• 제목/요약/키워드: Pb addition

검색결과 745건 처리시간 0.028초

Ba치환된 $Pb(Mg_{1/3}Nb_{2/3})O_3$-$PbTiO_3$-$PbZrO_3$계 세라믹스의 압전 및 변위특성에 관한 연구 (Piezoelectric and strain characteristics of PMN-PT-PZ ceramics with Ba addition)

  • 지승한;이덕출;이능헌
    • E2M - 전기 전자와 첨단 소재
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    • 제10권1호
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    • pp.20-25
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    • 1997
  • In this study, piezoelectric actuator samples were fabricated using 0.375PMN-0.37OPT-0.255PZ system ceramics with Barium substitution and the strain properties of them were investigated. Dielectric constant of the specimens increased with the increase of Ba content up to 5mol% and decreased with futher addition of Ba. The largest piezoelectric coefficient and electromechanical coupling coefficient were observed at the sintering temperature of 1250'C and Barium content of 5mol%. The characteristics of strain hysteresis was found largely with varing the sintering temperature on the single round type, and the strain is proportional to piezoelectric coefficient.

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$MnO_2$가 첨가된 0.36PSN-0.25PNN-0.39PT세라믹스의 유전 및 압전특성 (The piezoelectric and dielectric properties of $MnO_2$ doped $0.36Pb(Sc_{1/2}Nb_{1/2})O_{3}-0.25Pb(Ni_{1/3}Nb_{2/3})O_{3}-0.39PbTiO_3$ ceramics)

  • 장정완;이종덕;박상안;이성갑;박기엽
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 2000년도 하계학술대회 논문집 C
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    • pp.1809-1811
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    • 2000
  • High power piezoelectric materials are presently being extensively developed for applications such as ultrasonic motors and piezoelectric transformer In this study, the piezoelectric and dielectric properties of $MnO_2$ doped $0.36Pb(Sc_{1/2}Nb_{1/2})O_{3}-0.25Pb(Ni_{1/3}Nb_{2/3})O_{3}-0.39PbTiO_3$ (hereafter PSNNT), which is the morphotropic phase boundary composition of the PSN-PNN-PT system were investigated. $MnO_2$-addition into the $0.36Pb(Sc_{1/2}Nb_{1/2})O_{3}-0.25Pb(Ni_{1/3}Nb_{2/3})O_{3}-0.39PbTiO_3$ composition increases the piezoelectric coefficient up to $k_{p}{\fallingdotseq}$55.6[%] and $Q_{m}{\fallingdotseq}$252. Moreover, $MnO_2$ addition makes tetragonal phase more stable with respect to rhombohedral phase.

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전해콘덴사용 알루미늄박의 피막형성 거동에 관한 연구 (Anodizing Mechanism of Aluminum Foil Electrolytic Capactor.)

  • 김기호
    • 한국표면공학회지
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    • 제22권2호
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    • pp.62-68
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    • 1989
  • Pb2+ ino, added in ctching sohing, is electrodeposited on a alumiunm foil for electrolycic condenser to promote its capacitance. In addition, several factoral factors in etching process are varied to examine how they change the capacitance of the condenser. The capacitance of the condenser made of 0.1 ppm pb electrodeposited aluminum foil is enhanced about 20% than of conventional ane. It is thought out that the enhanement is the result of the act of PbO2, which existed for the conveting of electrodeposited Pb, as a promoter tunnel etching of aluminum foil.

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Study of properties of $YBa_2Cu_3O_x$ with PbO and $BapbO_3$ additives

  • Soh, Dae-Wha;Fan, Zhanguo
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2004년도 하계학술대회 논문집 Vol.5 No.1
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    • pp.543-546
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    • 2004
  • The melting temperature and critical temperature(Tc) of $YBa_2Cu_3O_x$ with deferent content impurities of PbO and $BaPbO_3$ were studied. When the PbO was used as addition in $YBa_2Cu_3O_x$, although the melting point could be reduced, the superconductivity(the transition width, ${\Delta}T_c$) became poor. From the XRD pattern of the sintered mixture of $YBa_2Cu_3O_x$ and PbO it was known that there is a reaction between $YBa_2Cu_3O_x$ and PbO, and the product is $BaPbO_3$. In the process of the reaction the superconducting phase of $YBa_2Cu_3O_x$ was decreased and in the sample $BaPbO_3$ became the main phase. Therefore the superconductivity was reduced. $BaPbO_3$ was chosen as the impurity for the comparative study. The single phase BaPbO3 was synthesized by the simple way from both mixtures of $BaPbO_3$ and PbO, $BaPbO_3\;and\;PbO_2$. Deferent contents of $BaPbO_3$(10%, 20%, 30%) were added in the $YBa_2Cu_3O_x$. By the phase analysis in the XRD patterns it was proved that there werenot reactions between $YBa_2Cu_3O_x$ and $BaPbO_3$. When $BaPbO_3$ was used as impurity in $YBa_2Cu_3O_x$ the superconductivity was much better than PbO as impurity in $YBa_2Cu_3O_x$. But the melting point of $YBa_2Cu_3O_x$ with $BaPbO_3$ could not be found when the temperature was lower than $1000^{\circ}C$ in the DTA measurement.

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Pb($Fe_{2/3}W_{1/3}$)$O_{3}$가 ($Pb_{x}Ca_{1-x}$)$ZrO_{3}$의 소결과 마이크로파 유전 특성에 미치는 영향 (Effect of Pb($Fe_{2/3}W_{1/3}$)$O_{3}$ on the sintering and dielectric characteristics of ($Pb_{x}Ca_{1-x}$)$ZrO_{3}$)

  • 임상규;김덕환;안철
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 1998년도 하계종합학술대회논문집
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    • pp.379-382
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    • 1998
  • In this paper, the microwave dielectric properties of the yPb($Fe_{2/3}W_{1/3}$)$O_{3}$ - (1-y)($Pb_{x}Ca_{1-x}$)$ZrO_{3}$ system were investigated. It was found that an addition of Pb($Fe_{2/3}W_{1/3}$)$O_{3}$ promotes the grain growth, the solid solution between the Pb-based perovskite and the Ca-based perovskite and the decreasing of the sintering temperature. Especially, we found that 0.05Pb($Fe_{2/3}W_{1/3}$)$O_{3}$-0.95($Pb_{x}Ca_{1-x}$)$ZrO_{3}$ ceramic has not only lower sintering temperature but also better dielectric properties than those of the (Pb, Ca)$ZrO_{3}$ systems.

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급속응고된 Al-Pb-Cu-Mg 합금의 마모특성에 미치는 미세조직의 영향 (Effect of the Microstructrure of Rapidly Solidified Al-Pb-Cu-Mg on the Wear ProPerty)

  • 김홍물
    • 한국분말재료학회지
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    • 제7권1호
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    • pp.12-18
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    • 2000
  • Effects of the microstrucrure of rapidy solidified Al-Pb-Cu-Mg alloys on the wear investigated. In order to overcome the miscility gap between Al and pb under equilibrium conditions, both in the solid and the liquid states, the alloy were rapidy solidifies to produce them in a segregation-free condition. Although the Pb particles showed relatively fine dispersion in the Al matrix in all the alloys by this process. the Al-16Pb alloy was found to have the most favorable microstructure with discretre with discrete Pb particles of abount 0.5 ${\mu}$m in size. With the addition of Cu and Cu-Mg to Al-16Pb, cellular structures were newly formed; not seen in the binary Al-Pb alloy. Wear properties of the Al-Pb binary alloys measured as a function of the sliding speen, sliding distance, and applied load showed that the Al-16Pb alloy has the best wear resistance, as expected from the fine microstructural features in this alloy. The were resistance of the alloy containing Cu-and Cu-Mg was higher than that of the Al-16Pvb alloy, due to matrix strengthening by precipitation hardeing. The wear mechanism was identified by examining the traces and wear debris.

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Properties of $YBa_2Cu_3O_x$ with PbO and $BaPbO_3$ additives

  • Fan, Zhanguo;Soh, Daewha;Cho, Yongjoon
    • 한국정보통신학회:학술대회논문집
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    • 한국해양정보통신학회 2004년도 SMICS 2004 International Symposium on Maritime and Communication Sciences
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    • pp.57-59
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    • 2004
  • The melting temperature and critical temperature (Tc) of YBa$_2$Cu$_3$Ox with deferent content impurities of PbO and BaPbO$_3$ were studied. When the PbO was used as addition in YBa$_2$Cu$_3$Ox, although the melting point could be reduced, the superconductivity (the transition wide, ΔTc) became poor. From the XRD pattern of the sintered mixture of YBa$_2$Cu$_3$Ox and PbO it was known that there is a reaction between YBa$_2$Cu$_3$Ox and PbO, and the product is BaPbO$_3$. In the process of the reaction the superconducting phase of YBa$_2$Cu$_3$Ox was decreased and in the sample BaPbO$_3$became the main phase. Therefore the superconductivity was reduced. BaPbO$_3$was chosen as the impurity for the comparative study. The single phase BaPbO$_3$was synthesized by the simple way from both mixtures of BaPbO$_3$and PbO, BaPbO$_3$and PbO$_2$. Deferent contents of BaPbO$_3$(10%, 20%, 30%) were added in the YBa$_2$Cu$_3$Ox. By the phase analysis in the XRD patterns it was proved that there were not reactions between YBa$_2$Cu$_3$Ox and BaPbO$_3$. When BaPbO$_3$was used as impurity in YBa$_2$Cu$_3$Ox the superconductivity was much better than PbO as impurity in YBa$_2$Cu$_3$Ox But the melting point of YBa$_2$Cu$_3$Ox with BaPbO$_3$could not be found when the temperature was lower than 1000 $^{\circ}C$ in the DTA measurement.

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$MnO_2$ 첨가에 따른 (Pb)(La,Ce)$TiO_3$ 세라믹스의 미세구조특성 (Microstructural Properties of (Pb)(La,Ce)$TiO_3$ ceramics as a function of $MnO_2$ addition)

  • 오동언;민석규;윤광희;류주현;박창엽
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 추계학술대회 논문집 Vol.14 No.1
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    • pp.442-445
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    • 2001
  • In this study, microstructural and dielectric properties of $Pb_{0.83}(La_{0.2}Ce_{0.8})_{0.08}TiO_3$(PCT) ceramics as a function of $MnO_2$ addition were investigated for 30MHz ceramic resonator application. Grain size was gradually increased according to the increase of $MnO_2$ addition amount and showed the highest value of $1.502{\mu}m$ at the 0.9wt% $MnO_2$. Moreover, density showed the highest value of $7.582 g/cm^3$ at the 0.7wt% $MnO_2$.All the composition ceramics,curie temperature was nearly constant around $330^{\circ}C$

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Preparation of YBCO with additives of PbO, $BaPbO_3$ and its Superconducting Properties

  • Zhanguo, Fan;Soh, Dae-Wha
    • 동굴
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    • 제78호
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    • pp.17-22
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    • 2007
  • The melting temperature and critical temperature (Tc) of $YBa_2Cu_3O_x$ with deferent content impurities of PbO and $BaPbO_3$ were studied. When the PbO was used as addition in $YBa_2Cu_3O_x$, although the melting point could be reduced, the superconductivity (the transition wide, ${\Delta}T_c$) became poor. From the XRD pattern of the sintered mixture of $YBa_2Cu_3O_x$ and PbO it was known that there is a reaction between $YBa_2Cu_3O_x$ and PbO, and the product is $BaPbO_3$. In the process of the reaction the superconducting phase of $YBa_2Cu_3O_x$ was decreased and in the sample $BaPbO_3$ became the main phase. Therefore the superconductivity was reduced. $BaPbO_3$ was chosen as the impurity for the comparative study. The single phase $BaPbO_3$ was synthesized by the simple way from both mixtures of $BaCO_3$ and PbO, $BaCO_3$ and $PbO_2$. Deferent contents of $BaPbO_3$ (10%, 20%, 30%) were added in the $YBa_2Cu_3O_x$. By the phase analysis in the XRD patterns it was proved that there were not reactions between $YBa_2Cu_3O_x$ and $BaPbO_3$. When $BaPbO_3$ was used as impurity in $YBa_2Cu_3O_x$ the superconductivity was much better than PbO as impurity in $YBa_2Cu_3O_x$. But the melting point of $YBa_2Cu_3O_x$ with $BaPbO_3$ could not be found when the temperature was lower than $1000^{\circ}C$ in the DTA measurement.

Bi2O3 첨가량에 따른 저온소결 PbTiO3계 세라믹스의 유전 및 압전특성 (Dielectric and Piezoelectric Characteristics of Low Temperature Sintering PbTiO3 System Ceramics with amount of Bi2O3 Addition)

  • 류주현;김도형;이상호;손은영
    • 한국전기전자재료학회논문지
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    • 제20권9호
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    • pp.771-775
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    • 2007
  • In this study, in order to develop low temperature sintering ceramics for thickness vibration mode multilayer piezoelectric transformer, $PbTiO_3$ system ceramics were fabricated using $Na_2CO_3,\;Li_2CO_3,\;MnO_2\;and\;Bi_2O_3$ as sintering aids and their dielectric and piezoeletric properties were investigated according to the amount of $Bi_2O_3$ addition. At the sintering temperature of $900^{\circ}C\;and\;Bi_2O_3$ addition of 0.1 wt%, density, grain size, thickness vibration mode eletromechanical coupling factor($k_t$), thickness vibration mode mechanical quality factor($Q_{mt}$) and dielecteic constant(${\varepsilon}_r$) showed the optimum value of $6.94g/cm^3,\;2.413{\mu}m$, 0.497, 3,162 and 209, respectively, for thickness vibration mode multilayer piezoelectric transformer application.