• 제목/요약/키워드: Pore Pattern

검색결과 116건 처리시간 0.026초

실리콘 및 사파이어 기판을 이용한 알루미늄의 양극산화 공정에 관한 연구 (Fabrication of Anodic Aluminum Oxide on Si and Sapphire Substrate)

  • 김문자;이진승;유지범
    • 한국재료학회지
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    • 제14권2호
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    • pp.133-140
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    • 2004
  • We carried out anodic aluminum oxide (AAO) on a Si and a sapphire substrate. For anodic oxidation of Al two types of specimens prepared were Al(0.5 $\mu\textrm{m}$)!Si and Al(0.5 $\mu\textrm{m}$)/Ti(0.1 $\mu\textrm{m}$)$SiO_2$(0.1 $\mu\textrm{m}$)/GaN(2 $\mu\textrm{m}$)/Sapphire. Surface morphology of Al film was analyzed depending on the deposition methods such as sputtering, thermal evaporation, and electron beam evaporation. Without conventional electron lithography, we obtained ordered nano-pattern of porous alumina by in- situ process. Electropolishing of Al layer was carried out to improve the surface morphology and evaluated. Two step anodizing was adopted for ordered regular array of AAO formation. The applied electric voltage was 40 V and oxalic acid was used as an electrolyte. The reference electrode was graphite. Through the optimization of process parameters such as electrolyte concentration, temperature, and process time, a regular array of AAO was formed on Si and sapphire substrate. In case of Si substrate the diameter of pore and distance between pores was 50 and 100 nm, respectively. In case of sapphire substrate, the diameter of pore and distance between pores was 40 and 80 nm, respectively

3차원적층조형법으로 제조된 타이타늄 금속 다공체의 기공구조 및 기계적 특성에 관한 연구 (A Study on Pore Structure and Mechanical Properties of Porous Titanium Fabricated by Three-dimensional Layer Manufacturing Process)

  • 손병휘;홍재근;현용택;배석천;김승언
    • 대한금속재료학회지
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    • 제50권2호
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    • pp.100-106
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    • 2012
  • This study was performed to fabricate porous titanium foam by three-dimensional layer manufacturing process, and to evaluate the porosities, compressive stress, Young's modulus and fracture pattern. Porous titanium foam was made of CP(Commercial Pure) titanium powder (${\leq}5{\mu}m$). Total porosities of titanium foam were in the range of 55-68%. Pore size distribution was $200-440{\mu}m$ for coarse pores, $50-100{\mu}m$ for intermediate pores and $5-10{\mu}m$ for fine pores. Compression elastic modulus and compression stress were decreased with increasing porosity. Young's modulus ranged from 1.04-5.62 GPa and maximum stress ranged from 20-241 MPa. Regarding the mechanical properties, 3D(Three Demensional) porous titanium fabricated layer manufacturing is a promising material for human bone replacement.

겐타마이신 설페이트를 서방화한 다공성 PLLA 지지체의 제조와 물성평가 (Fabrication and Characterization of Porous PLLA Scaffolds with Gentamicin Sulfate Release System)

  • 최명규;강길선;이일우;이종문;이해방
    • 폴리머
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    • 제25권3호
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    • pp.318-326
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    • 2001
  • 본 연구에서는 세포 배양시 감염방지용으로 널리 쓰이는 겐타마이신 설페이트(GS)가 서방화된 다공성 PLLA 지지체를 유화동결건조방법으로 제조하였다 이들의 물성을 전자현미경 및 수은다공도계로 특성결정하였고, 적심성은 푸른염색 수용액으로 관찰하였으며, 방출거동은 high performance liquid chromatography (HPLC)를 이용하여 측정하였다. GS가 5, 10 및 20%가 포접된 PLLA 지지체의 다공도는 80~90%이었으며 평균다공크기 범위는 30~57 ${\mu}{\textrm}{m}$ 그리고 가장 큰 것으로는 150${\mu}{\textrm}{m}$이상의 것도 관찰되었다. 전체적인 다공도의 모양은 다공과 다공사이의 연결이 양호하고 대부분이 열린 셀 구조를 하고 있는 것으로 나타났다. 대조군에 비해 GS의 농도가 증가함에 따라 PLLA 지지체의 다공도가 감소하는 것으로 보아 GS내의 설페이트 부분은 친수성 역할 그리고 겐타마이신 부분은 소수성 역할을 수행하는 계면활성제의 역할에 기인한 것으로 사료된다. PLLA 지지체의 방출거동은 GS의 농도가 증가함에 따라 방출되는 양이 증가하였고, 적심성 또한 향상되어 세포배양시 긍정적 효과를 끼칠 것으로 예상되었다.

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경사식 방파제의 수리특성 결정을 위한 수치해석 (Numerical Analysis on the Determination of Hydraulic Characteristics of Rubble Mound Breakwater)

  • 박현주;전인식;이달수
    • 한국해안해양공학회지
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    • 제14권1호
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    • pp.19-33
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    • 2002
  • 경사식 방파제의 설계에 필요한 정보를 제공할 목적으로 수리특성들의 계산을 비교적 쉽게 수행하기 위한 수치해석기법의 수립을 시도하였다. 수치해석은 방파제 외부의 파동장과 내부 공극매체에서의 파동장을 결합시킴으로써 반사율, 전달율(월파전달율과 투과전달율) 그리고 개체내부의 간극수압을 계산하는 것이다. 외부 파동장은 장파가정의 근사 이론을, 내부 파동장은 경계요소법을 이용하여 해석하였다. 수치해석결과를 수리실험결과와 비교한 결과, 반사율과 전달율은 허용오차 범위내에서 비교적 잘 일치하는 것으로 나타났다. 또한, 간극수압은 정량적으로는 다소의 차이를 보이나 정성적으로는 대체적으로 유사한 성향을 보이는 것으로 나타났다. 정량적 차이를 극복하기 위하여 전사면에서의 비선형 파동장에 의한 동수압을 직접 계측하여 수치해석에 입력하는 방안을 제시하였다

Envelope development and variation in Trachelomonas hispida (Euglenophyta)

  • Poniewozik, Malgorzata;Zieba, Emil;Sajnaga, Ewa
    • ALGAE
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    • 제33권4호
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    • pp.305-318
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    • 2018
  • In Trachelomonas hispida, the adult envelope that surrounds the monad is oval in shape and covered with spines. Development of the lorica is an interesting, but poorly known phenomenon. We observed in detail the formation of spineless envelopes of T. hispida using light microscopy and scanning electron microscopy. The results showed that young cells formed delicate and net-like envelopes. The structure changed with age, and mature specimens had solid, thick loricae with small pores. As the loricae aged, they changed their shape, and rope-like fibres from the external layer started to unwind, progressing from the apical pore, exposing the underlying net-like structure. X-ray spectrometry showed that Fe was the major mineral component in young and mature loricae, whereas old loricae did not contain Fe salts, although they did contain a high number of Mn compounds. We also noticed a different pattern of mineralization process in the envelopes. Apart from the even distribution of mineral deposition over the entire lorica, we observed that it started from the apical pore and ended at the posterior end. There was considerable morphological variation in envelope shape and ornamentation, which had collars and folds around the apical pore and process at the posterior end. This suggested that many varieties of T. hispida should be taxonomically reappraised. We also discuss a hypothetical role for the spines on lorica surfaces in aquatic ecosystems.

선행강우의 영향에 따른 불포화토의 침투특성 분석 (Effect of Antecedent Rainfall on Infiltration Characteristics in Unsaturated Soil)

  • 윤귀남;신호성;김윤태
    • 한국지반공학회논문집
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    • 제31권8호
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    • pp.5-15
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    • 2015
  • 불포화 지반에서 선행강우에 의한 강우침투특성을 분석하기 위하여 국내 편마암 풍화토에 대한 일차원 실내강우 침투실험을 수행하였다. 춘천 및 충주지역 시료에 대한 실내모형실험에서 불포화토의 음의 간극수압은 강우 재하시 급격히 감소하고, 강우 종료후 점차 회복되었다. 강우강도가 증가함에 따라 침투속도가 증가하였으며, 선행강우시보다 본강우에서 침투속도가 빠른 것으로 나타났다. 이는 선행강우에 의하여 증가된 지반의 높은 포화도가 본강우시 강우침투속도를 증가시킨 것으로 사료된다. 특히 점토함유량이 많은 충주시료에서 음의 간극수압의 회복 속도와 침투속도가 느리게 나타났다. 유한요소 사면안정에 대한 수치해석 결과는 강우 침투에 의한 음의 간극수압의 감소에 따른 사면 안전율을 감소와 강우 종료후 간극수압의 확산에 의한 추가적인 사면 안정성 저감을 보여주고 있다. 사면의 안전율은 선행강우시 보다 본강우에서 더욱 감소하였다. 선행강우는 불포화지반의 초기 간극수압의 크기와 깊이별 패턴에 지대한 영향을 미치며, 이는 강우 사면의 안정성 해석에 고려해야 할 중요한 요소이다.

Proplast와 Porous Polyethylene을 이용(利用)한 가토(家兎) 하악골(下顎骨) 증대술후(增大術後) 조직반응(組織反應) 및 골형성(骨形成)에 관(關)한 연구(硏究) (A Study on the Tissue Response and Bone Formation after Augmentation Using Proplast and Porous Polyethylene in Rabbit Mandible)

  • 김건중;류선열
    • Maxillofacial Plastic and Reconstructive Surgery
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    • 제11권1호
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    • pp.101-116
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    • 1989
  • Proplast and Porous Polyethylene which have porous structures as low-modulus polymers have been recently used in maxillofacial plastic and reconstructive surgery. The purpose of this study was to compare the response of adajacent tissue, new bone formation and stability after augmentation by differen methods of subperiosteal graft using proplast and purous polythylene in rabbit mandible. The augmentation procedure was carried out by dividing into two groups, A and B. A group consisted of subperiosteal graft on the cortex, and the other B group was made up only graft following artificial decortication in the mandibular body of rabbit. The experimental animals were sacrificed on the 1st, 2nd, 4th and 8th week after grafting for macroscopic and light microscopic examination. The samples extracted at the 6th postgrafting week were also used for biometric testing and scanning electron microscopic examination. The results obtained from this study were as follows : 1. Macroscopically, infection of graft site, deformation and migration of graft material were not observed in all experimental groups. 2. B group showed more rapid and increased bone formation and the greater stability than A group, and tissue response was similar to each other. 3. In the tissue response, macrophages and cellular infiltrations were observed in Proplast group, but few in PHDPE group. 4. In bone formation of A group, Proplast group showed no bone formation until the 8th week, but PHDPE group showed small quantity of osteoid tissue from the 2nd week and appositional bone growth with new bone formation at the 8th week. 5. In bone formation of B group, both Proplast and PHDPE group showed bone formation, but PHDPE group showed more rapid and larger bone formation. 6. In pattern of bone formation, Proplast group mainly showed appositional bone growth pattern connected with graft site. On the other hand, PHDPE group showed mixed pattern of new bone formation in the pore connective tissue with appositional bone growth from graff site. 7. The maximum mean values of shear stress were serially $111.3gf/mm^{2}$ in PHDPE of B group, $84.8gf/mm^{2}$ in PHDPE of A group, $32.9gf/mm^{2}$ in Proplast B group, and $15.7gf/mm^{2}$ in Proplast of A group. From above results, It was suggested that the capacity of bone formation and stability between bone and graft material were dependent on the pore size and structure of graft material itself, the state of graft site and tissue response.

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Tiny Pores Observed by New Solar Telescope and Hinode

  • 조경석;봉수찬;채종철;김연한;박영득
    • 천문학회보
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    • 제36권1호
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    • pp.37.2-37.2
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    • 2011
  • Our previous study on tiny pores (R < 2") observed by HINODE/Solar Optical Telescope (SOT) revealed that the plasma in the pores at the photosphere is always moving down and the pores are surrounded by the strong downward motions (highly red-shifted) of neighboring granulations. From this study, we speculated that the flow motions above the pore should be related with the motions at the photosphere, since the pore is strong magnetic field region. Meanwhile, SNU and KASI installed Fast Imaging Solar Spectrograph (FISS) in the Cude room of the 1.6 m New Solar Telescope (NST) at Big Bear Solar Observatory. FISS is a unique system that can do imaging of H-alpha and Ca II 8542 band simultaneously, which is quite suitable for studying of dynamics of chromosphere. To get some clue on the relationship between the photospheric and low-chromospheric motions at the pore region, we took a coordinate observation with NST/FISS and Hinode/SOT for new emerging active region (AR11117) on October 26, 2010. In the observed region, we could find two tiny pores and two small magnetic islands (SMIs), which have similar magnetic flux with the pores but does not look dark. Magnetic flux density and Doppler velocities at the photosphere are estimated by applying the center-of-gravity (COG) method to the HINODE/spectropolarimeter (SP) data. The line-of-sight motions above the photosphere are determined by adopting the bisector method to the wing spectra of Ha and CaII 8542 lines. As results, we found the followings. (1) There are upflow motion on the pores and downflow motion on the SMIs. (2) Towards the CaII 8542 line center, upflow motion decrease and turn to downward motion in pores, while the speed of down flow motion increases in the SMIs. (3) There is oscillating motion above pores and the SMIs, and this motion keep its pattern along the height. (4) As height increase, there is a general tendency of the speed shift to downward on pores and the SMIs. This is more clearly seen on the other regions of stronger magnetic field. In this talk, we will present preliminary understanding of the coupling of pore dynamics between the photosphere and the low-chromosphere.

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화학기상증착법을 이용한 알루미나 복합 분리막의 제조 (Preparation of Alumina Composite Membranes by Chemical Vapor Deposition)

  • 안상욱;최두진;현상훈
    • 한국세라믹학회지
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    • 제31권8호
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    • pp.927-933
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    • 1994
  • Alumina composite membranes were prepared by chemical vapor deposition (CVD) using aluminum-tri-isopropoxide as a precursor. Porous alumina supports were used in deposition, which were in disk shape with mean pore diameter of 0.1 ${\mu}{\textrm}{m}$ and prepared by slip-coasting process. film deposition morphology on porous support was simulated through depositing alumina film on polycrystalline silicon pattern, and its step coverage observed by SEM showed one deviated from uniform step coverage. N2 permeability through composite membranes and the pressure dependence decreased as the deposition time increased. Initially, the N2 permeability of the top layer was tend to decrease rapidly, and then the degree of decrease in N2 permeability was tend to diminish with deposition time. The N2 permeability increased with heat treatment temperature and the crack was generated in top layer at 100$0^{\circ}C$.

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고분자 전해질 연료전지 가시화 장치를 이용한 이상유동 현상 관찰 (Visualization of two-phae flow by using transparent Proton Exchange Membrane Fuel Cell)

  • 이동율;배중면
    • 한국신재생에너지학회:학술대회논문집
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    • 한국신재생에너지학회 2009년도 춘계학술대회 논문집
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    • pp.374-377
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    • 2009
  • The operating temperature of Proton Exchange Membrane Fuel Cell (PEMFC) usually has to be limited under $100^{\circ}C$ to maintain the proper ionic conductivity. Therefore, the only product from reaction, water, is in the liquid phase. Two-phase flow makes the flow phenomenon in the channel difficult to understand and predict. Water blocking in the PEMFC channel or the pore of Gas Diffusion Layer (GDL), called flooding, is known as the main effect of PEMFC degradation. To analyze two-phase flow, the PEMFC with transparent acrylic plate was used. Two-phase flow patterns were observed by varying the current density. When the PEMFC is mounted horizontally, water in the cathode is mainly transported on the interface between the channel and GDL.

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