• Title/Summary/Keyword: Phase boundaries

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A Study on Two Dimensional Phase Change Problem (상변화 축열계의 비정상 해석)

  • Won, Sung-Pil;Ro, Sung-Tack
    • The Magazine of the Society of Air-Conditioning and Refrigerating Engineers of Korea
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    • v.10 no.1
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    • pp.12-21
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    • 1981
  • The Enthalpy Model was verified in order to analyze two- dimensional phase change problems. By using the Enthalpy Model, interface locations, frozen fraction rates, heat flux distribution rut cooled surfaces, and surface-integrated heat flux were purely numerically calculated in rectangular thermal storage units, whose initial condition was saturated liquid and phase change material was cooled on its boundaries by convective heat transfer. The calculations were performed for various Stefan numbers and Biot numbers. The effect on those dimensionless numbers were explained.

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Dissolution on the Surface of Bioceramics Prepared by Commercial Calcium Phosphate Powders (상용 인산칼슘계 분말로 제조된 생체세라믹스의 표면용해 특성)

  • Seo D. S;Kim H;Lee J. K
    • Korean Journal of Materials Research
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    • v.14 no.1
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    • pp.35-40
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    • 2004
  • In this study, dissolution characteristics of four types of commercial calcium phosphate ceramics were investigated in distilled water with respect to chemical composition and microstructure. For all samples, no significant damage was observed after 3 days of immersion. Following the 7 days of immersion, surface dissolution of the ceramics containing a crystalline phase susceptible to water such as TCP, even pure hydroxyapatite, was initiated at grain boundaries and the dissolution was extended interior to the material along the grain boundaries. In the considerably dissolved area, there was grain separation followed by the formation of 20 $\mu\textrm{m}$ of cavities. In at least one case, the residual pores on the surface appeared to initiate dissolution. In a dissolved area, a crack during the fracture propagates along the grain boundaries resulting in intergranular fracture, while transgranular fracture occurs in a dense area without significant dissolution.

A Modified Viterbi Algorithm for Word Boundary Detection Error Compensation (단어 경계 검출 오류 보정을 위한 수정된 비터비 알고리즘)

  • Chung, Hoon;Chung, Ik-Joo
    • The Journal of the Acoustical Society of Korea
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    • v.26 no.1E
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    • pp.21-26
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    • 2007
  • In this paper, we propose a modified Viterbi algorithm to compensate for endpoint detection error during the decoding phase of an isolated word recognition task. Since the conventional Viterbi algorithm explores only the search space whose boundaries are fixed to the endpoints of the segmented utterance by the endpoint detector, the recognition performance is highly dependent on the accuracy level of endpoint detection. Inaccurately segmented word boundaries lead directly to recognition error. In order to relax the degradation of recognition accuracy due to endpoint detection error, we describe an unconstrained search of word boundaries and present an algorithm to explore the search space with efficiency. The proposed algorithm was evaluated by performing a variety of simulated endpoint detection error cases on an isolated word recognition task. The proposed algorithm reduced the Word Error Rate (WER) considerably, from 84.4% to 10.6%, while consuming only a little more computation power.

Magnetic NDE for Sensitization of Inconel 600 Alloy

  • Kikuchi, Hiroaki;Sumimoto, Takaki;Kamada, Yasuhiro;Kobayashi, Satoru
    • Journal of Magnetics
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    • v.18 no.3
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    • pp.348-351
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    • 2013
  • Inconel 600 alloy, Ni base alloy, is widely used for steam generator tubings where sensitization occurs at grain boundaries and sensitization will induce tubing failures. This alloy has usually paramagnetic property, however, it transforms into ferromagnetic property along grain boundaries when sensitization occurs: this means NDE using magnetism for sensitization is possible. Therefore, in this study, Inconel 600 alloys were heat treated at 873 K from 0 to 400 hours so as to generate sensitization and their magnetic properties were investigated in detail. The saturation and the residual magnetization increase with increasing heat treatment time and take a maximum. On the other hand, the coercive force decreases with the increase in time of heat treatment. We confirmed that characteristics at only grain boundaries change into ferromagnetic phase by a MFM observation. As a trial for industrial application, heat treated Inconel 600 alloy was scanned by a magnetic field sensor, and the variations in magnetization were obtained nondestructively. The results indicate a feasibility of magnetic NDE for sensitization of Inconel 600 alloy.

Transient Liquid Phase Bonding of Directionally Solidified Ni Base Superalloy, GTD-111(I) - Bonding Phenomena and Mechanism - (일방향응고 Ni기초내열합금 GTD-111의 천이액상확산접합(I))

  • 강정윤;권민석;김인배;김대업;우인수
    • Journal of Welding and Joining
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    • v.21 no.2
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    • pp.82-88
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    • 2003
  • The bonding phenomenon and mechanism in the transient liquid phase bonding(TLP Bonding) of directionally solidified Ni base superalloy, GTD-111 was investigated. At the bonding temperature of 1403K, liquid insert metal was eliminated by isothermal solidification which was controlled by the diffusion of B and Si into the base metal and solids in the bonded interlayer grew epitaxially from mating base metal inward the insert metal. The number of grain boundaries formed at the bonded interlayer was corresponded with those of base metal. The liquation of grain boundary and dendrite boundary occurred at 1433K. At the bonding temperature of 1453K which is higher than liquation temperature of grain boundary, liquids of the Insert metal were connected with liquated grain boundaries and compositions in each region mixed mutually. In Joints held for various time at 1453t phases formed at liquated grain boundary far from the interface were similar to those of bonded interlayer. With prolonged holding time, liquid phases decreased gradually and liquids of continuous band shape divided many island shape. But liquid phases did not disappeared after holding for 7.2ks at 1453k. Isothermal solidification process at the bonding temperature which is higher than the liquation temperature of the grain boundary was controlled by diffusion of Ti to be result in liquation than B or Si. in insert metal. (Received January 15, 2003)

Piezoelectric Characteristics of PMW-PNN-PZT Ceramics according to Post-Annealing Process (Post annealing에 따른 PMW-PNN-PZT 세라믹스의 압전 특성)

  • Yoo, Kyung-Jin;Yoo, Ju-Hyun;Park, Chang-Yub;Lee, Hyung-Gyu;Kang, Hyung-Won
    • Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
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    • 2005.11a
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    • pp.212-213
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    • 2005
  • In this study, in order to develop low temperature sintering piezoelectric actuator, $Pb_{0.985}Bi_{0.01}(Mg_{1/2}W_{1/2})_{0.03}(Ni_{1/3}Nb_{2/3})_{0.13}(Zr_{0.50},Ti_{0.50})_{0.84}$ (PMW-PNN-PZT) ceramic systems were fabricated using $CaCO_3-Li_2CO_3$, sintering aid through a post-annealing process. The sinterability of PMW-PNN-PZT ceranics was remarkably enhanced by liquid phase sintering of $CaCO_3$ and $Li_2CO_3$. But, it was confimed form the X-ray diffraction pattern that the secondary phase along grain boundaries, deteriorated the piezoelectric properties. The secondary phase along grain boundaries was significantly removed by annealing after sintering. The 0.2wt% $Li_2CO_3$-0.25wt% $CaCO_3$-added PMW-PNN-PZT ceramics post-annealed at 900$^{\circ}C$ for 90min exhibited the excellent electromechanical coupling factor($k_p$) of 63.3% and piezoelectric constant($d_{33}$) of 452pC/N, respectively, for multilayer piezoelectricactuatorapplication.

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Microstructure and Phase Transition of ZnO Varistor Ceramics (ZnO 바리스터 세라믹스의 미세구조와 상전이)

  • 김경남;한상목
    • Journal of the Korean Ceramic Society
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    • v.28 no.2
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    • pp.160-166
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    • 1991
  • Microstructure and phase changes during the sintering of ZnO varistors were studied in ZnO-Bi2O3-CoO-Sb2O3 and ZnO-Bi2O3-CoO-Sb2O3-Cr2O3 systems using acanning electron microscopy (SEM) with an energy dispersive X-ray analysis (EDAX), X-ray diffraction (XRD) and differential thermal analysis (DTA). The spinel phase and the Bi2O3 phase were formed by the decomposition of the pyrochlore phase during heating. The spinel particles (2-4$\mu\textrm{m}$), which were formed both along ther grain boundaries and within the ZnO grain, were always found near the pyrochlore phase. Intergranular phases (Bi2O3 and pyrochlore) were precipitated from the liquid phase during cooling. The Bi2O3 phases were located at the triple (or multiple) point of the ZnO grains. Cr2O3 played a role in decreasing the formation temperature of the spinel phase and Bi2O3 phase during sintering, and inhibited the grain growth.

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Cuckoo search optimization algorithm for boundary estimation problems in electrical impedance tomography

  • Minho Jeon;Sravan Kumar Konki;Anil Kumar Khambampati;Kyung Youn Kim
    • Journal of IKEEE
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    • v.28 no.2
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    • pp.187-198
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    • 2024
  • Estimating the phase boundary in two-phase flow is crucial for designing and optimizing industrial processes. Electrical impedance tomography (EIT) is a promising technique for imaging phase distribution in such flows. This paper proposes using a cuckoo search (CS) optimization algorithm to estimate the phase boundary with EIT. The boundary is parameterized using the Fourier series, and the coefficients are determined by the CS algorithm. The CS algorithm iteratively seeks the phase boundary configuration by minimizing a cost function. Computer simulations and phantom experiments demonstrate the effectiveness of this method in estimating phase boundaries in two-phase flow.

Effective time-frequency characterization of Lamb wave dispersion in plate-like structures with non-reflecting boundaries

  • Wang, Zijian;Qiao, Pizhong;Shi, Binkai
    • Smart Structures and Systems
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    • v.21 no.2
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    • pp.195-205
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    • 2018
  • Research on Lamb wave-based damage identification in plate-like structures depends on precise knowledge of dispersive wave velocity. However, boundary reflections with the same frequency of interest and greater amplitude contaminate direct waves and thus compromise measurement of Lamb wave dispersion in different materials. In this study, non-reflecting boundaries were proposed in both numerical and experimental cases to facilitate time-frequency characterization of Lamb wave dispersion. First, the Lamb wave equations in isotropic and laminated materials were analytically solved. Second, the non-reflecting boundaries were used as a series of frames with gradually increased damping coefficients in finite element models to absorb waves at boundaries while avoiding wave reflections due to abrupt property changes of each frame. Third, damping clay was sealed at plate edges to reduce the boundary reflection in experimental test. Finally, the direct waves were subjected to the slant-stack and short-time Fourier transformations to calculate the dispersion curves of phase and group velocities, respectively. Both the numerical and experimental results suggest that the boundary reflections are effectively alleviated, and the dispersion curves generated by the time-frequency analysis are consistent with the analytical solutions, demonstrating that the combination of non-reflecting boundary and time-frequency analysis is a feasible and reliable scheme for characterizing Lamb wave dispersion in plate-like structures.

Multi-Scale Modelling of a Phase Mixture Model and the Finite Element Method for Nanocrystalline Materials (나노결정 재료의 상혼합모델과 유한요소법을 결합한 멀티스케일 모델링)

  • 윤승채;서민홍;김형섭
    • Transactions of Materials Processing
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    • v.13 no.2
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    • pp.174-179
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    • 2004
  • The effect of grain refinement on the plastic deformation behaviour of nanocrystalline metallic materials is investigated. A phase mixture model in which a single phase material is considered as an effectively two-phase one is discussed. A distinctive feature of the model is that grain boundaries are treated as a separate phase deforming by a diffusion mechanism. For the grain interior phase two concurrent mechanisms are considered: dislocation glide and mass transfer by diffusion. The proposed constitutive model was implemented into a finite element code (DEFORM) using a semicoupled approach. The finite element method was applied to simulating room temperature tensile deformation of Cu down to the nanoscale grain size in order to investigate the pre- and post-necking behaviour.