• Title/Summary/Keyword: Phase sensitive method

Search Result 385, Processing Time 0.027 seconds

Surface profiling by the phase shifting method in fiber-optical confocal scanning interference microscopes (광섬유 공초점 간섭 현미경과 위상 변위법을 결합한 표면 검색)

  • 김대찬;이승걸
    • Korean Journal of Optics and Photonics
    • /
    • v.10 no.3
    • /
    • pp.201-207
    • /
    • 1999
  • The fiber-optical confocal scanning interference microscope with a simple configuration was constructed with a 4-port fiber-optic coupler, and the new method based on the phase shifting method was proposed for surface profiling by the system. In the method, the height of a specimen was determined from the phase of confocal beam. It was verified experimentally that the method was applicable to even the confocal interference microscope with a long-wavelength source and a low NA objective, and that the scanning time could be drastically reduced compared with the conventional method. Finally, it was found that our method is less sensitive to the variation of surface reflectivity than the conventional method.

  • PDF

HPLC를 이용한 Lysozyme chloride의 함량분석에 관한 연구

  • Lee, Jeong-Sook;Chae, Yong-Zoo
    • Proceedings of the PSK Conference
    • /
    • 2003.04a
    • /
    • pp.289.2-289.2
    • /
    • 2003
  • The aim of this work was to develop an reverse-phase method for the analysis lysozyme contents. This method was sensitive and reproducible. The experimental samples were 8 kinds of capsules and one tablet. collected in domestic area. The results were summarized as follows. (omitted)

  • PDF

IMPROVEMENT OF A SEMI-IMPLICIT TWO-PHASE FLOW SOLVER ON UNSTRUCTURED MESHES (비정렬 격자계에서의 물-기체 2상 유동해석코드 수치 기법 개선)

  • Lee, H.D.;Jeong, J.J.;Cho, H.K.;Kwon, O.J.
    • 한국전산유체공학회:학술대회논문집
    • /
    • 2010.05a
    • /
    • pp.380-388
    • /
    • 2010
  • A thermal-hydraulic code, named CUPID, has been developed for the analysis of transient two-phase flows in nuclear reactor components. A two-fluid three-field model was used for steam-water two-phase flows. To obtain numerical solutions, the finite volume method was applied over unstructured cell-centered meshes. In steam-water two-phase flows, a phase change, i.e., evaporation of condensation, results in a great change in the flow field because of substantial density difference between liquid and vapor phases. Thus, two-phase flows are very sensitive to the local pressure that determines the phase change. This in turn puts emphasis on the accurate evaluation of local pressure gradient. This paper presents a new numerical scheme to evaluate the pressure gradient at cell centers on unstructured meshes. The results of the new scheme for a simple test function a gravity-driven cavity, and a wall boiling two-phase flow are compared with those of the previous schemes in the cupid code.

  • PDF

Optimization of Manufacturing Conditions of Pressure-Sensitive Ink Based on MWCNTs (MWCNTs 기반 인쇄형 압력감응잉크의 제조 조건 최적화)

  • Park, Sung-Chul;Lee, In-Hwan;Bae, Yong-Hwan;Kim, Ho-chan
    • Journal of the Korean Society of Manufacturing Process Engineers
    • /
    • v.18 no.8
    • /
    • pp.1-7
    • /
    • 2019
  • Materials that can be used for 3D printing have been developed in terms of phase and functionality. Materials should also be easily printed with high accuracy. In recent years, the concept of 4D printing has been extended to materials whose physical properties such as shape or volume can change depending on the environment. Typically, such high-performance 3D printing materials include bio-inks and inks for sensors. This study deals with the optimization of the manufacturing method to improve the functional properties of the pressure sensitive material, which can be used as a sensor based on change of the resistance according to the pressure. Specifically, the number of milling for dispersion, the ratio of hardener for controlling elasticity, and the content of MWCNTs were optimized. As a result, a method of manufacturing a highly sensitive pressure-sensitive ink capable of use in 3D printing was introduced.

Cherent Detection of the Trellis Coded CPFSK on Phase Jitter Channels (위상 지터 채널하에서 트렐리스 부호화된 CPFSK의 동기 검파)

  • 김대중;김한종;정호영;강창언
    • Journal of the Korean Institute of Telematics and Electronics A
    • /
    • v.31A no.9
    • /
    • pp.26-33
    • /
    • 1994
  • In this paper, the performance of the trellis coded CPFSK with the coherent detection over mobile communication channels is calculated. The characteristics of channels, including phase jitter effects and fading effects, are examined and modeled. The phase jitter channel is modeled to have a nonzero mean and a gaussian distribution. The fading channel has a Rayleigh distribution in the multipath. For the optimal decoding method(MLSE), the Viterbi algorithm is used for the trellis structure of trellis coded CPFSK. The results indicate that the trellis coded CPFSK with a small moulation indes gets more sensitive, as the index gets smaller, to the phase noise under the phase jitter channel. Using the interleaving method. It gives considerable improvements in the error rate under the fading channel.

  • PDF

Sensitive Determination of Felodipine in Human Plasma by LC-MS/MS

  • Kim, Ho-Hyun;Roh, Hyeon-Jin;Lee, He-Joo;Han, Sang-Beom
    • Proceedings of the PSK Conference
    • /
    • 2003.04a
    • /
    • pp.283.2-283.2
    • /
    • 2003
  • This study established a highly sensitive novel quantification method for detecting felodipine in human plasma using LC-MS/MS. The mobile phase used after degassing was composed of 1 mM ammonium acetate and acetonitrile (20:80, pH 6.0), with flow rate of 200 uL/min. One mL plasma were pipetted into glass tubes and spiked with 0.1 mL of internal standard solution. (omitted)

  • PDF

HPLC Method for the Determination of Nicorandil in Human Plasma

  • Park, Sun-Hee;Shin, In-Chul
    • Biomolecules & Therapeutics
    • /
    • v.16 no.2
    • /
    • pp.168-172
    • /
    • 2008
  • The present study is to determine of sensitive nicorandil analysis method using HPLC and measure the pharmacokinetics parameters (bioavailability, $C_{max}$, $T_{max}$, Ke, $T_{1/2}$) of nicorandil (5 mg, Tab; Choongwae Pharma Corporation). Plasma (500 ul) was mixed with furosemide (internal standard, 500 ug/ml). Detection wavelength was 256 nm. The mixture of 0.01 M ammonium acetate and acetonitrile 80:20 (v/v) was used mobile phase. The HPLC separation was accomplished on ODC reverse HPLC column. The nicorandil was analyzed by a HPLC system, which consists of CAPCELL PAK C18 column (5 ${\mu}$m, 4.6 × 150 mm) and a chromatography data analysis S/W, using a isocratic mobile phase (mixture of 0.01 M ammonium acetate and acetonitrile 80:20 ) at 1.0 ml/min. Its sensitivity, selectivity, accuracy and precision must be adequate for the bioavailabilty study of nicorandil, and the linearity ($r^2$ ≥ 0.9994) of nicorandil was also proved in the range of 0.05 ug/ml . 3 ug/ml. The pharmacokinetic parameters of nicorandil (5 mg) tablets were measured as the follow. AUC: 0.19 ug/ml·hr, $C_{max}$: 0.14 ug/ml, $t_{max}$: 0.58 hr, Ke: 0.11 hr., $t_{1/2\beta}$: 6.76 hrs. This method is simple and sensitive HPLC method using UV detector for determination of nicorandil in human plasma.

Simultaneous Determination of Abamectin and Milbemectin Residues in Fruits

  • Lee, Young-Deuk;Kwon, Chan-Hyeok
    • Journal of Applied Biological Chemistry
    • /
    • v.43 no.2
    • /
    • pp.94-100
    • /
    • 2000
  • An analytical method was developed to determine abamectin and milbemectin residues in apple, pear, and citrus using HPLC with ultraviolet absorption detection. Abamectin and milbemectin were extracted with methanol from apple, pear, and citrus samples. The extract was diluted with saline water and dichloromethane partition was followed to recover the compounds from the aqueous phase. Florisil column chromatography and aminopropyl solid-phase extraction were employed as cleanup methods to remove most of co-extractives from the sample extract. Reverse-phase HPLC using an octadecylsilyl column was successfully applied to separate and quantitate abamectin and milbemectin residues in sample extracts at the wavelength of 245 nm. Recoveries of abamectin and milbemectin from fortified samples ranged 80.4~90.3% and 90.9~96.8%, respectively. Relative standard deviations of the analytical method were less than 10% for both acaricides. Detection limit of the analytical method was 0.003 mg/kg sample for all the analytes. The proposed method was reproducible and sensitive enough to evaluate terminal residues of abamectin and milbemectin in apple, pear, and citrus.

  • PDF

Measurement of magnetic kerr rotation and faraday fotation angles by polarization modulation method (편광 변조 방법에 의한 자기 Kerr 회전각 및 Faraday 회전각 측정)

  • 이용호;이상수;이용호
    • Korean Journal of Optics and Photonics
    • /
    • v.3 no.2
    • /
    • pp.105-110
    • /
    • 1992
  • In order to measure fine rotation angles by magneto-optic effects of magneto-optical recording thin films, a polarization modulation method is used. In the experiment, the polarization of laser (He-Ne laser) beam is modulated by a Faraday rotator and the amplified modulated signals are selectively detected by phase sensitive detector. The magnetic Kerr rotation and Faraday rotation hysteresis loops are investigated by this method for thermally evaporated amorphous TbFeCo thin films and RF sputtered garnet thin films. Rotation angles about $0.25^{\circ}$ are measured easily from TaFeCo thin films. In the case of longitudinal Kerr rotation, very small rotation angle of $2.5\times10^{-3^\circ}$ is measured with good accuracy of the measurement (about $1\times10^{-3^\circ}$). And it is found that each thin films have the hysteresis curves of high coercivity and good squareness.

  • PDF