale blade static test for certification. During the test, micro-failure signal and strain change of the blade were measured using acoustic emission sensors and strain gages. The blade has robust structure and weighs lighter compared to conventional blade since the new blade was designed by optimization process. The 3MW blade will be commercially applied to WinDS$3000^{TM}$ in 2010.

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An Experimental Study on the Transmission Loss of Perforated Tube Mufflers (다공관 소음기의 투과손실에 관한 실험적 연구)

  • 김찬묵;사종성;방극호
    • Proceedings of the Korean Society for Noise and Vibration Engineering Conference
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    • 2002.05a
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    • pp.346-352
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    • 2002
  • This paper is the experimental study to estimate the influence of various design parameters on the performance of mufflers with perforated tubes and through-flow partitions. Muffler types considered in the present work include through-flow chamber, through-flow chamber with partition, and cross-flow chamber. The influences of the design parameters on the performance of the mufflers can be outlined as follows. In the case of the through-f]ow type mufflers, increasing the tube thickness and the hole diameter of the perforated tubes does not change the maximum value of the transmission loss but decrease the cutoff frequency. In the case of the through-flow with partitions type mufflers, it is shown that combining a fe w short chambers and long chambers can modify the frequency locations of the resonance frequencies to optimize the performance of the mufflers. For the case of the cross-flow type mufflers, it is shown that the transmission loss of the mufflers is mainly affected by the lower porosity when the porosities are different in both sides of the plug. Overall, it is shown that performance of the through-flow type with partition type mufflers is excellent in the lower frequency region, where the cross-flow type mufflers have better performance in the higher frequency region.

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Effects of Mn, Co Additions and Microporosities on the Thermal Expansion Coefficient of powder Rolled Fe-36Ni Invar Strip (분말압연에 의해 제조된 인바(Fe-36Ni)판재의 열팽창 계수에 미치는 미세 기공 및 합금 원소 첨가 효과)

  • 이동원
    • Journal of Powder Materials
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    • v.2 no.3
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    • pp.223-230
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    • 1995
  • The effects of Mn and Co additions up to 0.6 and 2.0 wt% respectively and the amount of cold-rolled reduction on the thermal expansion coefficient (TEC) of powder rolled Fe-Ni Invar strips were investigated. The compacted strips were sintered, homogenized and cold-rolled to the final thickness of 0.8 mm, 0.65 mm and 0.4 mm. All the strips reached full density except the case of 0.8 mm sample which has a very few porosities. The interstitials which are well known to increase TEC were minimized to the level of 10 rpm C,5 and N,0 by the processing. TEC was found to decrease by increasing the cold reduction. The Mn content had little effect on the TEC. But in Fe-Ni-Co system, TEC decreased with Co content up to 0.4 wt% and then increased, yielding the minimum value of $0.2 {\times} 10-6/^{\circ}C$ at 0.4 wt% Co. This value is much lower than that of commercial Invar product. Such effect of Co is considered to be related with the maxiumum spontaneous- magnetostriction effect.

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Influence of Forest Practices on Soil Physical Properties and Facility of Purifying Water Quality in Pinus rigida Stands (리기다소나무 임분에서 산림관리작업이 토양의 물리성 및 산림의 수질정화기능에 미치는 영향)

  • Park, Jae-Hyeon
    • Journal of the Korean Society of Environmental Restoration Technology
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    • v.10 no.2
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    • pp.61-70
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    • 2007
  • This study aims to clarify the effect of forest management practices(thinning and pruning) on soil physical properties and water quality to get the fundamental information on the facility of purifying water quality after forestry practices. Rainfall, throughfall, stemflow, soil and stream water were sampled at the study site which consists of Pinus rigida in Jinju National University Experimental Forest for 4 years from Mar. 1, 2002 to Nov. 30, 2006. Averaged tree height of the management site increased by 1.6m, compared to the value of the non-management site in Pinus rigida. Increment of averaged D. B. H. at the management site showed 4.2cm more in Pinus rigida compared with that at non-management sites. Mesopore ratios (pF2.7) and total porosities of A layer soil at the management site increased more than those at the non-management sites in both stands. Otherwise, soil bulk density resulted in being reversely. Water qualities of throughfall, stemflow and buffered soil water were influenced more positively by the management practice. The average electrical conductivity of stream water was $32.9{\mu}S/cm$ within the range of non-polluted stream water.

Strength and Reliability of Porous Ceramics Measured by Sphere Indentation on Bilayer Structure

  • Ha, Jang-Hoon;Kim, Jong-Ho;Kim, Do-Kyung
    • Journal of the Korean Ceramic Society
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    • v.41 no.7
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    • pp.503-507
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    • 2004
  • The importance of porous ceramics has been increasingly recognized and adequate strength of porous ceramics is now required for structural applications. Porosities of porous ceramics act as flaws in inner volume and outer surface which result in severe strength degradation. The effect of pore structure, however, on strength and reliability of porous ceramics has not been clearly understood. We investigate the relationship between pore structure and mechanical properties using a sphere indentation on bilayer structure, porous ceramic top layer with soft polymer substrate. Porous alumina and silica were prepared to characterize the isolated pore structure and interconnected pore structure, respectively. The porous ceramic with 1mm thickness were bonded to soft polycarbonate substrate and then fracture strengths were estimated from critical loads for radial cracking of porous ceramics during sphere indentation from top surface. This simple and reproducible technique provides Weibull modulus of strength of porous ceramics with different pore structure. It shows that the porous ceramics with isolated pore structure have higher strength and higher Weibull modulus as well, than those with interconnected pore structure even with the same porosity.

Mechanical Properties of Cf/SiC Composite Using a Combined Process of Chemical Vapor Infiltration and Precursor Infiltration Pyrolysis

  • Kim, Kyung-Mi;Hahn, Yoonsoo;Lee, Sung-Min;Choi, Kyoon;Lee, Jong-Heun
    • Journal of the Korean Ceramic Society
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    • v.55 no.4
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    • pp.392-399
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    • 2018
  • $C_f/SiC$ composites were prepared via a process combining chemical vapor infiltration (CVI) and precursor infiltration pyrolysis (PIP), wherein silicon carbide matrices were infiltrated into 2.5D carbon preforms. The obtained composites exhibited porosities of 20 vol % and achieved strengths of 244 MPa in air at room temperature and 423 MPa at $1300^{\circ}C$ under an Ar atmosphere. Carbon fiber pull-out was rarely observed in the fractured surfaces, although intermediate layers of pyrolytic carbon of 150 nm thickness were deposited between the fiber and matrix. Fatigue fracture was observed after 1380 cycles under 45 MPa stress at $1000^{\circ}C$. The fractured samples were analyzed by transmission electron microscopy to observe the distributed phases.