• Transactions of the Korean Society of Mechanical Engineers
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• v.9 no.6
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• pp.743-749
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• 1985

In this study the usefulness of Gas Chromatograph for the measurement of engine exhaust gas composition was confirmed. It was found that the composition of standard gas which was used for the calibration of Gas Chromatograph should not be greatly different from that of exhaust gas. Although self-evident, it cannot be overemphasized that utmost attention should be paid to prevent even a minute amount of air being mixed into the gas throughout the sampling process.

• Korean Journal of Optics and Photonics
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• v.5 no.2
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• pp.191-197
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• 1994

We investigated the properties of various methods of 3 dimensional profilometry to choose the phase shifting technique for the reconstruction of the shape of a given specimen. The pattern was generated by a Twyman-Green interferometer and a PZT was used to shift the fringes on the target surface. The shape was calculated with Hariharan algorithm within the uncertainty of a scaling factor. The optical noise inherent in the laser source was observed to influence the final outcome to a great extent and the need for an exact calibration was noted. noted.

• Proceedings of the Korean Geotechical Society Conference
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• 2000.03c
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• pp.93-104
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• 2000

By means of analyzing the problems in monitoring plan, design, installation, operation based on maintenance monitoring system installed in subway tunnel section, the methods of improvement were proposed for applying to subway monitoring maintenance effectively in future. The choice of the better monitoring system, the operating method of monitoring system, the confidence and continuity of maintenance monitoring, the performance of responsible monitoring supervision in the phase of the planning of monitoring and design were proposed. The problem and developed plan in the different monitoring systems, the calibration and correction of monitoring system, the analysis for the results and plan for maintenance in the phase of installation of monitoring system and operation were also proposed.

• Proceedings of the Korean Society of Soil and Groundwater Environment Conference
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• 2003.04a
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• pp.111-114
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• 2003

A new monitoring system has been developed for in-situ and realtime measurement of ozone transport in unsaturated porous media using a fiber optic sensor. The calibration of the fiber optic transflection dip probe (FOTDP) system was successfully carried out at various ozone concentrations using a column with length of 30 cm and diameter of 5 cm packed with glass beads, which don't react with gaseous ozone. The breakthrough curves (BTCs) of ozone was obtained by converting the normalized intensity into ozone concentration. The FOTDP system reflected the ideal transport phenomena of gas phase ozone at various flow rates. The FOTDP system worked well for in-situ monitoring of gas phase ozone at various water saturations and in presence of SOM. However, the FOTDP system did not measure the ozone concentration at more than 70% water saturation.

• Proceedings of the KAIS Fall Conference
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• 2010.05b
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• pp.1230-1232
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• 2010

A simple, rapid and validated reverse d phase liquid chromatographic method has been developed for the determination of Letrozole (LZ) in pharmaceutical dosage. LZ was separated on ODS analytical column with a mixture of acetonitrile, water in the ratio 50:50 (v/v) as mobile phase at a flow rate of 1.0 mL /min. The effluent was monitored by UV detection at 265nm. Calibration plot was linear in the range of 160 to $240{\mu}g$/mL with the linear regression (r) = 0.999. The method was validated for recovery, precision, specificity.

• Herbal Formula Science
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• v.18 no.2
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• pp.251-257
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• 2010

Objectives : To develop and validate High-performance liquid chromatography-photodiode array methods for simultaneous determination of two constituents in Oryeong-san(ORS). Methods : Reverse-phase chromatography using a Gemini C18 column operating at $40^{\circ}C$, and photodiode array(PDA) detection at 280 nm, were used for quantification of the two marker components of ORS. The mobile phase using a gradient flow consisted of two solvent systems. Solvent A was $H_2O$ and solvent B was acetonitrile. Results : Calibration curves were acquired with correlation coefficient ($r^2$)>0.9999, and the relative standard deviation(RSD) values(%) for intra- and inter-day precision were not exceed 1.0%. The recovery rate of each compound was in the range of 93.01-104.16%, with an RSD less than 2.0%. The contents of two compounds in ORS were 1.10-3.72 mg/g. Conclusions : The established HPLC method will be helpful to improve quality control of ORS.

• Bulletin of the Korean Chemical Society
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• v.27 no.11
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• pp.1832-1838
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• 2006

The present paper is focused on sorption concentration of silver (I) on some complex-forming ion exchangers in the initial thiocyanate form and subsequent determination of Ag(I) in the phase of anion exchanger AN-25 by diffuse reflectance spectroscopy. The sorption and kinetic characteristics of the sorbents were investigated. The apparent stability constants of thiocyanate silver complexes in the ion exchanger phase were calculated. The sorption-spectroscopic method is proposed for Ag(I) determination in aqueous solutions. The calibration curve is linear in the concentration range of 10-200 mg/L (sample volume is 10.0 mL) and the detection limit is 2 $\mu$g/mL. The presence of $Na^+,\;K^+,\;Mg^{2+}$ (macrocomponents) as well as of Ni (II), Co (II), Cu (II) do not hinder the determination of silver (I).

• YAKHAK HOEJI
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• v.31 no.5
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• pp.315-321
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• 1987

A high performance liquid chromatographic method was developed for the determination of glycyrrhetinic acid contained in licorice powder. Glycyrrhetinic acid which is hydrolysate of glycyrrhizin extracted from licorice powder, was determined with good result by HPLC using 2-bromoacetyltriphenylene labeling reagent. The glycyrrhetinic acids were labeled with 2-bromoacetyltriphenylene in acetonitrile using 18-crown-6-ether and KOH as a catalyst. Derivatized glycyrrhetinic acids were separated from the extracted licorice powder on a reversed-phase column (chemopak $C_{18}$) using 100% acetonitrile as a mobile phase and monitored by an UV-detector at 268nm. Linearity of calibration curve was obtained between 5 ng and 20 ng, and the lower limit of detection was 2 ng. The recovery of glycyrrhetinic acid to licorice powder was about 99.3%. This method was sensitive, reliable and useful for, determination of glycyrrhetinic acid.

• Journal of the Korea institute for structural maintenance and inspection
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• v.5 no.4
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• pp.161-167
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• 2001

By means of analyzing the problems in monitoring plan, design, installation, operation based on maintenance monitoring system installed in subway tunnel section, the improved methods of were proposed for applying to subway monitoring maintenance effectively in the future. The choice of the better monitoring system, the operating method of monitoring system, the confidence and continuity of maintenance monitoring, the performance of responsible monitoring supervision in the phase of the planning of monitoring and design were proposed. The problem and developed plan in the different monitoring systems, the calibration and correction of monitoring system, the analysis for the results and plan for maintenance in the phase of installation of monitoring system and operation were also proposed.

• Environmental Engineering Research
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• v.10 no.2
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• pp.71-78
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• 2005

A series of column experiments was conducted to develop a monitoring system for in-situ and realtime measurement of ozone transport in unsaturated porous media using a fiber optic sensor. The calibration of the fiber optic transflection dip probe (FOTDP) system was successfully carried out at various ozone concentrations using a column with length of 30 cm and diameter of 5 cm packed with glass beads, which don't react with gaseous ozone. The breakthrough curves (BTCs) of ozone were obtained by converting the normalized intensity into ozone concentration. The FOTDP system worked well for in-situ monitoring of gas phase ozone at various water saturations and in presence of soil organic matter (SOM). However, the FOTDP system did not measure the ozone concentration at more than 70% water saturation.