• Title/Summary/Keyword: Phase-Average

Search Result 2,226, Processing Time 0.031 seconds

Determination of Nitrovin in Fishery Products by Liquid Chromatography-tandem Mass Spectrometry (LC-MS/MS를 이용한 수산물 중 니트로빈의 정량분석법 개발 및 검증)

  • Kim, Joohye;Shin, Dasom;Kang, Hui-Seung;Jeong, Jiyoon;Rhee, Gyu-Seek
    • Journal of Food Hygiene and Safety
    • /
    • v.33 no.2
    • /
    • pp.118-123
    • /
    • 2018
  • The objective of this study was to develop a sensitive method for the identification and determination of nitrovin in fishery products by using a solid-phase extraction (SPE), as performed with a liquid chromatography-tandem mass spectrometry (LC-MS/MS). The samples were extracted with a mixture of acetonitrile and water, and were then defatted with acetonitrile saturated hexane, after which further clean-up was accomplished with SPE on the hydrophilic-lipophilic balance (HLB) cartridges. The analytes were subsequently ionized in the positive mode of an electrospray ionization (ESI), and where thereby detected in a process of multiple reaction monitoring (MRM). The linearity (expressed as correlation coefficients) of the matrix calibration curves was > 0.985. The limit of the quantification for the nitrovin was measured at 0.001 mg/kg. The accuracy (expressed as average recovery) was noted between 72.1 and 122%. The precision (expressed as coefficient variation) was noted from 2.9 to 16.9%. According to the CODEX CAC/GL-71 guideline accuracy, precision, linearity, and limit of detection were determined in three matrices (which were flatfish, eel and shrimp). The proposed method was suitable for analyzing the associated nitrovin residues. This application and result can also be a factor to contribute to the non-detection drugs management in fishery products.

Variation of the Sea Surface Height around the Korean Peninsula with the Use of Multi-satellite Data (Topex/Poseidon, Jason-1, ERS, Envisat) and its Association with Sea Surface Temperature (복합위성자료(Topex/Poseidon, Jason-1, ERS, Envisat)를 이용한 한반도 주변해역에서의 해수면 고도 변화와 해수면 온도의 상관성 연구)

  • Ha, Kyung-Ja;Jeong, Gi-Yong;Jang, Sae-Rom;Kim, Ki-Young
    • Korean Journal of Remote Sensing
    • /
    • v.22 no.6
    • /
    • pp.519-531
    • /
    • 2006
  • Sea surface height (SSH) around fe Korean Peninsula was investigated as a rising rate of $3.89mm\;yr^{-1}$ on the average from 1993 to 2005, which is 1.3 times higher rising rate, compared to the world ocean. In the present study, to investigate SSH changes in regional sections of the East Sea, the Yellow Sea, the South Sea, and the Korea Strait, DT-MSLA (Delayed Time-Maps of Sea Level Anomalies) with multi-satellite data (Topex/Poseidon, Jason-1, ERS, Envisat), provided by AVISO (Archiving, Validation and Interpretation of Satellite Oceanographic data), was used. The periodicity in interannual variability was dominant for $4\sim5$ year in summer, and 3 year in winter as well as an increasing trend. The amplitude and phase for the annual and semi-annual mode in SSH and SST were investigated with harmonic analysis. The geographical distribution of amplitudes for comparison of SSH and SST are slightly reverse in southwest-northeast tilted direction. The monthly SST and SSH is highly correlated correlation coefficient about 0.7 with lag of one or two months over the East Sea and the South Sea during June-August. These results suggest that the Kuroshio stream is dominant during summer over these regions.

Effect of pH on the Synthesis of $LiCoO_2$ with Malonic Acid and Its Charge/Discharge Behavior for a Lithium Secondary Battery

  • Kim, Do Hun;Jeong, Yu Deok;Kim, Sang Pil;Sim, Un Bo
    • Bulletin of the Korean Chemical Society
    • /
    • v.21 no.11
    • /
    • pp.1125-1132
    • /
    • 2000
  • The pH effect of the precursor solution on the preparation of $LiCoO_2$ by a solution phase reaction containing malonic acid was carried out. Layered $LiCoO_2$ powders were obtained with the precursors prepared at the different pHs (4, 7, and 9) and heat-treated at $700^{\circ}C(LiCoO_2-700)$ or $850^{\circ}C(LiCoO_2-850)$ in air. pHs of the media for precursor synthesis affects the charge/discharge and electrochemical properties of the $LiCoO_2electrodes.$ Upon irrespective of pH of the precursor media, X-ray diffraction spectra recorded for $LiCoO_2-850$ powder showed higher peak intensity ratio of I(003)/I(104) than that of $LiCoO_2-700$, since the better crystallization of the former crystallized better. However, $LiCoO_2$ synthesized at pH 4 displayed an abnormal higher intensity ratio of I(003)/I(104) than those synthesized at pH 7 and 9. The surface morphology of the $LiCoO_2-850$ powders was rougher and more irregular than that of $LiCoO_2-700$ made from the precursor synthesized at pH 7 and 9. The $LiCoO_2electrodes$ prepared with the precursors synthesized at pH 7 and 9 showed a better electrochemical and charge/discharge characteristics. From the AC impedance spectroscopic experiments for the electrode made from the precursor prepared in pH 7, the chemical diffusivity of Li ions (DLi+) in $Li0.58CoO_2determined$ was 2.7 ${\times}$10-8 $cm^2s-1$. A cell composed of the $LiCoO_2-700$ cathode prepared in pH 7 with Lithium metal anode reveals an initial discharge specific capacity of 119.8 mAhg-1 at a current density of 10.0 mAg-1 between 3.5 V and 4.3 V. The full-cell composed with $LiCoO_2-700$ cathode prepared in pH 7 and the Mesocarbon Pitch-based Carbon Fiber (MPCF) anode separated by a Cellgard 2400 membrane showed a good cycleability. In addition, it was operated over 100 charge/discharge cycles and displayed an average reversible capacity of nearly 130 mAhg-1.

Thermoelectric Properties of Sb Deficiency N-Type Skutterudite Co4Sb12 (Sb가 결핍된 N형 Skutterudite Co4Sb12의 열전 특성)

  • Tak, Jang-Yeul;Van Du, Nguyen;Jeong, Min Seok;Lee, NaYoung;Nam, Woo Hyun;Seo, Won-Seon;Cho, Jung Young
    • Journal of the Korean Institute of Electrical and Electronic Material Engineers
    • /
    • v.32 no.6
    • /
    • pp.496-500
    • /
    • 2019
  • In this study, we investigate the effect of an Sb-deficiency on the thermoelectric properties of double-filled n-type skutterudite ($In_{0.05}Yb_{0.15}Co_4Sb_{12-x}$). Samples were prepared by encapsulated induction melting, consecutive long-time annealing, and finally spark plasma sintering processes. The Sb-deficient sample contained a $CoSb_2$ secondary phase. Both the double-filled n-type skutterudite pristine and Sb-deficient samples showed metallic behavior in electrical conductivity with increasing temperature. The carrier concentration of the Sb-deficient sample decreased compared with that of the pristine sample. Due to a decrease in carrier concentration, the Sb deficient sample showed decreased electrical conductivity and an increased Seebeck coefficient compared with the conductivity and coefficient of the pristine sample. Furthermore, the Sb deficient sample showed an increase in the power factor (${\sigma}{\cdot}S^2$); the power factor maximum shifted to athe lower temperature side than ones of the pristine sample. As a result, the Sb-deficient sample represents an improved average figure of merit (ZT) and a $ZT_{max}$ temperature lower than that of the pristine sample. Therefore, we propose that Sb-deficient double-filled n-type skutterudite thermoelectric material ($In_{0.05}Yb_{0.15}Co_4Sb_{12-x}$) be used in the 573~673 K temperature range.

The Processing control of NiCuZn Ferrite (I) - Mixing and Size Reduction of Raw Materials by Wet Ball Milling. (NiCuZn Ferrite의 제조공정 제어 (제1보) - 습식 볼밀링에 의한 다성분 원료의 혼합 및 분쇄 공정의 고찰)

  • 류병환;김선희;최경숙;고재천
    • Journal of the Korean Magnetics Society
    • /
    • v.5 no.6
    • /
    • pp.928-936
    • /
    • 1995
  • In this research, the processing control of NiCuZn Ferrite has been developed. The mixing and the size reduction of raw materials have been proceeded. In order to produce NiCuZn Ferrite, highly concentrated slurry with fixed ratio and wet ball milling were used. First, the dispersion behavior of raw mixture at the region of pH4~pH11 has been studied. Using wet ball milling operation, the best conditions of mixing and size reduction have been determined. Further more, the most suitable conditions, such as, dispersant kind, dispersant amount, milling time, and slurry concentration have been studied. The poly acrylic ammonium salt (PAN) was chosen as a suitable dispersant to have effective dispersion in basic region. The slurry of raw mixture without dispersant, showed high viscosity and poor grindability. As 0.7 wt% of PAN was added, the concentrated slurry (up to 55 vol%) was possible, and showed well grindability. After 18 h ball milling of 30 vol% of mixture slurry with 0.7 wt% of PAN, the average particle size and specific surface area of raw mixture were $0.54\mu\textrm{m}$ and $12.92m^{2}/cc$, respectively. The ball milled raw mixture, calcined at $700^{\circ}C$ for 3h, was totally changed into NiCuZn Ferrite with spinel phase.

  • PDF

Development of 1×16 Thermo-optic MZI Switch Using Multimode Interference Coupler (다중모드 간섭현상을 이용한 1×16 마하젠더 스위치 개발)

  • Kim, Sung-Won;Hong, Jong-Kyun;Lee, Sang-Sun
    • Korean Journal of Optics and Photonics
    • /
    • v.17 no.5
    • /
    • pp.469-474
    • /
    • 2006
  • A $1{\times}16$ thermo-optic switch with small excess loss using multimode interference(MMI) couplers is designed, fabricated, and measured. This paper introduces the proposed $1{\times}16$ thermo-optic switch, and discusses the measurement results. The $1{\times}16$ thermo-optic switch is farmed as 4-stage which consists of 15 unit devices. The unit devices are the $2{\times}2$ thermo-optic switches with Mach-Zehnder interferometer(MZI) structure. The characteristics of the $1{\times}16$ thermo-optic switch depends strongly on each unit device. The unit deviceconsists of two 3-dB general interference MMI couplers and two single mode waveguide arms as a phase shifter. First of all, the 3-dB optical splitter and $2{\times}2$ MZI thermo-optic switch have been tested to confirm the characteristics of the unit devices of the $1{\times}16$ MZI thermo-optic switch. Using the measurement results of the unit devices, the $1{\times}16$ MZI thermo-optic switch can be produced with better characteristics. The resultant structure of the MMI coupler with the optical light source of wavelength of 1550nm for the $1{\times}16$ thermo-optic switch is that the width and the optimized length are $25{\mu}m\;and\;1580{\mu}m$, respectively. The smallest excess loss fur the unit device is -0.5dB and the average excess loss is -0.7dB.

Analysis of Causes and Impact of Change Orders in the U.S. Military Construction Projects (미군 시설공사 설계변경 요인과 영향에 대한 연구)

  • Park, Insung;Kim, Harim;Lee, Hak-Ju;Kim, Do-Hyung;Min, Yoon-Gi;Cho, Hunhee
    • Journal of the Korea Institute of Building Construction
    • /
    • v.21 no.3
    • /
    • pp.213-219
    • /
    • 2021
  • Change orders that occur frequently during the construction phase, af ect the construction performance in terms of cost, time, quality, safety and environment, and place a huge burden for stakeholders of given projects. This study analyzed the causes of change orders and their impact on the basis of 721 cases and a questionnaire of 164 domestic U.S. military construction participants in a total of 24 U.S. military projects. Important factors for change orders in the US military construction projects were engineering change due to design errors (348 cases, 48.3%), user requests change(86 cases, 11.9%), and different site conditions (69 cases, 9.6%). In addition, due to the change orders, construction cost increased by 6.56% on average and construction period was extended by 21.1% compared to the original schedule. As a result, it is anticipated that domestic construction companies can obtain a better understanding of change orders and construction performance, which may be difficult due to accessibility and limitations to military facilities. Also, it is proposed a successor study that guides in the right direction for the U.S. Military Construction.

Scan Matching based De-skewing Algorithm for 2D Indoor PCD captured from Mobile Laser Scanning (스캔 매칭 기반 실내 2차원 PCD de-skewing 알고리즘)

  • Kang, Nam-woo;Sa, Se-Won;Ryu, Min Woo;Oh, Sangmin;Lee, Chanwoo;Cho, Hunhee;Park, Insung
    • Korean Journal of Construction Engineering and Management
    • /
    • v.22 no.3
    • /
    • pp.40-51
    • /
    • 2021
  • MLS (Mobile Laser Scanning) which is a scanning method done by moving the LiDAR (Light Detection and Ranging) is widely employed to capture indoor PCD (Point Cloud Data) for floor plan generation in the AEC (Architecture, Engineering, and Construction) industry. The movement and rotation of LiDAR in the scanning phase cause deformation (i.e. skew) of PCD and impose a significant impact on quality of output. Thus, a de-skewing method is required to increase the accuracy of geometric representation. De-skewing methods which use position and pose information of LiDAR collected by IMU (Inertial Measurement Unit) have been mainly developed to refine the PCD. However, the existing methods have limitations on de-skewing PCD without IMU. In this study, a novel algorithm for de-skewing 2D PCD captured from MLS without IMU is presented. The algorithm de-skews PCD using scan matching between points captured from adjacent scan positions. Based on the comparison of the deskewed floor plan with the benchmark derived from TLS (Terrestrial Laser Scanning), the performance of proposed algorithm is verified by reducing the average mismatched area 49.82%. The result of this study shows that the accurate floor plan is generated by the de-skewing algorithm without IMU.

Study on the Cultural Marketing Factors of Tourism Destination in the Era of Convergence : Focusing on the Brand Attitude and Brand Equity Differences by segmented groups (융복합시대의 관광지 문화마케팅에 관한 연구 : 세분집단별 브랜드태도 및 자산 인식 차이를 중심으로)

  • Yoon, Yeong Hye;Kim, Mi Seong;Kang, Hwa;Yoon, Yoo Shik
    • Korea Science and Art Forum
    • /
    • v.37 no.2
    • /
    • pp.205-217
    • /
    • 2019
  • This study began with the focusing the growth of importance of cultural marketing and its successes by applying to branding in a phase in which the cultural production era has arrived after the industrial production era. This study aimed to reveal the effect of cultural marketing, which are used as marketing strategy in the tourism field, on brand attitude and awareness. Therefore, this study tried to investigate the brand equity and attitude in accordance with the cultural marketing factors by survey Chinese tourists visiting Korea. The result and contents of the study are as follows. First, it was confirmed that the research question on the possibility of market segmentation in accordance with cultural marketing factors; the market segments were classified as Cluster 1 general involvement perceived group, Cluster 2 high involvement perceived group, Cluster3 middle involvement perceived group. Second, it revealed significant differences on brand attitude among the segments; Cluster 2 showed high brand attitude and Cluster 3 showed average level on brand attitude. Third, it found a statistically significant differences in the perception of brand equity including perceived quality, brand awareness and brand image of tourism destination. In conclusion, this study was able to identify market segments in accordance with cultural marketing factors of tourism destination and revealed significant differences in the segments by brand attitude and brand equity. This could provide practical implication that various cultural marketing activities to generate positive results on brand equity and brand attitude and cultural marketing strategies is also needed to increase foreign tourists' awareness of these cultural marketing activities.

Induction Heating of Cylinderical MoSi2-based Susceptor (실린더형 MoSi2계 발열체의 유도가열 적용)

  • Lee, Sung-Chul;Kim, Yo Han;Myung, Jae-ha;Kim, Bae-Yeon
    • Korean Chemical Engineering Research
    • /
    • v.57 no.4
    • /
    • pp.553-558
    • /
    • 2019
  • In present study, the cylindrical susceptor by the slip casting method was designed to apply high-temperature induction heating by using $(Mo,W)Si_2$ ceramics. $MoSi_2$-based materials were synthesized by SHS (Self-propagating High-temperature Synthesis) method. The phase and crystal structure of $MoSi_2$-based materials were confirmed by XRD analysis. The shape of cylindrical mold was synthesized for various thickness by using the slip casting method. Finally, the susceptor for induction heating was processed by sintering and heat treatment to form $SiO_2$ layer, which was confirmed on the surface of susceptor by SEM/EDS analysis. To evaluate the heating performance of $(Mo,W)Si_2$ cylinder susceptor, we measured the maximum surface temperature and heating rate in comparison with the rod heating element under constantly applied power. The induction heating of the $(Mo,W)Si_2$ cylinder showed excellent heating performance, reaches the maximum temperature of $1457^{\circ}C$, with the average heating rate of $19^{\circ}C/s$ at 2 kW