• Journal of Powder Materials
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• v.22 no.4
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• pp.266-270
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• 2015

The synthesis of NiTi alloy powders by hydrogen reduction and dehydrogenation process of NiO and $TiH_2$ powder mixtures is investigated. Mixtures of NiO and $TiH_2$ powders are prepared by simple mixing for 1 h or ball milling for 24 h. Simple-mixed mixture shows that fine NiO particles are homogeneously coated on the surface of $TiH_2$ powders, whereas ball milled one exhibits the morphology with mixing of fine NiO and $TiH_2$ particles. Thermogravimetric analysis in hydrogen atmosphere reveals that the NiO and $TiH_2$ phase are changed to metallic Ni and Ti in the temperature range of 260 to $290^{\circ}C$ and 553 to $639^{\circ}C$, respectively. In the simple-mixed powders by heat-up to $700^{\circ}C$, agglomerates with solid particles and solidified liquid phase are observed, and the size of agglomerates is increased at $1000^{\circ}C$. From the XRD analysis, the presence of liquid phase is explained by the formation and melting of $NiTi_2$ inter-metallic compound due to an exothermic reaction between Ni and Ti. The simple-mixed powders, heated to $1000^{\circ}C$, lead to the formation of NiTi phase but additional Ni-, Ti-rich and Ti-oxide phases. In contrast, the microstructure of ball-milled powders is characterized by the neck-grown particles, forming $Ni_3Ti$, Ti-oxide and unreacted Ni phase.

• Bulletin of the Korean Chemical Society
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• v.28 no.11
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• pp.1980-1984
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• 2007

An HPLC chiral stationary phase (CSP) which has only two ureide functional groups was prepared starting from (1S,2S)-1,2-diaminocyclohexane. The CSP was successful in the resolution of various N-(3,5- dinitrobenzoyl)-α-amino acids, the separation (α) and the resolution factors (RS) being within the range of 1.11-1.35 and 2.19-5.17, respectively with the use of 20% 2-propanol in hexane containing 0.1% trifluoroacetic acid as a mobile phase. However, ethyl esters of N-(3,5-dinitrobenzoyl)-α-amino acids were not resolved or resolved with only marginal separation and resolution factors on the CSP under the identical mobile phase condition. From these results, the complexation of the carboxylate anions of analytes inside the double-ureide pocket of the CSP was expected to play some important role for the chiral recognition. In contrast, N-(3,5- dinitrobenzoyl)-α-amino acid N-propylamides were resolved on the CSP with reasonable separation and resolution factors. Enantioselective hydrogen bonding interactions between analytes and the CSP were presumed to be responsible for these resolutions.

• Proceedings of the KIEE Conference
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• 2002.06a
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• pp.187-190
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• 2002

In contrast to conventional electromagnetic motor, USM(Ultrasonic Motor), as piezoelectric ceramic applying ultrasonic mechanical vibration and as frictional-movement type motor, get rotational torque by elastic friction between stator and rotator, The USM, which is small motor without iron cores and coil as a simple structure, has little load weight, has character of high torque at low speed, and can apply a direct drive type without deceleration gear as low speed type. A response of USM from control input is satisfactory, and also generates much torque in low speed driving, and holding torque is much without supplying power. In this study, I designed and made Ultrasonic motor-digital multi controller(USM- DMC) using FPGA chip, A54SX72A made in Actel Corporation. By the minute, USM-DMC can control frequency, duty ratio, and phase difference of USM by llbit digital input from Pc. Therefore, when we use this controller, we can apply to typical parameter, frequency, phase difference, and voltage parameter, to control as well as we can do mixing control like phase-frequency, phase-voltage, frequency-voltage, frequency-phase-voltage, What is more, the strongest point is that it can trace frequency based on optimized frequency because we can input optimized resonant frequency while in motoring.

• KOREAN JOURNAL OF CROP SCIENCE
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• v.51 no.1
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• pp.41-47
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• 2006

To understand the heading habit of recently developed 20 Korean rice cultivars, rice plants in a phytotron were exposed to different temperature: $22.5^{\circ}C(day\;27^{\circ}C/night\;18^{\circ}C),\;27.5^{\circ}C(day\;32^{\circ}C/night\;23^{\circ}C)$, and day-length conditions: 10, 12, 13, 14, 15 hours. Four rice cultivars (Sobibyeo, Juanbyeo, Ilpumbyeo and Shindongjinbyeo) showed relatively short Basic Vegetative Phase (BVP) of 17 to 18 days, while Dasanbyeo showed the longest (35 days) BVP, compared to other remaining 15 tested cultivars which exhibited 24 to 31 days of BVP. In this experiment, it was tried out to separate the eliminable vegetative phase into photosensitivity and thermo-sensitivity with two different pathways. Many tested cultivars, however, exhibited quite different responses under low temperature and / or long day-length conditions. Especially, Surabyeo and Juanbyeo were the most difficult cultivars to separate into photo- or thermo-sensitivity in that the eliminable vegetative phase of these two cultivars increased greatly only under low temperature $(22.5^{\circ}C)$ and long day-length (15 hr.) conditions. Regarding the heading response to temperatures, tested cultivars could be categorized into 2 groups. In 1st group of rice cultivars, the eliminable vegetative phase decreased almost equally as the temperature changed from $20.0^{\circ}C\rightarrow22.5^{\circ}C\rightarrow25.0^{\circ}C\rightarrow27.5^{\circ}C$. In contrast, the 2nd group of rice cultivars exhibited eliminable vegetative phase slowly decreasing when the temperature changed from $22.5^{\circ}C\rightarrow25.0^{\circ}C\rightarrow27.5^{\circ}C$, but rapidly decreasing when the mean temperature changed from $20.0^{\circ}C\;to\;22.5^{\circ}C$. All the cultivars belonged to 2nd group, the heading date would be very delayed if cool summer comes.

• Composites Research
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• v.22 no.3
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• pp.18-28
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• 2009

Blends of poly(lactic acid) (PLA) and poly(butylene terephthalate) (PBT) were prepared by reaction extrusion with para-phenylene diisocyanate (PPDI). The crystallization behavior and biodegradability were investigated by using a differential scanning calorimeter (DSC), a wide angle X-ray diffractometer (WAXD), a contact angle goniometer, and a buffer solution containing esterase. The addition of PBT into PLA polymer matrix induced the cold crystallization of PLA phase, and the crystallization rate of PLA phase was significantly accelerated when both PBT and PPDI participated in the reaction with PLA simultaneously. But the chain extension caused by PPDI decreased the crystallinity and hydrophilicity of PLA and PBT phases. The crystallinity and hydrophilicity did not affect the biodegradability of PLA/PBT blends. However, phase separation between PLA and PBT in PLA/PBT blends increased the interfacial area exposed to the hydrolysis of enzyme, resulting in the improved degradability rate of PLA phase. In contrast, the improved interfacial adhesion between PLA and PBT matrices by the reaction with PPDI reduced the area exposed to the enzyme to decrease the degradation rate of PLA phase.

• Membrane Journal
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• v.34 no.4
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• pp.216-223
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• 2024

In comparison to commonly employed polypropylene (PP) material, polymethylpentene (PMP) exhibits low surface energy and reduced crystallinity, allowing fabrication of asymmetric membranes with a dense skin layer. However, its higher melting point poses significant challenges with respect to polymer processability. In this work, we utilized the N-TIPS method, which combines the advantages of non-solvent induced phase separation (NIPS) and thermally induced phase separation (TIPS), to fabricate PMP membranes. Cyclohexane was employed as the solvent for preparing the PMP dope solution, while water, ethanol (EtOH), and isopropanol (IPA) were used as nonsolvents. When cyclohexane-immiscible water was used as the nonsolvent, the resulting membrane exhibited TIPS morphology with unifrom pore structure but lacked suface uniformity. In contrast, when cyclohexane-miscible alcohols (EtOH, IPA) were employed, the membranes displayed NIPS morphology with a dense skin layer with higher mechanical strength. Furthermore, the effect of polyethylene glycol (PEG) as a pore forming agent was investigated to better control the surface pore size.

• Journal of the Korea Fashion and Costume Design Association
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• v.4 no.1
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• pp.143-153
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• 2002

Fashion has been analyzed and explained in diverse ways. Fashion, like every phase of culture, is a reflection of the Zeitgeist. In order to understand the changing fashion we must understand the changing society. For fashion of a period are expressions of the interrelation of the various elements of the culture, including the social and political values, the economic and industrial progress, art, the development of technology, etc... Particularly fashion is closely connected with a style of art. In a style of art, futurism focused on the "dynamism" resulting from super-speed and high-technology. This study aimed to review literatures, fashion magazines, web-site in order to know how the dynamism of futurism is expressed in modern fashion. The results of this study were as follows; 1. Dynamism was expressed by means of lines, colors, patterns through the eyesights visually. Asymmetrical oblique lines, zig-zag lines or bold cutting expressed the mechanical and offensive dynamism. In contrast, such lines as curves and spirals expressed the soft and natural dynamism. Primary colors or complementary contrast expressed energetic and rhythmical dynamism. The geometrical patterns and automobile wheels patterns expressed dynamism resulting from mechanical aesthetics. 2. Dynamism was expressed through repeat of lines, colors, patterns, and textiles. Particularly Vinyl material, fluorescent material, metallic material, beads, and spangle expressed a strong dynamism. On the other hand, natural materials, paper and other similar ones are used to signify the orientation towards a futuristic high-technology society.y society.

• Proceedings of the Korean Society of Precision Engineering Conference
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• 2003.06a
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• pp.690-693
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• 2003

Soft x-ray microscopy provides a unique set of capabilities in-between those of visible light and electron microscopy. It has long been recognized that nature provides a 'water window' spectral region between the K shell x-ray absorption edges of carbon (~290eV) and oxygen (~540eV), where organic materials show strong absorption and phase contrast, while water is relatively non-absorbing. This enables imaging of hydrated biological specimens that are several microns thick with high intrinsic contrast using x-rays with a wavelength of 2.3~4.4nm. Soft X-ray microscopy is therefore well suited to the study of specimens like single biological cells. The most direct advantage of X-ray microscope is their high spatial resolution when compared with visible light microscopes, combined with an ability to image hydrated specimens that are several microns with a minimum of preparation. Our study describes the conceptual design of soft x-ray microscope system based on a laser-based source for biomedical application with high resolution ($\leq$50nm) and short exposure time ($\leq$30sec).

• Tunnel and Underground Space
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• v.1 no.2
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• pp.181-203
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• 1991

The effects of geologic structures such as rock joins and bedding planes on the thermal conductivity of a discontinuous rock mass are studied. The expressions for the equivalent thermal conductivities of jointed rock masses are derived and found to be anisotropic. The degree of anisotropy depends primarily on the thermal properties contrast between the joint phase and surrounding intact rock, the joint density expressed as volume fraction and the inclination angle of the joint. Within the context of 2-dimensional finite element heat transfer scheme, the isotherms around a circular hole are analyzed for both the isotropic and anisotropic rock masses in 3 different thermal boundary conditions. i.e. temperature, heat flux and convection boundary conditions. The temperature in the stratified anisotripic rock mass is greatly influenced by the thermal properties of the rock formation in contact with the heat source. Using the excavation-temperature coupled elastic plastic finite element method, analyzed is the thermo-mechanical stability of a circular opening subjected to 10$0^{\circ}C$ at a depth of 527m. It is found that the thermal stress concentration was enough to deteriorate the stability and form a plastic yield zone around the opening, in contrast to the safety factor greater than 2 resulted form the excavation-only analysis.

• Korean Journal of Fisheries and Aquatic Sciences
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• v.22 no.1
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• pp.36-40
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• 1989

The eels, Anguilla japonica, were reared in a tank with daily feeding for up to 97 days, and otoliths were regularly collected for the observation of their microstructures. Microscopic observation of the thin-sectioned otolith under dark field provided significant information on daily growth increments as well as the difference in visual contrast shown by the increments. Clearly defined elver mark formed during the metamorphosis from leptocephalus to the elver can be considered as the origin of the age for the sedentary yellow eel in continental water. The close correspondence between the number of increments outside elver mark and chronological age in days from the beginning of feeding indicates that increment deposition on a daily basis was initiated with the start of feeding for the sedentary yellow eel. Either 7 or 14 daily growth increments were grouped together into 2 alternative units, each distinguished by prominent checks or by visual contrast. The absence of any apparent environmental variations with 7 or 14 day period in the reared tank implies that the phase of the moon could be a zeitgeber for the endogenous rhythm.