• Title/Summary/Keyword: Plot Point

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Normalization and Search of the UV/VIS Spectra Measured from TLC/HPTLC (TLC/HPTLC에서 측정된 자외/가시부 스펙트럼의 표준화 및 검색)

  • Kang, Jong-Seong
    • YAKHAK HOEJI
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    • v.38 no.4
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    • pp.366-371
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    • 1994
  • To improve the identification power of TLC/HPTLC the in situ reflectance spectra obtained directly from plates with commercial scanner are used. The spectrum normalization should be carried out prior to comparing and searching the spectra from library for the identification of compounds. Because the reflectance does not obey the Lambert-Beer's law, there arise some problems in normalization. These problems could be solved to some extent by normalizing the spectra with regression methods. The spectra are manipulated with the regression function of a curve obtained from the correlation plot. When the parabola was used as the manipulating function, the spectra were identified with the accuracy of 97% and this result was better than that of conventionally used the point and area normalization method.

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A Study on the Alkalimetric Titration with Gran Plot in Noncomplexing Media for the Determination of Free Acid in Spent Fuel Solutions

  • 서무열;이창헌;손세철;김정숙;엄태윤
    • Bulletin of the Korean Chemical Society
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    • v.20 no.1
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    • pp.59-64
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    • 1999
  • Based on the study of hydrolysis behaviour of U(Ⅵ) ion and major fission product metal ions such as Cs(Ⅰ), Ce(Ⅲ), Nd(Ⅲ), Mo(Ⅵ), Ru(Ⅱ), and ZR(Ⅳ) in the titration media, the performance of noncomplexing-alkalimetric titration method for the determination of free acid in the presence of these metal ions was investigated and its results were compared to those from the completing methods. The free acidities could be determined as low as 0.05 meq in uranium solutions in which the molar ratio of U(Ⅵ)/H+ was less than 5, when the end-point of titration was estimated by Gran plot. The biases in the determinations were less than 1% and about +3% respectively for 0.4 meq and 0.05 meq of free acid at the U(Vl)/H+ molar ratio of up to 5. Applicability of this method to the determination of free acid in spent fuel solutions was confirmed by the analysis of nitric acid content in simulated spent fuel solutions and in a real spent fuel solution.

Application of BMP for Reduction of Runoff and NPS Pollutions (강우유출수와 비점오염물질을 저감하기 위한 최적관리기법의 적용)

  • Won, Chul-Hee;Shin, Min-Hwan;Shin, Hyun-Jun;Lim, Kyoung-Jay;Choi, Joong-Dae
    • Journal of The Korean Society of Agricultural Engineers
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    • v.55 no.5
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    • pp.1-7
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    • 2013
  • The objective of this research was to experimentally test the effect of tillage methods on the reduction of runoff, non-point source (NPS) pollution load, sediment and discharge under a rainfall simulation. We used the runoff plots of $5m{\times}30m$ ($L{\times}W$) in size. Experimental treatments were conventional tillage (CT), CT-rice straw bundle (CT-RSB) and two no-till (NT) plots; slope of 3 % or 8 % ; and rainfall intensity of 30 mm/hr. The rainfall simulation was conducted to three times. The time to initial runoff from NT plots was less than that from CT plots regardless of the slope and it was delayed about 65~90 % compared to that of CT plot. And sediment discharge of 8 % slope reduced to 55 % compared to CT plot. But the sediment discharge was not occurred at 3 % slope. The NT and CT-RSB methods have a great possibility of reducing runoff and NPS pollution loads. Runoff rate of NT plots was significantly lower than those of CT plot. The average NPS pollution loads of the NT plots and CT-RSB plot reduced about 55~80 % and 2.1~40 % compared to those of the CT plots, respectively. It was also shown that runoff and NPS pollution loads reduction by NT method could be very significant and contribute to improve the water quality of streams in agricultural regions. It was concluded that the use of NT method on agricultural fields could reduce soil erosion and muddy runoff significantly and help improve the water quality and aquatic ecosystem.

Evaluation of Flexural Strength of Silicon Die with Thickness by 4 Point Bending Test (4점굽힘시험에 의한 실리콘 다이의 두께에 따른 파단강도 평가)

  • Min, Yoon-Ki;Byeon, Jai-Won
    • Journal of the Microelectronics and Packaging Society
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    • v.18 no.1
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    • pp.15-21
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    • 2011
  • In this study, flexural strength and fracture behavior of silicon die from single crystalline silicon wafer were investigated as a function of thickness. Silicon wafers with various thickness of 300, 200, 180, 160, 150, and 100 ${\mu}m$ were prepared by mechanical grinding and polishing of as-saw wafers. Flexural strength of 40 silicon dies (size: 62.5 mm${\times}$4 mm) from each wafer was measured by four point bending test, respectively. For statistical analysis of flexural strength, shape factor(i.e., Weibull modulus) and scale factor were determined from Weibull plot. Flexural strength reflecting both statistical fracture probability and size (thickness) effect of brittle silicon die was obtained as a linear function of die thickness. Fracture appearance was discussed in relation with measured fracture strength.

Evaluation for Non-Point Sources Reduction Effect by Vegetated Ridge and Silt Fence (식생밭두렁과 실트펜스를 이용한 밭 비점오염 저감효과 평가)

  • Kim, Dong-Hyeon;Kim, Sang-Min
    • Journal of The Korean Society of Agricultural Engineers
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    • v.57 no.5
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    • pp.129-137
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    • 2015
  • The objective of this study was to test the non-point source pollution (NPS) control by the vegetated ridge and silt fence through field monitoring. The experiment plots were established with three sizes which are 5 m width by 22 m length with 8 %, 3 % slope and 15m width by 15 m length with 6 % slope. Flumes with the floating type stage gages were installed at the outlet of each plot to monitor the runoff. For a rainfall monitoring, tipping bucket rain gage was installed within the experiment site. Water quality samples were monitored during the heavy rainfall occurred. The amount of rainfall from 4 monitored events ranged from 27.6 mm to 130 mm. The runoff reduction rate could vary depending on slope, soil, crop growth condition, rainfall amount, rainfall intensity, antecedent moisture condition, and many other factors. The runoff from vegetated ridge and silt fence treatment plots was 24.05 % and -8.28 % lower than that from control plot, respectively. The monitoring results showed that the average pollution loads reduced by vegetated ridge compared to control were BOD 36.62~53.60 %, SS 40.41~73.71 %, COD 39.34~56.41 %, DOC 49.08~53.67 %, TN 26.74~67.23 %, and TP 52.72~91.80 %; by silt fence compared to control were SS 41.73 %, COD 1.93 %, and TN 2.38 %. The paired t-test result indicated that the vegetated ridge and silt fence were statistically significant effect in SS load reduction, with a 5 % significant level. Monitored results indicated that vegetated ridge and silt fence were both effective to reduce the pollutant from the field surface runoff.

Basic Studies on the Consumptive Use of Water Required for Dry Field Crops (3) -Red Pepper and Radish- (밭작물 소비수량에 관한 기초적 연구(III)-고추 및 가을 무우-)

  • 김철기;김진한;정하우;최홍규;권영현
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.32 no.1
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    • pp.55-71
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    • 1990
  • The purpose of this study is to find out the basic data for irrigation plans of red pepper and radish during the growing period, such as total amount of evapotranspiration, coefficent of evapotranspiration at each growth stage, the peak stage of evapotranspiration, the maximum ten day evapotranspiration , optimum irrigation point, total readily available moisture and intervals of irrigation date. The plots of experiment were arranged with split plot design which were composed of two factors, irrigation point for main plot and soil texture for split plot, and three levels ; irrigation point with pH1.7-2.0, pF2.1-2.4 and pF2.5-2.8, at soil texture of sandy soil, sandy loam and silty clay for both red pepper and radish, with two replications. The results obtained are summarized as follows. 1.1/10 exceedance probability values of maximum total pan evaporation during growing period for red peppr and radish were shown as 663.6 mm and 251.8 mm. respectively, and those of maximum ten day pan evaporation for red pepper and radish, 67.1 mm and 46.9 mm, respectively. 2.The time that annual maximum of ten day pan evaporation can he occurred, exists at any stage between the middle of May and the late of August for red pepper, and at any stage between the late of August and the late September for radish. 3.The magnitude of evapotranspiration and its coefficient for red pepper was occurred large in order of pF1.7-2.0 pF2.1-2.4 and pF2.5~2.8 in aspect of irrigation point and the difference in the magnitude of evapotranspiration and of its coefficient between levels of irrigation point was difficult to be found out due to the relative increase in water consumption resulted from large flourishing growth at the irrigation point in lower water content for radish. In aspect of soil texture they were appeared large in order of sandy loam, silty clay and sandy soil for both red pepper and radish. 4.The magnitude of leaf area index was shown large in order of pF2.1-2.4, pF2.5-2.8, and pFl.7-2.0, for red pepper and of pF2.5-2.8, pF2.1-2.4, pFl.7-2.0 for radish in aspect of irrigation point, and large in order of sandy loam, silty clay, sandy soil for both red pepper and radish in aspect of soil texture 5.1/10 exceedance probability value of evapotranspiration and its coefficient during the growing period for red pepper were shown as 683.5 mm and 1.03, respectively, while those of radish, 250.3 mm and 0, 99. respectively. 6.The time that the maximum evapotranspiration of red pepper can be occurred is in the middle of August around the date of ninetieth to hundredth after transplanting, and the time for radish is presumed to be in the late of September, around the date of thirtieth to fourtieth after sowing. At that time, 1/10 exceedance probability value of ten day evapotranspiration and its coefficient for red pepper is assumed to be 81.8 mm and 1.22, respectively, while those of radish, 49, 7 mm and 1, 06, respectively. 7.Optimum irrigation point for red pepper on the basis of the yield of raw matter is assumed to be pFl.7-2.0 for sandy soil, pF2.5-2.8 for sandy loam, and pF2.1-2.4 for silty clay. while that for radish is appeared to be pF2.5-2.8 in any soil texture used. 8.The soil moisture extraction patterns of red pepper and radish have shown that maximum extraction rates exist at 7 cm deep layer at the beginning stage of growth in any soil texture and that extraction rates of 21 cm to 35 cm deep layer are increased as getting closer to the late stage of growth. And especially the extraction rates have shown tendency to be greatest at 21cm deep layer from the most flourishing stage of growth for red pepper and at the last stage of growth for radish. 9.The total readily available moisture on the basic of the optimum irrigation point become 3.77-8.66 mm for sandy soil, 28.39-34.67 mm for sandy loam and 18.40-25.70 mm for silty clay for red pepper of each soil texture used but that of radish that has shown the optimum irrigation point of pF2.5-2.8 in any soil texture used. 12.49-15.27 mm for sandy soil, 23.03-28.13 mm for sandy loam, and 22.56~27.57 mm for silty clay. 10.On the basis of each optimum irrigation point. the intervals of irrigation date at the growth stage of maximum consumptive use of red pepper become l.4 days for sandy soil, 3.8 days for sandy loam and 2.6 days for silty clay, while those of radish, about 7.2 days.

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Study on the Evapotranspiration of Crisphead Lettuce by the Weighing Lysimeter (Weighing Lysimeter에 의한 결구상치의 증발산량 조사연구)

  • 김시원;김선주;노희수
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.28 no.4
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    • pp.41-48
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    • 1986
  • This study was fulfilled by the weighing lysimeter method at the experimental farm of KonKuk University from April to June of 1986 to investgate the amount of evapotranspiration ( ET-lettuec )by the growing periods, evapotranspiration ratio, amount of watering per one time, days of intermission and soil moisture extraction pattern of the crisphead lettuce cultivated in the clay loam soil by different watering points of pFl.7, pF2.O, pF2.7. The results obtained are summar ized as follows : 1.The total evapotranspiration(ETlettuce) of the pFl.7 treatment plot was 358,9mm., 314.9mm in the pF2.O plot and 281.8mm in the pF2.7 plot, therefore the total ETlettuec increased with the difference of 33mm-44mm by the decrease of watering point. 2.The daily maximum ETlettuce by the watering points was 7.66mm, 6:54mm, 5.98mm, respectively in the last ten days of May, and the mean daily ETlettuce during the growing season by the watering points of pFl.7, pF2.O and pF2.7 was 5.44mm(384.5g), 4.77mm(337.2g) and 4.27mm(301.8g), respectively. 3.The evapotranspiration ratio showed maximum value in the middle of May which was the beginning of mid-season stage, and the mean evapotranspiration ratio during the total growing period was 1A7, 1.29, 1.15 by the watering points. 4.The days of watering intermission by the watering points of pFl.7, pF2.O and pF2.7 was 1.0day, 2.9days and 12.Sdays, respectively. 5.The yield of the crisphead lettuce by the watering treatments showed very high significance, and the pF2.O was confirmed as a optimum watering point. 6.The soil moisture extraction pattern(SMEP) of the pF2.0 treatment plot in the initial stage was 85.6% in the 1st and 2nd soil layer and 14.4% in the 3rd and 4th layer, and in the midseason stage, the moisture extraction proportion of the under layer accounted for 34.7%which showed that the root elongated to the lowest soil layer, and there was no difference of the SMEP between the mid-season and late-season stage. 7.The correlation coefficient between the ETlettuce and yield of lettuce by the three watering points was.739, which showed the significance of 5%.

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Determination of Free Acid in U(VI)-Al(III) Solutions by Gran Plot Titration (Gran Plot 적정법을 이용한 U(VI)-AI(III) 용액의 자유산 농도 측정)

  • Suh, Moo-Yul;Lee, Chang-Heon;Sohn, Se-Chul;Kim, Jung-Suk;Kim, Won-Ho;Eom, Tae-Yoon
    • Analytical Science and Technology
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    • v.12 no.3
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    • pp.177-183
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    • 1999
  • The determination method of free acid in spent U-Al nuclear fuel solutions by Gran plot titration was described. Effect of U(VI) and Al(III) on the alkalimetric titration of nitric acid was investigated in oxalate complexing media as well as in noncomplexing media. Positive biases were observed in both titration media when the end-point was estimated by the Gran plot method. It was found that the cause of the bias was U(VI) in the oxalate complexing media, but Al(III) in the noncomplexing media. The relative error was less than 1% in the titration of 0.1 M $HNO_3$ at a U(VI) : Al(III) : $H^+$ mole ratio of up to 2:12:1 as long as the pH of the oxalate titration media was sustained to be below 5.0 at the beginning of titration. The method was successfully applied to the determination of nitric acid in a solution of HANARO reactor fuel with U:Al mole ratio of 1:6.

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Lowess and outlier analysis of biological oxygen demand on Nakdong main stream river (낙동강 본류 측정소들의 생물학적 산소요구량 수치에 대한 비모수적 회귀분석과 특이점분석)

  • Kim, Jong Tae
    • Journal of the Korean Data and Information Science Society
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    • v.25 no.1
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    • pp.119-130
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    • 2014
  • This paper is based on water information system of NIE, National Institute of Environmental Research. We used monthly data of water quality from January, 2013 to August, 2013 starting from measuring point A (nbA) to measuring point N (nbN) located along the Nakdong river main stream. Statistical water quality analysis of BOD (biological oxygen demand) is specified by R programming depending on month, year, and points. Based on BOD measured from Nakdong river's measuring points, we used exploratory data analysis and locally weighted scatter plot smoother (Lowess) trend analysis, which is a method of non-parametic regression analysis, to analyze long-term water tendency and water quality distribution depending on points. Also, we analyzed the period and the measuring point of which the outliers are abundant. As a result, compared to BOD measured in nbM located in Busan along the downstream, BOD measured in nbG located in Daegu and nbI located in Changwon along the midstream showed higher rate of water pollution at a severe level.

Basic Studies on the Consumptive Use of Water Required for Dry Field Crops (2) -Garlic and Cucumber- (밭작물소비수량에 관한 기초적 연구(II)-마늘 및 오이-)

  • 김철기;김진한;정하우;최홍규;권영헌
    • Magazine of the Korean Society of Agricultural Engineers
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    • v.31 no.3
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    • pp.41-56
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    • 1989
  • The purpose of this study is to find out the basic data for irrigation plans of garlic and cucumber during the growing period, such as total amount of evapotranspiration, coefficients of evapotranspiration at each growth stage, the peak stage of evapotranspiration and the maximum evapotranspiraton, optimum irrigation point, total readily available moisture, and intervals of irrigation date. The plots of experiment were arranged with split plot design which were composed of two factors, irrigation point for main plot and soil texture for split plot, and three levels ; irrigation points with pP 1.7-2.1, pP 2.2-2.5, pP 2.6-2.8, for garlic and those with pP 1.9, pF 2.3, pP 2.7, for cucumber, soil textures of silty clay, sandy loam and sandy soil for both garlic and cucumber, with two replications. The results obtained are summarized as follows 1.There was the highest significant correlation between the avapotranspiration of garlic and cucumber and the pan evaporation, beyond all other meteorological factors considered, as mentioned in the previous paper. Therefore, the pan evaporation is enough to be used as a meteorological index measuring the quantity of evapotranspiration. 2.1/10 probability values of maximum total pan evaporation during growing period for garlic and cucumber were shown as 495.8mm and 406.8mm, respectively, and those of maximum ten day pan evaporation for garlic and cucumber, 63.8mm and 69.7mm, respectively. 3.The time that annual maximum of ten day pan evaporation can be occurred, exists at any stage between the middle of May and the late of June(harvest period) for garlic, and at any stage of growing period for cucumber. 4.The magnitude of evapotranspiration and of its coefficient for garlic and cucumber was occurred in the order of pF 1.7-2.1>pF 2.2-2.5>pF 2.6-2.8 and of pF 1.9>pF 2.3>pF2.7 respectively in aspect of irrigation point and of sandy loam>silty clay>sandy soil in aspect of soil texture for both garlic and cucumber. 5.The magnitude of leaf area index was shown in the order of pF 2.2-2.5>pF 1.7-2.1>pF 2.6-2.8 for garlic and of pF 1.9>pF 2.3>pF 2.7 for cucumber in aspect of irrigation point, and of sandy loam>sandy soil>silty clay in aspect of soil texture for both garlic and cucumber. 6.1/10 probability value of evapotranspiration and its coefficient during the growing period for garlic were shown as 391.7mm and 0.79 respectively, while those of cucumber, 423.lmm and 1.04 respectively. 7.The time the maximum evapotranspiration of garlic can be occurred is at the date of thirtieth before harvest period and the time for cucumber is presumed to be at the date of sixtieth to seventieth after transplanting, At that time, 1/10 probability value of ten day evapotranspiration and its coefficient for garlic is presumed to be 65.lmm and 1.02 respectively, while those of cucumber, 94.8mm and 1.36 respectively. 8.In aspect of irrigation point, the weight of raw garlic and cucumber were increased in the order of pF 2.2-2.5>pF 1.7-2.1>pF 2.6-2.8 and of pF 1.9>pF 2.3>pF 2.7 respectively. Therefore, optimum irrigation point for garlic and cucumber is presumed to be pF 2.2-2.5 and pF 1.9 respectively, when the significance of yield between the different irrigation treatments is considered. 9.Except the mulching period of garlic that soil moisture extraction patterns were about the same, those of garlic and cucumber have shown that maximum extraction rate exists at 7cm deep layer at the beginning stage after removing mulching for garlic and at the beginning stage of growth for cucumber and that extraction rates of 21cm to 35cm deep layer are increased as getting closer to the late stage of growth. 10.Total readily available moisture of garlic in silty clay, sandy loam, sandy soil become to be 18.71-24.96mm, 19.08-25.43mm, 10.35- 13.80mm respctively on the basis of the optimum irrigation point with pF 2.2-2.5, while that of cucumber, 11.8lmm, 12.03mm, 6.39mm respectively on the basis of the optimum irrigation point with pF 1.9. 11.The intervals of irrigation date of garlic and cucumber at the growth stage of maximum consumptive use become to be about three and a half days and one and a half days respectively, on the basis of each optimum irrgation point.

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