• Title/Summary/Keyword: Plasma Carburizing

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Influence of Treatment Temperature on Surface Characteristics during Low Temperature Plasma Carburizing and DLC duplex treatment of AISI316L Stainless Steel (AISI316L 강에 저온 플라즈마침탄 및 DLC 복합 코팅처리 시 처리온도에 따른 표면특성평가)

  • Lee, In-Sup
    • Journal of Ocean Engineering and Technology
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    • v.25 no.6
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    • pp.60-65
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    • 2011
  • A low temperature plasma carburizing process was performed on AISI 316L austenitic stainless steel to achieve an enhancement of the surface hardness without degradation of its corrosion resistance. Attempts were made to investigate the influence of the processing temperatures on the surface hardened layer during low temperature plasma carburizing in order to obtain the optimum processing conditions. The expanded austenite (${\gamma}_c$) phase, which contains a high saturation of carbon (S phase), was formed on all of the treated surfaces. Precipitates of chromium carbides were detected in the hardened layer (C-enriched layer) only for the specimen treated at $550^{\circ}C$. The hardened layer thickness of ${\gamma}_c$ increased up to about $65{\mu}m$ with increasing treatment temperature. The surface hardness reached about 900 $HK_{0.05}$, which is about 4 times higher than that of the untreated sample (250 $HK_{0.05}$). A minor loss in corrosion resistance was observed for the specimens treated at temperatures of $300^{\circ}C{\sim}450^{\circ}C$ compared with untreated austenitic stainless steel. In particular, the precipitation of chromium carbides at $550^{\circ}C$ led to a significant decrease in the corrosion resistance. A diamond-like carbon (DLC) film coating was applied to improve the wear and friction properties of the S phase layer. The DLC film showed a low and stable friction coefficient value of about 0.1 compared with that of the carburized surface (about 0.45). The hardness and corrosion resistance of the S phase layer were further improved by the application of such a DLC film.

Spark Plasma Sintering Method to Replace Carburizing Process (침탄 공정 대체를 위한 방전 플라즈마 소결 방법)

  • Jeon, Junhyub;Lee, Junho;Seo, Namhyuk;Son, Seung Bae;Jung, Jae-Gil;Lee, Seok-Jae
    • Journal of Powder Materials
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    • v.29 no.3
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    • pp.219-225
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    • 2022
  • An alternative fabrication method for carburizing steel using spark plasma sintering (SPS) is investigated. The sintered carburized sample, which exhibits surface modification effects such as carburizing, sintered Fe, and sintered Fe-0.8 wt.%C alloys, is fabricated using SPS. X-ray diffraction and micro Vickers tests are employed to confirm the phase and properties. Finite element analysis is performed to evaluate the change in hardness and analyze the carbon content and residual stress of the carburized sample. The change in the hardness of the carburized sample has the same tendency to predict hardness. The difference in hardness between the carburized sample and the predicted value is also discussed. The carburized sample exhibits a compressive residual stress at the surface. These results indicate that the carburized sample experiences a surface modification effect without carburization. Field emission scanning electron microscopy is employed to verify the change in phase. A novel fabrication method for altering the carburization is successfully proposed. We expect this fabrication method to solve the problems associated with carburization.

Study on the Mechanical Properties of Power Metallurgy Spline Hub for Clutch Disc (클러치 디스크용 분말야금 스플라인 허브의 기계적성질에 관한 연구)

  • 최문일;장진호;강성수
    • Transactions of the Korean Society of Automotive Engineers
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    • v.6 no.5
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    • pp.104-110
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    • 1998
  • In automotive industries, various processes for the cost reduction have been investigated lively. As one of them, powder metallurgy becomes influential. Compared to other methods used for he manufacture of steel components the Powder metallurgy process is competitive primarily due to the small number of production steps to reach the final geometry and thereby also the energy-efficiency. In this paper, to alter present forging process into powder metallurgy process by which the automotive clutch disc spline hub is manufactured machining process, the mechanical properties of sintered materials is investigated by specimen test. Selecting the 3 kinds of materials-SMF 4040, SMF 9060 and DHP-1, their properties according to heat treatment such as carburizing -tempering and plasma-nitrodizing are compared. By result of specimen test - tensile test, compression ring test, Impacting test, measurment of hardness, and microstructure analysis - we concluded that SMF 9060 and carburizing-tempering heat treatment is an optimal material and heat treatment method for the spline hub. It will be able to reduce manufacturing cost and weight.

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The Effects of Gas Compositions During Post Nitriding on the AISI 316L Stainless Steel after Plasma Carburizing

  • Lee, Insup
    • Journal of Surface Science and Engineering
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    • v.48 no.6
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    • pp.269-274
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    • 2015
  • In this experiment, post-nitriding treatment was performed at $400^{\circ}C$ on AISI 316 stainless steel which was plasma carburized previously at $430^{\circ}C$ for 15 hours. Plasma nitriding was implemented on AISI 316 stainless steel at various gas compositions (25% $N_2$, 50% $N_2$ and 75% $N_2$) for 4 hours. Additionally, during post nitriding Ar gas was used with $H_2$ and $N_2$ to observe the improvement of surface properties. After treatment, the behavior of the hybrid layer was investigated by optical microscopy, X-ray diffraction, and micro-hardness testing. Potentiodynamic polarization test was also used to evaluate the corrosion resistance of the samples. Meanwhile, it was found that the surface hardness increased with increasing the nitrogen gas content. Also small percentage of Ar gas was introduced in the post nitriding process which improved the hardness of the hardened layer but reduced the corrosion resistance compared with the carburized sample. The experiment revealed that AISI 316L stainless steel showed better hardness and excellent corrosion resistance compared with the carburized sample, when 75% $N_2$ gas was used during the post nitriding treatment. Also addition of Ar gas during post nitriding treatment degraded the corrosion resistance of the sample compared with the carburized sample.