• Title/Summary/Keyword: Polarizing microscope

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In Situ Observation of Domain Structure of $NaNbO_3$ Using Polarizing Microscope (편광 현미경을 이용한 Sodium Niobate 단결정의 분역 구조 관찰)

  • 정선태
    • Journal of the Korean Ceramic Society
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    • v.34 no.12
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    • pp.1235-1239
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    • 1997
  • Sodium niobate single crystals were grown by high temperature solution growth with Na2O/B2O3 flux. The phase transitions and domain structures of sodium niobate were observed using transmission polarizing microscope from room temperature to $650^{\circ}C$. There was imperfect extinction region within as-grown crystals and this area could be removed by heat treatment. The area existed within crystal till 3$65^{\circ}C$, in which temperature the space group of sodium niobate is changed from Pbma to Pmnm. The phase transition from Pbma to Pmnm happened abruptly with changing domain structure. At 48$0^{\circ}C$, 52$0^{\circ}C$ and 572$^{\circ}C$, the colors and walls of domains were changed. All domains disappeared and the space group of sodium niobate was changed from P4/mbm to Pm3m at 64$0^{\circ}C$. When sodium niobate changed from high temperature phase to low temperature phase, the memory effect of domain structure was not observed.

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EVALUATION OF THE ACCURACY OF THE ELECTRONIC APEX LOCATOR USING THE POLARIZING MICROSCOPE (편광현미경을 이용한 전자적근관장측정기의 정확성에 관한 연구)

  • Park, Han-Soo;Yoon, Soo-Han
    • Restorative Dentistry and Endodontics
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    • v.17 no.1
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    • pp.235-243
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    • 1992
  • The purpose of this study was to evaluate the accuracy of an electronic apex locator, the Neosono - M, in determining the location of the cementodentinal junction. A total of 26 teeth with 46 canals were evaluated. The apex locator was used to locate the file and the teeth extracted. The specimen were prepared with highspeed burs and sandpaper discs to a thickness of $250{\sim}300{\mu}m$. Distances were measured from the cementodentinal junction with the use of polarizing microscope. Measurements made by the apex locator were also compared with those by the X - ray. The results were as follows. 1. The apex locator and X - ray were to measure a mean value of 0.17, 0.45mm coronal to the CDJ respectively. There was no significant difference between the accuracy of the apex locator and that of X - ray. 2. There was no significant difference between the accuracy of apex locator in vital and in nonvital teeth, and between in narrow and in wide canals. 3. The files in nonvital and narrow group were apical to the CDJ significantly than those of vital and narrow, vital and wide, and non vital and wide groups.

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A STUDY ON THE EARLY DETECTION OF ENAMEL CARIES BY THE LUMINESCENCE EXCITED BY ARGON LASER (아르곤 레이저 광감각법의 법랑질 우식증 조기탐지 효과에 관한 연구)

  • Lee, Nan-Young;Lee, Chang-Seop;Lee, Sang-Ho
    • Journal of the korean academy of Pediatric Dentistry
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    • v.24 no.1
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    • pp.313-324
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    • 1997
  • The aim of the present study was to describe an safe and convenient method for the early detection of enamel caries using laser fluorescence. Fluorescence from natually carious lesion of human teeth illuminated by an argon laser(488nm) was observed and photographed using barrier filter. Intact enamel was found to fluorescence with a yellowish light. Whereas, incipient caries lesions in the enamel were dearly visible as dark areas in contrast to the fluorescence surroundings. For evaluation of accuracy of this method, lesion depth measured by the laser fluorescence in light microscope was compared with that polarizing microscope. The results from the present study can be summarized as follows : 1. Enamel caries of smooth surface was observed as pale white spot and undefined outline in ordinary light. Whereas, lesion was clearly visible as dark spot in laser fluorescence. 2. There was no difference between ordinary light view and laser fluorescence in occlusal surface and interproximal surface. 3. There was no significant difference between the lesion depth observed by laser fluorescence with light microscope and polarizing microscope. Apparent correlation exists between two groups.

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OPTICAL SENSITIVITY OF LASER FLUORESCENCE FOR INCIPIENT CARIES DETECTION (초기우식병소에 대한 레이저 fluorescence의 광학적 탐지감도)

  • Kim, Hyo-Suck;Kim, Wang-Kwen;Lee, Chang-Seop;Lee, Sang-Ho
    • Journal of the korean academy of Pediatric Dentistry
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    • v.26 no.1
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    • pp.109-118
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    • 1999
  • The aim of this study was to evaluate the optical density of laser fluorescence for detection of incipient caries. Prepared and polished bovine enamel specimens were demineralized in a STPP solution for varying periods of time between 3 hrs. and 60 hrs. with an area of sound enamel retained on each specimen. The randomized specimens were analyzed for optical density of enamel demineralization using laser fluorescence. The specimens were sectioned and examined lesion depth by polarizing light microscope. Results were analyzed statistically with SAS program. The results from this study can be summarized as follows: 1. Optical density measured by laser fluorescence and lesion depth measured by polarizing light microscope was increased as demineralization time was increased(p<0.001). 2. Between optical density measured by laser fluorescence and lesion depth measured by polarizing light microscope was correlated highly(${\gamma}{\geq}0.74956$, p<0.001). 3. Regressive equation was obtained in this study as follows. Y=[X-0.260851]/0.000271(R-square:0.5618, p<0.001) (X:DENSITY, Y:DEPTH) In summary, optical density measured by laser fluorescence would be within the range of possibility to quantitatively presume demineralization amount of incipient caries lesion

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Developing Web Contents for Rock-forming Mineral Observation under Polarizing Microscope (편광현미경을 이용한 조암광물 관찰 웹 컨텐츠 개발)

  • Lee, Chang-Zin;Park, Cheol-Mo;Ryu, Chun-Ryol
    • Journal of the Korean earth science society
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    • v.30 no.2
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    • pp.176-184
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    • 2009
  • The purpose of this study is to develop and apply the web contents about the optical characteristics of rock forming minerals. The web contents developed in this study are fundamentally made up so as to show clearly the learning objective and the teaching and learning contents, and to review one content easily and search for another content freely. In addition to the web contents, the photos and moving images of the optical characteristics of rock forming minerals cited in the middle and high school textbooks are demonstrated for the students to recognize the mineral characteristics on the screen. The analysis on the quality level and teaming effect of teaching and teaming materials based on the investigation of the MALSAM after the application of the web contents to the class, showed that most students evaluated were effective for understanding the optical characteristics of the rock-forming minerals. About 62% of the students who used the web contents were able to identify the rock-forming minerals on the thin section under the polarizing microscope.

Measurement of Relative Phase Distribution of Onion Epidermal cells by using Relative Phase Microscope (상대위상 현미경을 이용한 양파 표피세포의 상대위상 측정)

  • Sin, In-Hui;Kim, Deok-Yeong
    • Proceedings of the Optical Society of Korea Conference
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    • 2006.07a
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    • pp.147-148
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    • 2006
  • Relative phase distribution of onion epidermal cells was measured by using the relative phase microscope with inverse linear polarizing method. Decrease of relative phase distribution of onion epidermal cells was also investigated as the elapse of time. In decrease of relative phase distribution, relative phase of cell membrane in onion epidermal cells decreased radically as compared with that of cytoplasm.

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Investigation and Removal Method of Efflorescence Phenomenon of Traditional Bricks - Focusing on the Efflorescence of Hwaseong Fortress in Suwon - (전(塼)의 백화현상 규명 및 제거방안 연구 - 수원화성 백화현상을 중심으로 -)

  • Chung, Kwang-Yong;Cha, Hyun-Seok
    • Journal of architectural history
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    • v.22 no.6
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    • pp.59-66
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    • 2013
  • This study progressed an investigation on the cause of the efflorescence phenomenon of bricks in Suwon Hwaseong Fortress, which is designated as a UNESCO World Heritage by using diverse scientific analyses. The samples were taken in Hwaseong and analyzed using XRD and SEM-EDS for the material identification of efflorescence. We observed under a polarizing microscope and measured absorption factors for the basic investigation for traditional bricks. As a result of material identification, soluble salt($Na_2SO_4$, $KNO_3$) and insoluble salt($CaCO_3$) were detected. There was no big difference between original bricks and repaired bricks under the polarizing microscope. However, in terms of the water absorption rate, bricks which were used for repair nowadays showed low water absorption rate(1%). In conclusion, soluble salt and insoluble salt appeared due to an effect of an air pollution and joint mortar. Soluble salt was removed in the rainy season, but insoluble salt was not removed. As a result of the efficiency and safety tests for chemicals removing efflorescence, chemical E is likely to be the suitable chemicals for the efflorescence phenomenon of traditional bricks in Suwon Hwaseong Fortress. In the future, consideration whether the use of lime is available or not should be studied through comprehensive researches including repair work, construction work and the environment factor with lime. Also, physical, chemical identifications of repairing bricks will be required.

Ferroelectric Domans in $BaTiO_3$ ($BaTiO_3$의 강유전성 분역)

  • 박봉모;정수진
    • Journal of the Korean Ceramic Society
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    • v.33 no.1
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    • pp.56-64
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    • 1996
  • A large amount of papers about the cubic-to-tetragonal phase transition the ferroelectric domain structures of the BaTiO3 were already reported but there exist still some needs to observe the domain behaviors directly. In this study the domain structures of the tinned plates prepared from ta single crystal grown by the TSSG technique were observed using a polarizing microscope TE and X-ray topography. The spatial relation be-tween the orientation states of domains was investigated and the effects of external stresses and electric fields on the behaviors of ferroelectric and ferroelastic domains were studied. All the 90$^{\circ}$walls cut off in the crystal are the wedge shaped lamellar domains and all the straight boundaries in the observed domain patte군 can be interpreted as the head-to-tail 90$^{\circ}$walls. The irregular overlapped boundaries commonly observed by using a polarizing microscope and X-ray topography are complex combinations of well-known 90$^{\circ}$walls and are domain walls were predominant and were stabilized after surface polishing. In the paraelectric phase region the domain walls vanished but the residual surface strain patterns could be seen at the same positions of the stabilized 90$^{\circ}$a-a walls in the tetragonal phase region, These stabilized walls resulted from the surface strain had a memory effect in domain formation during the repeated phase transitions and could notr be affected by an external electtric field.

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The effects of fluoride releasing orthodontic sealants on the prevention and the progressive inhibition of enamel demiheralization in vitro (광중합형 및 자가중합형 교정용 전색제의 치아우식예방 및 진행억제효과에 관한 실험적 연구)

  • Chae, Seung-Won;Cho, Jae-O;Yoon, Young-Jooh;Kim, Kwang-Won
    • The korean journal of orthodontics
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    • v.27 no.6 s.65
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    • pp.979-995
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    • 1997
  • The purpose of this study was to identify the preventive and the progressive inhibitory effects of enamel demineralization with fluoride releasing light-and self-cured orthodontic sealants(FluoroBond), in vitro, under the polarizing light microscope and the scanning electon microscope. The polarizing light microscopic group was subdivided into seven groups(Group A-Group G). The scanning electron microscopic group was also subdivided into seven groups(Group A'-Goup G'). For polarizing light microscopic evaluation, longitudinal sections were made longitudinally by Maruto cutter(Maruto Co., Japan) and Maruto grinding machine(Maruto Co., Japan). Sections were examined and photographed by the polarizing light microscope(Olympus Optical Co., Japan) using crossed polars and with the enamel rod longitudinal axis oriented at $45^{\circ}$ to the extinction position. For scanning electron microscopic evaluation, the specimens were coated with a highly conducting layer of gold palladium in a model Hus-4 high-vacuum evaporator and examined in an ISI-100B scanning electron microcope operated at 20kV. The results of this study were as follows : 1. The mean depths of artificial carious lesions under a polarized light microscope were $Group\;A(5.08{\mu}m),\;Group\;B(47.82{\mu}m,\;Group\;C(8.42{\mu}m),\;Group\;D(7.20{\mu}m),\;Group\;E(85.41{\mu}m),\;Group\;F(60.38{\mu}m),\;Group\;G(60.13{\mu}m)$. 2. There were statistically significant differences in Group B compared with Group A, C, and D(p<0.05), and also, in Group I compared with Group F and Group G(p<0.05). 3. Light-and self-cured orthodontic sealants had the preventive effects of enamel demineralization. 4. Light-and self-cured orthodontic sealants had the progressive inhibitory effects of enamel demineralization. 5. The time progress of demineralizing agent had no influence on the samples of light-and self-cured orthodontic sealants under the scanning electron microscope. 6. There was no difference between the specimens of light-and self-cured orthodontic sealants both in the polarized light microscopic group and in the scanning electron microscopic group.

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