• Title/Summary/Keyword: Partition

Search Result 1,949, Processing Time 0.032 seconds

Synthesis of Cocoa Butter Alternative from Coconut Oil Fraction and Palm Oil Fractions by Lipase-Catalyzed Interesterification (Coconut Oil 분별유와 Palm 분별유로부터 효소적 Interesterification에 의한 코코아 버터 대체유지 합성)

  • Bae, Sang-Kyun;Lee, Kyung-Su;Lee, Ki-Teak
    • Journal of the Korean Society of Food Science and Nutrition
    • /
    • v.39 no.10
    • /
    • pp.1487-1494
    • /
    • 2010
  • Structured lipid (SL) for cocoa butter alternative was synthesized by interesterification of coconut oil fraction and palm stearin (6:4 and 8:2, by weight) in a shaking water bath at $60^{\circ}C$ and 180 rpm. It was performed for various reaction times (1, 2, 3, and 6 hr). The reaction was catalyzed by sn-1,3 specific Lipozyme TLIM (immobilized lipase from Thermomyces lanuginosus). SL-solid part was obtained from acetone fractionation at $0^{\circ}C$. SL-solid part was blended with other palm oils and fractions for desirable property of cocoa butter alternative (SL-solid part : palm middle fraction : palm stearin solid : palm oil, 70.4:18.4:2.9:8.3, by weight). In reversed-phase HPLC analysis, triacylglycerol species of cocoa butter alternative had partition number of 40 (10.77%), 42 (13.06%), 44~46 (17.38%) and 48 (51.88%). Major fatty acids of cocoa butter alternative were lauric acid (16.5%), myristic acid (12.28%), palmitic acid (46.03%), and linoleic acid (14.75%). Solid fat content (SFC) and polymorphic form (${\beta}'$ form) of cocoa butter alternative prepared were similar to those of commercial cocoa butter replacer (CBR).

Analysis of Multiple Pesticide Residues in Apples and Pears Using Gas-Liquid Chromatography (Gas-Liquid Chromatography를 이용한 사과 및 배 중의 농약 다성분 잔류분석법)

  • Park, Ju-Hwang;Kim, Taek-Kyum;Oh, Chang-Hwan;Kim, Jeong-Han;Lee, Young-Deuk;Kim, Jang-Eok
    • Korean Journal of Environmental Agriculture
    • /
    • v.23 no.3
    • /
    • pp.148-157
    • /
    • 2004
  • A rapid analytical method was developed to determine multiple pesticide residues in apples and pears using gas-liquid chromatography (GLC). The samples were extracted with water-miscible solvents and purified by cleanup procedures serially comprising liquid-liquid partition and solid-phase extraction (SPE). Each analyte was separated and determined by a high-resolution GLC equipped with electron-capture detector (ECD) and nitrogen-phosphorous detector (NPD). A total of 196 pesticides, which were previously classified into 5 groups each for ECD and NPD based on their retention behaviors on the capillary column and responses to the detector, were subjected to the recovery experiment. In compliance with the analytical criteria, 70 to 120% of recovery and less than 20% relative standard deviation the proposed method could be successfully applied to analyze 136 and 133 pesticide residues in apples and pears, respectively, which enabled not only rapid screening but quantitation of the residues. Even though less reliability was resulted from unacceptable recovery range, rest of pesticides including 43 and 45 analyzes in apples and pears, could be also detected for their identity. The proposed method fliled to cover 17 and 18 pesticides for apples and pears, which mostly showed high polarity or heat-lability but could be suitable far fast surveilance or monitoring of fruit harvests.

Design of Data-centroid Radial Basis Function Neural Network with Extended Polynomial Type and Its Optimization (데이터 중심 다항식 확장형 RBF 신경회로망의 설계 및 최적화)

  • Oh, Sung-Kwun;Kim, Young-Hoon;Park, Ho-Sung;Kim, Jeong-Tae
    • The Transactions of The Korean Institute of Electrical Engineers
    • /
    • v.60 no.3
    • /
    • pp.639-647
    • /
    • 2011
  • In this paper, we introduce a design methodology of data-centroid Radial Basis Function neural networks with extended polynomial function. The two underlying design mechanisms of such networks involve K-means clustering method and Particle Swarm Optimization(PSO). The proposed algorithm is based on K-means clustering method for efficient processing of data and the optimization of model was carried out using PSO. In this paper, as the connection weight of RBF neural networks, we are able to use four types of polynomials such as simplified, linear, quadratic, and modified quadratic. Using K-means clustering, the center values of Gaussian function as activation function are selected. And the PSO-based RBF neural networks results in a structurally optimized structure and comes with a higher level of flexibility than the one encountered in the conventional RBF neural networks. The PSO-based design procedure being applied at each node of RBF neural networks leads to the selection of preferred parameters with specific local characteristics (such as the number of input variables, a specific set of input variables, and the distribution constant value in activation function) available within the RBF neural networks. To evaluate the performance of the proposed data-centroid RBF neural network with extended polynomial function, the model is experimented with using the nonlinear process data(2-Dimensional synthetic data and Mackey-Glass time series process data) and the Machine Learning dataset(NOx emission process data in gas turbine plant, Automobile Miles per Gallon(MPG) data, and Boston housing data). For the characteristic analysis of the given entire dataset with non-linearity as well as the efficient construction and evaluation of the dynamic network model, the partition of the given entire dataset distinguishes between two cases of Division I(training dataset and testing dataset) and Division II(training dataset, validation dataset, and testing dataset). A comparative analysis shows that the proposed RBF neural networks produces model with higher accuracy as well as more superb predictive capability than other intelligent models presented previously.

A System of Audio Data Analysis and Masking Personal Information Using Audio Partitioning and Artificial Intelligence API (오디오 데이터 내 개인 신상 정보 검출과 마스킹을 위한 인공지능 API의 활용 및 음성 분할 방법의 연구)

  • Kim, TaeYoung;Hong, Ji Won;Kim, Do Hee;Kim, Hyung-Jong
    • Journal of the Korea Institute of Information Security & Cryptology
    • /
    • v.30 no.5
    • /
    • pp.895-907
    • /
    • 2020
  • With the recent increasing influence of multimedia content other than the text-based content, services that help to process information in content brings us great convenience. These services' representative features are searching and masking the sensitive data. It is not difficult to find the solutions that provide searching and masking function for text information and image. However, even though we recognize the necessity of the technology for searching and masking a part of the audio data, it is not easy to find the solution because of the difficulty of the technology. In this study, we propose web application that provides searching and masking functions for audio data using audio partitioning method. While we are achieving the research goal, we evaluated several speech to text conversion APIs to choose a proper API for our purpose and developed regular expressions for searching sensitive information. Lastly we evaluated the accuracy of the developed searching and masking feature. The contribution of this work is in design and implementation of searching and masking a sensitive information from the audio data by the various functionality proving experiments.

Removal Characteristics of Volatile Organic Compounds in Biofilters and Stoichiometric Analysis of Biological Reaction by Carbon Mass Balance (바이오필터의 휘발성유기화합물 제거특성 및 탄소물질수지를 이용한 생물반응의 양론적 해석)

  • Kim, Dae-Keun
    • Journal of Korean Society of Environmental Engineers
    • /
    • v.32 no.8
    • /
    • pp.747-753
    • /
    • 2010
  • This study was performed to investigate the removal characteristics of volatile organic compounds (VOCs) in the gasphase biofilters, and to propose a stoichiometric analysis approach to characterize biological reaction through carbon mass balance. The VOCs studied were toluene, styrene, methyl ethyl ketone (MEK), and methyl isobutyl ketone (MIBK) as a single substrate for each biofilter. The critical loading rate was determined to be $46.9\;g/m^3{\cdot}hr$, $25.8\;g/m^3{\cdot}hr$, $96.3\;g/m^3{\cdot}hr$, and $66.5\;g/m^3{\cdot}hr$ for toluene, styrene, MEK, and MIBK, respectively. The obtained results indicated that the critical loading rate was well correlated the octanol-water partition coefficient. In the analysis of carbon mass balance, carbon recovery to $CO_2$ became relatively lower as substrate loadings increased, but higher for carbon recovery to biomass. Stoichiometric analysis revealed that biomass yield increased as substrate loadings increased, and its coefficient (g biomass/g substrate) varied from 0.31 to 0.57 for toluene, 0.29 to 0.57 for styrene, 0.08 to 0.56 for MEK, and 0.14 to 0.53 for MIBK.

Modeling for the fate of Organic Chemicals in a Multi-media Environment Using MUSEM (다매체 환경 모델 MUSEM을 이용한 유해화학물질의 환경거동예측 모델링)

  • Roh, Kyong-Joon;Kim, Dong-Myung
    • Journal of the Korean Society for Marine Environment & Energy
    • /
    • v.10 no.4
    • /
    • pp.201-210
    • /
    • 2007
  • Pollution by chemical substances such as POPs, EDCs and PBTs in the ecosystem has become more complex and varied, increasing the possibility of irreversible damage to human health or the ecosystem. It is necessary to have a exposure assessment in a multi-media environment for various chemical substances is required for efficient management. This study applied MUSEM(Multi-media Simplebox-systems Environmental Model), a multimedia environmental model that can simultaneously evaluate the possibility of exposure of hundreds of chemical substances in order to efficiently manage chemical substances that can have negative impact on human health or ecological environment through environmental contamination. MUSEM executed the modeling for Japan by setting all 47 prefectures of japan as the regional area for 62 chemical substances and the rest of the territory of japan, excluding regional area, as the continental area and made the estimation of concentration among environment media in each administrative area and made the sensitivity analysis on Tokyo area. The results of simulation for chemical distribution showed that most of the target chemicals located in water region. The result of sensitivity analysis for octanol-water partition rate showed that the concentration change of soil in urban/industrial area and sediment in freshwater was high. In the case of sensitivity analysis for degradation rate showed that the concentration change of freshwater, soil in urban/industrial area, and sediment in freshwater was high.

  • PDF

Gas-Liquid Chromatographic Determination of Haloxyfop-R and lts Methyl Ester Residues in Soils and Soybeans (토양과 대두중 Haloxyfop-R 및 Haloxyfop-R-methyl의 기체크로마토그래피를 이용한 잔류분석)

  • Lee, Young-Deuk
    • Korean Journal of Environmental Agriculture
    • /
    • v.16 no.4
    • /
    • pp.333-340
    • /
    • 1997
  • An analytical method was developed to determine residues of haloxyfop-R and its methyl ester in soils and soybeans using gas-liquid chromatography (GLC) with electron capture detector (ECD). Soil or soybean sample was acidified and extracted with acetone. The extract was then subjected to ion-associated partition to individually separate haloxyfop-R and the neutral methyl ester. One phase containing haloxyfop-R was methylated with $BF_3$/methanol, partitioned to n-hexane and analyzed by GLC/ECD. The other phase containing the methyl ester was further purified by Florisil column chromatography prior to GLC determination. No cross contamination was found between two phases containing each of the acid and methyl ester, thus two compounds can be separately determined as the identical haloxyfop-R-methyl. Overall recoveries of haloxyfop-R from fortified samples averaged 88.2${\pm}$3.9% (n=12) and 88.3${\pm}$4.0% (n=6) for soils and soybeans respectively, and those of haloxyfop-R-methyl showed mean values of 89.2${\pm}$4.0% (n=12) and 85.6${\pm}$5.6% (n=6). Detection limits of both haloxyfop-R and its methyl esterwere 0.005㎎/㎏ and 0.01㎎/㎏ for soil and soybean samples respectively.

  • PDF

Evaluation of Deformation Characteristics and Vulnerable Parts according to Loading on Compound Behavior Connector (복합거동연결체의 하중재하에 따른 변형 특성 및 취약부위 산정)

  • Kim, Ki-Sung;Kim, Dong-wook;Ahn, Jun-hyuk
    • Journal of the Society of Disaster Information
    • /
    • v.15 no.4
    • /
    • pp.524-530
    • /
    • 2019
  • Purpose: In this paper, we construct a detailed three-dimensional interface element using a three-dimensional analysis program, and evaluate the composite behavior stability of the connector by applying physical properties such as the characteristics of general members and those of reinforced members Method: The analytical model uses solid elements, including non-linear material behavior, to complete the modeling of beam structures, circular flanges, bolting systems, etc. to the same dimensions as the design drawing, with each member assembled into one composite behavior linkage. In order to more effectively control the uniformity and mesh generation of other element type contact surfaces, the partitioning was performed. Modeled with 50 carbon steel materials. Results: It shows the displacement, deformation, and stress state of each load stage by the contact adjoining part, load loading part, fixed end part, and vulnerable anticipated part by member, and after displacement, deformation, The effect of the stress distribution was verified and the validity of the design was verified. Conclusion: Therefore, if the design support of the micro pile is determined based on this result, it is possible to identify the Vulnerable Parts of the composite behavior connector and the degree of reinforcement.

Characteristic of Mixing and DO Concentration Distribution in Aeration Tank by Microbubble Supply (마이크로버블 공급에 의한 폭기조내 교반과 용존산소 분포 특성)

  • Lim, Ji-young;Kim, Hyun-Sik;Park, Dae-Seok;Cho, Young-Gun;Song, Seung-Jun;Park, Soo-Young;Kim, Jin-Han
    • Journal of the Korea Academia-Industrial cooperation Society
    • /
    • v.17 no.5
    • /
    • pp.251-259
    • /
    • 2016
  • This study examined the DO concentration distribution and ORP distribution using microbubbles on pilot-scale aeration tanks. As a result of MLSS mixing and oxygen transfer phenomenon using microbubbles, different DO concentrations were observed depending on the circulation of the liquid with the microbubble supply location on the lateral of an aeration tank. The simulation results of CFD (computational fluid dynamics) program showed that MLSS mixed with a microbubble supply in the middle the reactor is much better than on the left side of the reactor. A single reactor containing an anaerobic, anoxic, and aerobic zone, was evaluated without partition according to the location of the microbubble supply based on the experiments and CFD analysis. MLSS was separated into solid-liquid by the microbubble supply in the aeration tank. Consequently, selecting the appropriate microbubble size is important for MLSS mixing and was maintained at the proper DO concentration for biological treatment.

Path-based In-network Join Processing for Event Detection and Filtering in Sensor Networks (센서 네트워크에서 이벤트 검출 및 필터링을 위한 경로기반 네트워크-내 조인 프로세싱 방법)

  • Jeon, Ju-Hyuk;Yoo, Jae-Soo;Kim, Myoung-Ho
    • Journal of KIISE:Databases
    • /
    • v.33 no.6
    • /
    • pp.620-630
    • /
    • 2006
  • Event-detection is an important application of sensor networks. Join operations can facilitate event-detection with a condition table predefined by a user. When join operations are used for event-detection, it is desirable, if possible, to do in-network join processing to reduce communication costs. In this paper, we propose an energy-efficient in-network join algorithm, called PBA. In PBA, each partition of a condition table is stored along the path from each node to the base station, and then in-network joins are performed on the path. Since each node can identify the parts to store in its storage by its level, PBA reduces the cost of disseminating a condition table considerably Moreover, while the existing method does not work well when the ratio of the size of the condition table to the density of the network is a little bit large, our proposed method PBA does not have such a restriction and works efficiently in most cases. The results of experiments show that PBA is efficient usually and especially provides significant cost reduction over existing one when a condition table is relatively large in comparison with the density of the network, or the routing tree of the network is high.