• Title/Summary/Keyword: Phase variation

검색결과 2,040건 처리시간 0.027초

HPLC Analysis of Organic Acids, Phenol, and Benzopyrene in Wood Vinegar (HPLC에 의한 목초액 중의 유기산, 페놀 및 벤조피렌의 분석법 개발)

  • Lee, Gye-Won;Kim, A-Ram;Cho, Jae-Soo
    • YAKHAK HOEJI
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    • 제52권1호
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    • pp.12-19
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    • 2008
  • The organic acids (formic acid, acetic acid and propionic acid), phenol and benzopyrene in wood vinegar were determine by HPLC. An $Atlantis^{TM}dC_{18}$ column with a acetonitrile: 0.1% phosphoric acid (5: 95, organic acids), acetonitrile: water (10 : 90, phenol), 100% acetonitrile (benzopyrene) as a mobile phase was used. Retention time of acetic acid, formic acid, propionic acid, phenol and benzopyrene was 4.77, 3.73, 9.08, 30.97 and 6.10 min, respectively. The calibration curves of organic acids, phenol, benzopyrene were linear over the concentration range of $30{\sim}500,\;60{\sim}1000$, and $3{\sim}50\;{\mu}g/ml$ with correlation coefficient of above 0.999. The limit of detection (LOD) and limit of quantitation (LOQ) of acetic acid, formic acid, propionic acid, phenol, and benzopyrene was 1.71 and 5.19, 1.11 and 3.35, 4.87 and 14.74, 6.45 and 19.55, 0.08 and $0.24\;{\mu}g/ml$, respectively. The coefficients of variation for intra- and inter-day assay were $0.21{\sim}4.14$ and $0.07{\sim}1.19%$, respectively and the precision was $95{\sim}115%$. From this study, we suggest that HPLC is suitable method for the determination of organics in wood vinegar and could be applied to quality control of wood vinegar.

ULF electromagnetic variation associated with seismic wave (지진파에 의해 발생하는 ULF 전자기장 변동)

  • Lee Heuisoon;Lee Choon-Ki;Kwon Byung-Doo;Yang Jun-Mo;Oh Seokhoon;Song Yoonho;Lee Tae Jong;Uchida Toshihiro
    • 한국지구물리탐사학회:학술대회논문집
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    • 한국지구물리탐사학회 2005년도 공동학술대회 논문집
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    • pp.197-202
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    • 2005
  • The electromagnetic signals associated with the seismic activity in the south-east offshore of Kii peninsula, Japan, were clearly recorded at the MT sites in Jeju island, Korea. In this research, we have identified the co-seismic electromagnetic signals associated with the seismic activity and have analyzed the characteristics of significant electromagnetic variations. The analysis of phase velocity, power spectral density, MT impedance and polarization direction shows that the significant earthquake signals have the frequency band of about 0.05 to 0.5 Hz and that the sources of electromagnetic field are local effects of passing seismic waves. The simple approximation using electrokinetic effect successfully explains the co-seismic EM signals coincides with measured data but cannot explain the localities of electromagnetic variations.

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A Study on Laser Assisted Machining for Silicon Nitride Ceramics (III) - Variation of the Main Cutting Force and Life of Cutting Tool by LAM of SSN and HIPSN - (질화규소 세라믹의 레이저 예열선삭에 관한 연구 (III) - SSN 및 HIPSN의 예열선삭시 절삭력 및 공구수명의 특성 -)

  • Kim, Jong-Do;Lee, Su-Jin;Kang, Tae-Young;Suh, Jeong;Lee, Jae-Hoon
    • Journal of Welding and Joining
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    • 제28권6호
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    • pp.35-39
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    • 2010
  • Generally, ceramic material is very difficult to machine due to high strength and hardness. However, ceramic material can be machined at high temperature by plastic flow as metallic material due to the deterioration of the grain boundary glassy phase. Recently, a new method was developed to execute cutting process with CBN cutting tool by local heating of surface with laser. There are various parameters in LAM because it is a complex process with laser treatment and machining. During laser assisted machining, high power results in reducing of cutting force and increasing tool life, but excessive power brings oxidation of the surface. The effect of laser power, feed rate, cutting depth and etc. were investigated on the life of cutting tool. Chips were observed to find out suitable machining conditions. Chips of SSN had more flow-types than HIPSN. It means SSN is easier to machining. The life of cutting tool was increased with increasing laser power and decreasing feed rate and cutting depth.

Factors Affecting Agrobacterium tumefaciens-mediated Transformation of Panax ginseng C.A. Meyer

  • Kim, Ok-Tae;Jung, Su-Jin;Bang, Kyong-Hwan;Kim, Young-Chang;Shin, Yu-Su;Sung, Jung-Sook;Park, Chun-Geon;Seong, Nak-Sul;Cha, Seon-Woo;Park, Hee-Woon
    • Korean Journal of Medicinal Crop Science
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    • 제15권2호
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    • pp.100-104
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    • 2007
  • A protocol for the production of transgenic Panax ginseng C.A. Meyer was established via Agrobacterium tumefaciens-mediated genetic transformation of direct somatic embryos. A number of conditions related to the co-cultivation were tested with respect to maximizing transformation efficiency. The results showed that pH of the co-cultivation medium (5.7), the bacterial growth phase (optical density; $OD_{600}$ = 0.8), co-cultivation period (3 days), and acetosyringone concentration $(100\;{\mu}M)$ had positive effects on transformation. Selected plantlets were cultured on the medium at an elevated hygromycin level(30 mg/l). Integration of the transgenes into the P. ginseng nuclear genome was confirmed by PCR analysis using hpt primers and by Southern hybridization using hpt-specific probe. The transgenic plantlets were obtained after 3-month cultivation and did not show any detectable variation in morphology or growth characteristics compared to wild-type plants.

An analysis on the Earth geoid surface variation effect for use of the tilt sensor in celestial navigation system

  • Suk, Byong-Suk;Yoon, Jae-Cheol;Lyou, Joon
    • 제어로봇시스템학회:학술대회논문집
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    • 제어로봇시스템학회 2005년도 ICCAS
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    • pp.1867-1870
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    • 2005
  • The celestial navigation is one of alternatives to GPS system and can be used as a backup of GPS. In the celestial navigation system using more than two star trackers, the vehicle's ground position can be solved based on the star trackers' attitude information if the vehicle's local vertical or horizontal angle is given. In order to determine accurate ground position of flight vehicle, the high accurate local vertical angle measurement is one of the most important factors for navigation performance. In this paper, the Earth geophysical deflection was analyzed in the assumption of using the modern electrolyte tilt sensor as a local vertical sensor for celestial navigation system. According to the tilt sensor principle, the sensor measures the tilt angle from gravity direction which depends on the Earth geoid surface at a given position. In order to determine the local vertical angle from tilt sensor measurement, the relationship between the direction of gravity and the direction of the Earth center should be analyzed. Using a precision orbit determination software which includes the JGM-3 Earth geoid model, the direction of the Earth center and the direction of gravity are extracted and analyzed. Appling vector inner product and cross product to the both extracted vectors, the magnitude and phase of deflection angle between the direction of gravity and the direction of the Earth center are achieved successfully. And the result shows that the angle differences vary as a function of latitude and altitude. The maximum 0.094$^{circ}$angle difference occurs at 45$^{circ}$latitude in case of 1000 Km altitude condition.

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Flood Runoff Analysis of Small River Basin using Geographic Information System (지리정보시스템을 이용한 소하천유역의 홍수유출 해석)

  • Lee, Yeon-Kil;Park, Sung-Chun;Lee, Kwan-Soo
    • Journal of the Korean Association of Geographic Information Studies
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    • 제6권1호
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    • pp.24-36
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    • 2003
  • Many rainfall-runoff model, which is applied discharge calculation for effective water-resource planning and management needs topographic and parameter of basin character. But it is very difficult to apply real a phase. Accordingly in this study filling up these problems. Applying GIS(geographic information system) through environment creating input data or concerning with GIS and rainfall runoff model. We built environment that analyze hydrograph showing discharge variation by time. GIS software for constructing input data is used by ArcView. For analysis of hydrograph in Basin, TOPMODEL applied topographic index. Besides for estimate of appliance to rainfall-runoff model, simple storm event and complex storm event are applied rainfall data which was before.

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Immune Responses to Viral Infection (바이러스 감염에 대한 면역반응)

  • Hwang, Eung-Soo;Park, Chung-Gyu;Cha, Chang-Yong
    • IMMUNE NETWORK
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    • 제4권2호
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    • pp.73-80
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    • 2004
  • Viruses are obligate intracellular parasites which cause infection by invading and replicating within cells. The immune system has mechanisms which can attack the virus in extracellular and intracellular phase of life cycle, and which involve both non-specific and specific effectors. The survival of viruses depends on the survival of their hosts, and therefore the immune system and viruses have evolved together. Immune responses to viral infection may be variable depending on the site of infection, the mechanism of cell-to-cell spread of virus, physiology of the host, host genetic variation, and environmental condition. Viral infection of cells directly stimulates the production of interferons and they induce antiviral state in the surrounding cells. Complement system is also involved in the elimination of viruses and establishes the first line of defence with other non-specific immunity. During the course of viral infection, antibody is most effective at an early stage, especially before the virus enters its target cells. The virus- specific cytotoxic T lymphocytes are the principal effector cells in clearing established viral infections. But many viruses have resistant mechanism to host immune responses in every step of viral infection to cells. Some viruses have immune evasion mechanism and establish latency or persistency indefinitely. Furthermore antibodies to some viruses can enhance the disease by the second infection. Immune responses to viral infection are very different from those to bacterial infection.

Effects of Mn, Cr and Co on the Magnetic Properties of Fe-Ni Invar Alloys (Fe-Ni 인바합금의 자기적성질에 미치는 Mn, Cr 및 Co의 첨가효과)

  • 이종현;김희중;강일구;김학신
    • Journal of the Korean Magnetics Society
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    • 제3권1호
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    • pp.7-12
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    • 1993
  • The effects of Mn, Cr or Co addItion on the magnetic properties of Fe-Ni Invar alloys were investigated. The composition range of the three additives is up to 5wt%. In the temperature range of room temperature-$250^{\circ}C$, the variation of specific magnetization with the addition of Mn, Cr or Co in the Fe-Ni alloys except for 5wt% Co shows the phenomenon characteristics of the Invar effect, viz., the specific magnetization decreases very abrubtly with the temperature and the dependence of temperature on the specific magnetization is in the mixed form of $T^{3/2}$ and $T^{2}$. In the room temperature, the amount of increase in the specific magnetization, Curie temperature and coercivity is in order of Co > Cr > Mn. In the case of 5wt% Co an anomalous phenomena were observed due to the occurrance of ferromagnetic $\alpha$ phase which reduces the invar effect.

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Mechanical Constitutive Model for Frozen Soil (동토지반에 대한 역학적 구성모델)

  • Shin, Ho-Sung;Kim, Ji-Min;Lee, Jang-Guen;Lee, Seung-Rae
    • Journal of the Korean Geotechnical Society
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    • 제28권5호
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    • pp.85-94
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    • 2012
  • Recently, growing interests in frozen ground have stimulated us to advance fundamental theories and systematic researches on soil behavior under freezing conditions. Unlike the well-established soil mechanics theory, temperature variation and phase change of pore-water cause water migration to cold side, ground heaving, sharp increase in earth pressure, etc., which bring about serious problems in frozen geotechnical structures. Elasto-plastic mechanical constitutive model for frozen/unfrozen soil subjected to fully coupled THM phenomena is formulated based on a new stress variable that is continuous in frozen-unfrozen transitional regions. Numerical simulations are conducted to discuss numerical reliability and applicability of the developed constitutive model: one-dimensional heaving pressure, tri-axial compression test, and one-side freezing tests. The numerical results show that developed model can efficiently describe complex THM phenomena of frozen soil, and they can be utilized to analyze and design the geotechnical structures under freezing conditions, and predict their long-term behavior.

Estimation of Emission Factor (Residual Rate) and Inventory of HFC-134a from Mobile Air Conditioners of Scrap Truck (폐트럭으로부터 온실가스 HFC-134a의 탈루배출계수와 인벤토리 산정에 대한 연구)

  • Kim, Eui-Kun;Kim, Seungdo;Kim, Hyerim;Lee, Young Phyo;Byun, Seokho;Lee, Dong Won
    • Journal of Environmental Science International
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    • 제22권9호
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    • pp.1105-1113
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    • 2013
  • This paper attempted to estimate the emissions of HFC-134a from scrap truck as a result of measuring the residual quantities of HFC-134a in air conditioner of scrap truck. We measured the residual amounts in the scrap truck of 138 by applying commercial recover for refrigerants. The average residual rate(disposal-phase emission factor) is reported to be $44.3{\pm}3.3%$ within a confidence interval of 95%. Recent year model trucks exhibit the higher residual rates. Little variation, however, is observed in regard to vehicle size. The HFC-134a emission quantity from scrap truck in 2011 is estimated to be 55,908 $tCO_2$-eq that demonstrates 21.4% increase to compare with that in 2007. As the numbers of truck have increased dramatically during the last two decades, the emissions of HFC-134a from scrap truck would increase sharply in the next coming years. HFC-134a is a very high GWP greenhouse gas. therefore have to reduce the emissions from the scrap truck and need to find ways to recycle. The chemical compositions of refrigerants from scrap truck are quite similar to those of new refrigerants, suggesting that the refrigerants from scrap truck could be reused as refrigerant.