• Journal of Welding and Joining
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• 제28권6호
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• pp.40-44
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• 2010

Laser assisted machining (LAM) has been researched in order to machine the silicon nitride ceramics economically and effectively. LAM is an effective machining method by local heating of the cutting part to the softening temperature of the silicon nitride using laser beam. When silicon nitride ceramics is heated using a laser beam, the surface of silicon nitride ceramic is softened, oxidized and decomposed. And then surface hardness is decreased. Through machining in low viscosity and hardness conditions, silicon nitride was machined effectively and the life span of tool was increased. The plastic deformation was occurred due to softening of amorphous YSiAlON above $ 1,000^{\circ}C$. Transgranular fracture of ${\beta}-Si_3N_4$ was occurred when YSiAlON was not softened, but mostly intergranular fracture was occurred by the plastic deformation of softened YSiAlON.

• Journal of Pharmaceutical Investigation
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• 제25권3호
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• pp.213-221
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• 1995

The steady shear flow properties of six kinds of commercial toothpastes were measured using a concentric cylinder type rheometer. In this paper, the shear rate and temperature dependencies of their flow behavior were investigated and the validity of the Casson and Herschel-Bulkley models was examined. Further, the flow properties over a wide temperature range were quantitatively evaluated by calculating the various material parameters. Main results obtained from this study can be summarized as follows: (1) Toothpastes are plastic fluids with a yield stress and their flow behavior shows shear-thinning characteristics. (2) With increasing temperature, the degree of shear-thinning becomes weaker and the Newtonian flow behavior occurs at a lower shear rate range. (3) The Herschel-Bulkley model is more effective than the Casson model in predicting their flow behavior. (4) As the temperature increases, the yield stress, plastic viscosity and consistency index become smaller, on the contrary, the flow behavior index becomes larger.

• Elastomers and Composites
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• 제43권2호
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• pp.72-81
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• 2008

포장도로의 소성변형을 줄여보고자 개질아스팔트가 나타나고 있다. 본 연구에서는 타이어 고무 등을 이용하여 개질된 아스팔트의 물성을 알아 보았다. 마샬안정도와 인장강도가 각각 98% 및 43% 증가하여 타이어 고무의 개질효과를 알 수 있었다. 점도, 침입 및 열 분석에서 아스팔트의 변형저항성이 향상되었음을 알 수 있었다. IR 및 GPC 실험에서 개질제의 구조가 아스팔트의 구조와 유사할 경우 두 화합물 사이에 화학결합이 발생하여 분자들의 크기가 증가함으로써 개질효과가 커짐을 알 수 있었다.

• Earthquakes and Structures
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• 제22권2호
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• pp.203-218
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• 2022

In this paper, quasi-static tests were carried out on three prefabricated reinforced concrete column-steel beam (RCS) sub-assemblages with floor slabs and one comparison specimen without floor slab. The effects of axial compression and floor slab on the seismic performance were studied, and finite element simulations were conducted using ABAQUS. The results showed that the failure of prefabricated RCS sub-assemblages with floor occurred as a joint beam and column failure mode, while failure of sub-assemblages without floor occurred due to beam plastic hinge formation. Compared to the prefabricated RCS sub-assemblages without floor slab, the overall stiffness of the sub-assemblages with floor slab was between 19.2% and 45.4% higher, and the maximum load bearing capacity increased by 26.8%. However, the equivalent viscosity coefficient was essentially unchanged. When the axial compression ratio increased from 0.24 to 0.36, the hysteretic loops of the sub-assemblages with floor became fuller, and the load bearing capacity, ductility, and energy dissipation capacity increased by 12.1%, 12.9% and 8.9%, respectively. Also, the initial stiffness increased by 10.2%, but the stiffness degradation accelerated. The proportion of column drift caused by beam end plastic bending and column end bending changed from 35% and 46% to 47% and 36%, respectively. Comparative finite element analyses indicated that the numerical simulation outcomes agreed well with the experimental results.

• 한국안광학회지
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• 제9권2호
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• pp.481-489
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• 2004

Poly(triazine bissulfide)s는 상간이동촉매하에서 bis(4-chloro-3-nitrophenyl)sulfone와 6-dibutylamino-1,3,5-triazine-2,4-dithiol로도 합성하였으며, 또한 m-dibromide xylene와 p-dibromide xylene으로 cetyltrimethyl ammonium bromide와 함께 $70^{\circ}C$에서 24시간 동안 6-dibutylamino-1,3,5-triazine-2,4-dithiol로 반응시켜서도 합성하였다. 캐스트필름을 만들기 위해서 합성한 이들에 대한 용해도, 열적 성질, 평균분자량 등에 대해서 좋은 결과를 얻었다. 이러한 결과는 기능성 광학플라스틱 재료인 고분자물질을 합성하는데 있어서 중요한 것임을 보여주는 것이다. 최대대수정도는 $50{\sim}60^{\circ}C$이상에서 0.57~1.40dl/g의 값을 보였다.

• 한국자기학회지
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• 제8권5호
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• pp.275-281
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• 1998

커플링제 종류에 따른 플라스틱 페라이트 이방성 자석의 레올러지와 자기특성에 미치는 영향을 조사하여 비교하였다. 커플링제는 silane A174와 titanete TTS를 사용하였으며, 고분자 결합제는 polypropylene(PP), 자성분말은 Sr-페라이트를 사용하였다. TTS의 첨가가 A174의 첨가보다 혼합물의 점도 감소와 자기특성 증가에 더 효과적이었다. 커플링제가 첨가되지 않은 혼합물과 비교하여, A174는 23%, TTS는 50%의 점도 감소 효과를 나타내었다. (전단율 1280 sec-1에서). 4 kOe의 자장하에서 사출성현한 플라스틱 이방성 자석은 커플링제로 처리되지 않은 자석 (잔류자속밀도 : 1.89 kG, 최대자기에너지적 : 0.84 MGOe)에 비해 A174 처리에 의해 잔류자속밀도는 2.25 kG, 최대자기에너지적은 1.23 MGOe로 향상되었으며, TTS의 처리에 의해 잔류자속밀도는 2.35 kG, 최대자기 에너지적은 1.33 MGOe로 각각 향상되었다.

• Journal of Pharmaceutical Investigation
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• 제37권3호
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• pp.137-148
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• 2007

Using a strain-controlled rheometer [Rheometrics Dynamic Analyzer (RDA II)], the steady shear flow properties of a semi-solid ointment base (vaseline) have been measured over a wide range of shear rates at temperature range of $25{\sim}60^{\circ}C$. In this article, the steady shear flow properties (shear stress, steady shear viscosity and yield stress) were reported from the experimentally obtained data and the effects of shear rate as well as temperature on these properties were discussed in detail. In addition, several inelastic-viscoplastic flow models including a yield stress parameter were employed to make a quantitative evaluation of the steady shear flow behavior, and then the applicability of these models was examined by calculating the various material parameters (yield stress, consistency index and flow behavior index). Main findings obtained from this study can be summarized as follows : (1) At temperature range lower than $40^{\circ}C$, vaseline is regarded as a viscoplastic material having a finite magnitude of yield stress and its flow behavior beyond a yield stress shows a shear-thinning (or pseudo-plastic) feature, indicating a decrease in steady shear viscosity as an increase in shear rate. At this temperature range, the flow curve of vaseline has two inflection points and the first inflection point occurring at relatively lower shear rate corresponds to a static yield stress. The static yield stress of vaseline is decreased with increasing temperature and takes place at a lower shear rate, due to a progressive breakdown of three dimensional network structure. (2) At temperature range higher than $45^{\circ}C$, vaseline becomes a viscous liquid with no yield stress and its flow character exhibits a Newtonian behavior, demonstrating a constant steady shear viscosity regardless of an increase in shear rate. With increasing temperature, vaseline begins to show a Newtonian behavior at a lower shear rate range, indicating that the microcrystalline structure is completely destroyed due to a synergic effect of high temperature and shear deformation. (3) Over a whole range of temperatures tested, the Herschel-Bulkley, Mizrahi-Berk, and Heinz-Casson models are all applicable and have an almostly equivalent ability to quantitatively describe the steady shear flow behavior of vaseline, whereas the Bingham, Casson,and Vocadlo models do not give a good ability.

• 한국산업융합학회 논문집
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• 제6권3호
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• pp.171-176
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• 2003

The poly(triazine bissulfide) synthesized from 6-dibutylamino-1,3,5-triazine-2,4-dithiol with bis(4-chloro-3-nitrophenyl) sulfone in the presence of the phase transfer catalyst, the maximum algebra viscosity (0.57 dL/g) is stable at reaction temperature of $60^{\circ}C$ overall. We could not acquire the good result about solubility, thermal property, and molecular weight to make cast film, we made base for the synthesis of functionalization polymer material.

• 한국정밀공학회지
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• 제23권1호
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• pp.159-165
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• 2006

Many rubber products are used in industrial products such as various hoses, rubber belts and oil seals etc. Especially, more then 200 rubber parts are used in the automobile, but design technology of these is largely dependent on Held experiences. These methods brought about too much time and cost in the developing procedures. However, with the help of recent rapid development of non-liner computer analysis, we can develop new sound products at low cost. Therefore in this study, optimizations of design variables such as location and number of gate in order to develop CLIP rubber product made of EPDM were performed by CAE in which Cross-WLF equations are adopted. The validity of proposed variables is evaluated by comparison with real forming results.

• 한국콘크리트학회:학술대회논문집
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• 한국콘크리트학회 1995년도 봄 학술발표회 논문집
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• pp.42-47
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• 1995

The flow properties of xoncrete depend on form of fine aggregate, the ratio of voides of fine aggregate and cement paste So, in this study, investigated for the improvement of rheology properties on mortar and paste replaced by Zeolite $\circled1$ The slump flow have to do with correlation on yielding value of mortar respectirely. $\circled2$The increase ratio of strength Mortar and paste 10% replaced by Zeolite was presented significently but the slump flow was decteased stiffly as the increase of plastic viscosity at the ratio of replacement over 10%