• Title/Summary/Keyword: Pb

Search Result 7,034, Processing Time 0.032 seconds

A Study on the Characteristics of Low Pb Sn-5%Pb-1.5%Pb-1.5Ag-x%In Solder Alloys (저 Pb Sn-5%Pb-1.5%Ag-x%In계 솔도 합금의 특성에 관한 연구)

  • Hong, Sun-Guk;Ju, Cheol-Hong;Gang, Jeong-Yun;Kim, In-Bae
    • Korean Journal of Materials Research
    • /
    • v.8 no.11
    • /
    • pp.1011-1019
    • /
    • 1998
  • This work designed Sn-5%Pb-1.5%Ag-x%In solder alloy to develop the solder alloy with low Pb content. This solder alloy doesn't cause environmental pollution. and this study reviewed the probability of replacement of Sn-37%Pb solder as evaluation of melting range, wettability. microstructure, microhardne'ss, tensile strength, drossability of this new solder alloys. The level of international regulation in dissolution amount of Pb ion was 3ppm. But dissolution amount of Pb ion in Sn-5%Pb solder alloy confirmed not to threat the global environmental is 0.46ppm. The melting range of this solder alloy was $183-192^{\circ}C$. Also the range of solidification was very narrow within $5^{\circ}C$. The wettability was similar to Sn-37%Pb solder, and the effect of amount of In addition of wettability couldn't be founded. The probability of replacement in the melting range and wettability is very high. And microhardness of this solder alloy was 1.5 times of conventional type solder. Tensile strength of new solder alloys was a little high than that of conventional type solder. With increasing amount of In% addition, tensile strength was increased, but elongation was decreased. The solder alloy of l%In addition revealed AgSn and Pb on dendrite microstructure boundary, and $Ag_3Sn$, $Ag_3In$ and Pb were revealed on it at the solder alloy of 3% In addition. The drossability was superior to Sn-37%Pb solder alloy and the solder alloys of 2% In addition was not generated for 3hrs.

  • PDF

The effects of both store and private brand apparel product attributes on satisfaction and repurchase intention at large discount stores (대형할인점의 점포속성과 PB 의류 제품속성이 만족도 및 재구매 의도에 미치는 영향)

  • Ju, Seong-Rae;Chung, Myung-Sun
    • The Research Journal of the Costume Culture
    • /
    • v.22 no.1
    • /
    • pp.143-157
    • /
    • 2014
  • The aims of this study were to identify the dimensions of both store and PB apparel product attributes at large discount stores, and to empirically examine the effects of each dimension of store and PB apparel product attributes on satisfaction with PB apparel products and on repurchase intension. Questionnaires were given to 264 large discount store customers, who have experienced buying PB apparel products at large discount stores. The results were as follows. First, purchased PB items and image, improvement of PB apparel products showed differences by gender. Second, the dimensions for store attributes were categorized as convenient of shopping environment, product quality, customer service, advertising reach, convenient location, and reasonable prices. The PB apparel product attributes were categorized as material handling management, quality, fashion ability, and brand power. Third, generally, both store and PB apparel product attributes at large discount stores are significantly related to PB apparel satisfaction and repurchase intention. PB satisfaction and repurchase intention of males were partly affected by store attributes and PB apparel product attributes. PB satisfaction and repurchasing intention of females, however, were partly affected by only PB apparel product attributes, not store attributes.

Metabolic Changes in Growing Rats Fed Diets with Different Levels of Lead and Lipid (납(Pb) 과 지방수준을 달리한 식이로 사육한 성장기 흰쥐의 체내대사변화)

  • 김정숙
    • Journal of Nutrition and Health
    • /
    • v.20 no.4
    • /
    • pp.225-236
    • /
    • 1987
  • This study was performed to investigate the effects of lead poisoning and different levels of dietary lipid on lead and lipid metabolism in the rats. Forty eight male weanling rats of Sprague-Dawley strain weighing 73.1$\pm$11.1g were blocked into 6 groups according to body weight. Dietary lipid were given at the lev딘 of 5, 20 and 40% of total caloric intake and lead were either administered or not. The results obtained are summerized as follows ; 1) Food intake, weight gain, F.E.R. liver and epididymal. fat pad weights, weight and length of bone, hematocrit and hemoglobin content in Pb-adminstered groups were lower than these in Pb-free groups. 2) Plasma lipid and cholesterol levels were tended to be higher in Pb-administered groups than in Pb-free groups, while liver lipid and cholesterol levels were tended to be lower in Pb-adminstered groups. 3) Fecal dry matter excretion was tended to be higher in Pb-adminstered groups than in Pb-free groups, and were increased with increasing dietary lipid level. Daily fecal excretions of lipid and cholesterol were higher in high lipid groups than in low lipid groups and these levels were even higher in the animals exposed to Pb than in Pb-free groups. 4) Pb contents in blood, liver, kidney and bone were significantly higher in Pb administered groups than in Pb-free groups. Pb levels of blood, liver and bone did not show any significant difference among groups with different levels of dietary lipid, but Pb concentration in kidney of Pb-adminstered groups increased with increasing dietary lipid level.

  • PDF

Influence on Dielectric Properties and Evaporation of PbO According to Substituting $Nd^{3+}$ for $Pb^{2+}$ in $Pb(Mg_{1/3}Nb_{2/3})O_3$ System ($Pb(Mg_{1/3}Nb_{2/3})O_3$계 세라믹스의 $Pb^{2+}$$Nd^{3+}$로 치환함에 따른 유전특성 및 PbO 휘발에 관한 연구)

  • 김성열;이응상
    • Journal of the Korean Ceramic Society
    • /
    • v.30 no.3
    • /
    • pp.175-180
    • /
    • 1993
  • Influence of Nd3+ substitution for Pb2+ on the dielectric properties and the PbO evaporation according to substituting Nd3+ for Pb2+ in Pb(Mg1/3Nb2/3)O3 system ceramics have been investigated. The dielectric constant at the curie temperature and evaporation of PbO were decreased with increase of Nd3+ amounts. The percentage of PbO evaporation was 2.5wt% in the PMN system substituted Nd3+ for Pb2+, while it was 3.7wt% in the PMN system.

  • PDF

Effects of $PbTiO_3$ Addition on Dielectric Properties and Extent of PbO Loss in Nd-Doped $Pb(Mg^{1/3}Nb^{2/3})O_3$ System ($Nd^{3+}$로 치환된 $Pb(Mg^{1/3}Nb^{2/3})O_3$$PbTiO_3$ 첨가에 따른 유전특성과 PbO 휘발)

  • 김성열;이응상
    • Journal of the Korean Ceramic Society
    • /
    • v.30 no.8
    • /
    • pp.671-677
    • /
    • 1993
  • Effects of PbTiO3 addition on dielectric properties and extent of PbO loss in Nd-doped Pb(Mg1/3Nb2/3)O3 system were investigated. As the proportion of dopping increased, the phase transition temperature shifted to low region, and the dielectric constant at room temperature decreased rapidly. But as the proportion of PbTiO3 increased, the phase transition temperature shifted to high retion, and the dielectric constant at room temperature increased. The substitution of Nd3+ for Pb2+ decreased the amount of PbO evaporation, therefore the sample sintered well in case of only 1 mole% adding excess PbO.

  • PDF

Microstructure and Dielectric Properties in $40Pb(Mg_{1/3}Nb_{2/3})O_3-30PbTiO_3-30Pb(Mg_{1/2}W_{1/2})O}3$ Ceramics with Excess $91PbO-9WO_3$ Addition ($91PbO-9WO_3$가 과잉첨가된 $40Pb(Mg_{1/3}Nb_{2/3})O_3-30PbTiO_3-30Pb(Mg_{1/2}W_{1/2})O}3$계 세라믹스의 미세구조와 유전특성)

  • 길영배;이응상
    • Journal of the Korean Ceramic Society
    • /
    • v.34 no.3
    • /
    • pp.281-288
    • /
    • 1997
  • The effects of 0 to 6 mol% excess 91PbO-9WO3 addition on the microstructure and the dielectric pro-perties in 40Pb(Mg1/3Nb2/3)O3-30PbTiO3-30Pb(Mg1/2W1/2)O3 ternary system were investigated. Excess 91PbO-9WO3 addition enhanced densification at relatively lower temperature due to the formation of liquid phase. The dielectric constant of the specimen with standard composition was 16,400 and that of specimen with 1 mol% excess additive was the maximum of 18,500. And more than 2 mol% excess addition decreased dielec-tric constant. Specimens with 2~4 mol% 91PbO-9WO3 addition showed dual peak maxima in the tem-perature dependence of dielectric constant. In the specimens which have more than 5 mol% excess addition a new phase with W-rich composition was formed at grain boundary.

  • PDF

Biosorption and Desorption of Pb by Using Sargassum sagamianum (해조류, Sargassum sagamianum을 이용한 Pb 흡착 및 탈착)

  • Seo, Geun-Hak;An, Gap-Hwan;Gong, In-Su
    • KSBB Journal
    • /
    • v.14 no.5
    • /
    • pp.611-615
    • /
    • 1999
  • Biosorption of Pb was evaluated for Sargassum sagamianum. An adsorption equilibrium was reached in about 1 hr. The uptake capacity of Pb was 224.5 mg Pb/G biomass. The adsorption parameters for Pb were determined according to Langmuir and Frueundlich model. With increasing pH, more negative sites are becoming available for adsorption of Pb. When Ca and Mg concentration increases in Pb solution, Pb was selectively adsorbed. The Pb adsorbed by S. sagamianu could be desorbed by desorption process and the efficiency from 0.1M HCl, 0.1M HNO$_3$and 0.1M EDTA was above 95%. S. Sagamianum was reused 6 times and the total uptake was 736.8 mg Pb/g biomass.

  • PDF

Effect of Excess PbO on Grain Growth and Densification of (65)Pb(${Mg_{1/3}}{Nb_{2/3}}$)$O_3$-(35)$PbTiO_3$ Ceramics ((65)Pb(${Mg_{1/3}}{Nb_{2/3}}$)$O_3$-(35)$PbTiO_3$의 입자성장과 치밀화에 미치는 과량 PbO의 영향)

  • Lee, Jong-Bong;Hur, Tae-Moo;Lee, Ho-Yong;Choi, Kyun;Kim, Doe-Yeon
    • Journal of the Korean Ceramic Society
    • /
    • v.37 no.7
    • /
    • pp.673-680
    • /
    • 2000
  • The effect of excess PbO(0, 1, 2, 4, and 8 mol%) on grain growth and densification of (65)Pb(Mg1/3Nb2/3)O3-(35)PbTiO3 [mol%] ceramics has been investigaetd. With increasing the amount of excess PbO and sintering time, densities of sintered samples decreased gradually. The samples containing less than 1 mol% of PbO showed normal grain growth behavior, however abnormal grain growth was observed to occur in the samples with more than 2 mol% of PbO. In the samples with more than 2 mol% of PbO, the number of abnormal grains decreased and thus the average grain size became smaller with increasing the amount of excess PbO. These results demonstrated that the abnormal grain growth started to occur when a critical amount of excess PbO was added to a (65)Pb(Mg1/3Nb2/3)O3-(35)PbTiO3 sample. Since PMN-PT grains in a liquid matrix were angular, the observed abnormal grain growth was explained to proceed through the two dimensional nucleation process.

  • PDF

Properties of $YBa_2Cu_3O_x$ with PbO and $BaPbO_3$ additives

  • Fan, Zhanguo;Soh, Daewha;Cho, Yongjoon
    • Proceedings of the Korean Institute of Information and Commucation Sciences Conference
    • /
    • 2004.05a
    • /
    • pp.57-59
    • /
    • 2004
  • The melting temperature and critical temperature (Tc) of YBa$_2$Cu$_3$Ox with deferent content impurities of PbO and BaPbO$_3$ were studied. When the PbO was used as addition in YBa$_2$Cu$_3$Ox, although the melting point could be reduced, the superconductivity (the transition wide, ΔTc) became poor. From the XRD pattern of the sintered mixture of YBa$_2$Cu$_3$Ox and PbO it was known that there is a reaction between YBa$_2$Cu$_3$Ox and PbO, and the product is BaPbO$_3$. In the process of the reaction the superconducting phase of YBa$_2$Cu$_3$Ox was decreased and in the sample BaPbO$_3$became the main phase. Therefore the superconductivity was reduced. BaPbO$_3$was chosen as the impurity for the comparative study. The single phase BaPbO$_3$was synthesized by the simple way from both mixtures of BaPbO$_3$and PbO, BaPbO$_3$and PbO$_2$. Deferent contents of BaPbO$_3$(10%, 20%, 30%) were added in the YBa$_2$Cu$_3$Ox. By the phase analysis in the XRD patterns it was proved that there were not reactions between YBa$_2$Cu$_3$Ox and BaPbO$_3$. When BaPbO$_3$was used as impurity in YBa$_2$Cu$_3$Ox the superconductivity was much better than PbO as impurity in YBa$_2$Cu$_3$Ox But the melting point of YBa$_2$Cu$_3$Ox with BaPbO$_3$could not be found when the temperature was lower than 1000 $^{\circ}C$ in the DTA measurement.

  • PDF

Biosorption of Pb and Cr by using Sargassum sagamianum (비틀대모자반, Sargassum sagamianum을 이용한 Pb 및 Cr 생체흡착 및 회수)

  • SUH Kuen-Hack;AHN Kab-Hwan;LEE Hack-Sung;LEE Hwae-Geon;CHO Jin-Koo;HONG Yong-Ki
    • Korean Journal of Fisheries and Aquatic Sciences
    • /
    • v.32 no.4
    • /
    • pp.399-403
    • /
    • 1999
  • Biosorption of Pb and Cr to Sargassum sagamianum was evaluated in the various conditions. An adsorption equilibrium was reached in about 15 min. for Pb and Cr. The uptake capacity was 224.5 mg Pb/g biomass and 77.5 mg Cr/g biomass, respectively. The adsorption parameters for Pb and Cr were determined according to Langmuir and Freundlich model. Biosorption of Pb and Cr was increased with an increase in pH value. Pb and Cr adsorbed by S. sagamianum could be recovered by desorption process with 0.1M HCl, 0.1M $HNO_3$ and 0.1M EDTA and the efficiency of Pb desorption was above $90\%$, whereas the efficiency of Cr desorption was below $51\%$.

  • PDF