• Title/Summary/Keyword: Particulate material

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Fabrication of Fe-TiC Composite Powder by High-Energy Milling and Subsequent Reaction Synthesis (고에너지 밀링 및 합성반응에 의한 Fe-TiC 복합분말 제조)

  • Ahn, Ki-Bong;Lee, Byung-Hun;Lee, Young-Hee;Khoa, Hyunh Xuan;Kim, Ji-Soon
    • Journal of Powder Materials
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    • v.20 no.1
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    • pp.53-59
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    • 2013
  • Fe-TiC composite powder was fabricated via two steps. The first step was a high-energy milling of FeO and carbon powders followed by heat treatment for reduction to obtain a (Fe+C) powder mixture. The optimal condition for high-energy milling was 500 rpm for 1h, which had been determined by a series of preliminary experiment. Reduction heat-treatment was carried out at $900^{\circ}C$ for 1h in flowing argon gas atmosphere. Reduced powder mixture was investigated by X-ray Diffraction (XRD), Field Emission-Scanning Electron Microscopy (FE-SEM) and Laser Particle Size Analyser (LPSA). The second step was a high-energy milling of (Fe+C) powder mixture and additional $TiH_2$ powder, and subsequent in-situ synthesis of TiC particulate in Fe matrix through a reaction of carbon and Ti. High-energy milling was carried out at 500 rpm for 1 h. Heat treatment for reaction synthesis was carried out at $1000{\sim}1200^{\circ}C$ for 1 h in flowing argon gas atmosphere. X-ray diffraction (XRD) results of the fabricated Fe-TiC composite powder showed that only TiC and Fe phases exist. Results from FE-SEM observation and Energy-Dispersive X-ray Spectros-copy (EDS) revealed that TiC phase exists uniformly dispersed in the Fe matrix in a form of particulate with a size of submicron.

Histological comparison of different compressive forces on particulate grafts during alveolar ridge preservation: a prospective proof-of-concept study

  • Lee, Sung-Jo;Kang, Dae-Young;Cho, In-Woo;Shin, Hyun-Seung;Shin, Seung-Il;Fischer, Kai R.;Park, Jung-Chul
    • Journal of Periodontal and Implant Science
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    • v.50 no.3
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    • pp.197-206
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    • 2020
  • Purpose: The aim of this study was to determine the impact of different compressive forces on deproteinized bovine bone mineral (DBBM) particles covered by native bilayer collagen membrane (NBCM) during alveolar ridge preservation (ARP) in the molar area, and to identify any histomorphometric and clinical differences according to the compressive force applied. Methods: Sockets were filled with DBBM after tooth extraction, and different compressive forces (30 N and 5 N, respectively) were applied to the graft material in the test (30 N) and control (5 N) groups. The DBBM in both groups was covered with NBCM in a double-layered fashion. A crossed horizontal mattress suture (hidden X) was then made. A core biopsy was performed using a trephine bur without flap elevation at the implant placement site for histomorphometric evaluations after 4 months. The change of the marginal bone level was measured using radiography. Results: Twelve patients completed the study. The histomorphometric analysis demonstrated that the mean ratios of the areas of new bone, residual graft material, and soft tissue and the implant stability quotient did not differ significantly between the groups (P>0.05). However, the mean size of the residual graft material showed a significant intergroup difference (P<0.05). Conclusions: The application of 2 compressive forces (5 N, 30 N) on particulate DBBM grafts during open-healing ARP in the posterior area led to comparable new bone formation, implant feasibility and peri-implant bone level.

Surface Analysis of Fluorine-Plasma Etched Y-Si-Al-O-N Oxynitride Glasses

  • Lee, Jung-Ki;Hwang, Seong-Jin;Lee, Sung-Min;Kim, Hyung-Sun
    • Proceedings of the Materials Research Society of Korea Conference
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    • 2009.05a
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    • pp.38.1-38.1
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    • 2009
  • Plasma etching is an essential process for electronic device industries and the particulate contamination during plasma etching has been interested as a big issue for the yield of productivity. The oxynitride glasses have a merit to prevent particulate contamination due to their amorphous structure and plasma etching resistance. The YSiAlON oxynitride glasses with increasing nitrogen content were manufactured. Each oxynitride glasses were fluorine-plasma etched and their plasma etching rate and surface roughness were compared with reference materials such as sapphire, alumina and quartz. The reinforcement mechanism of plasma etching resistance of the YSiAlON glasses studied by depth profiling at plasma etched surface using electron spectroscopy for chemical analysis. The plasma etching rate decreased with nitrogen content and there was no selective etching at the plasma etched surface of the oxynitride glasses. The concentration of silicon was very low due to the generation of SiF4 very volatile byproduct and the concentration of aluminum and yttrium was relatively constant. The elimination of silicon atoms during plasma etching was reduced with increasing nitrogen content because the content of the nitrogen was constant. And besides, the concentration of oxygen was very low on the plasma etched surface. From the study, the plasma etching resistance of the glasses may be improved by the generation of nitrogen related structural groups and those are proved by chemical composition analysis at plasma etched surface of the YSiAlON oxynitride glasses.

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Fabrication of High-performance Carbon Counter Electrode for Dye-sensitized Solar Cells (염료감응 태양전지용 고성능 탄소 상대전극 제작)

  • Jang, Yeon-Ik;Lee, Seung-Yong;Kim, Dong-Hwan;Park, Jong-Ku
    • Journal of Powder Materials
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    • v.14 no.1 s.60
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    • pp.44-49
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    • 2007
  • In the fabrication of dye-sensitized solar cells (DSSCs), carbon counter electrode has been tested for replacing the platinum counter electrode which has two drawbacks: limited surface area and high material cost. Poor mechanical stability of carbon layer due to weak bonding strength to electrically conductive TCO (transparent conducting oxide) glass substrate is a crucial barrier for practical application of carbon counter electrode. In the present study a carbon counter electrode with high conversion efficiency, comparable to Pt counter electrode, could be fabricated by adaption of a bonding layer between particulate carbon material and TCO substrate.

Assessment of Inhalation Dose Sensitivity by Physicochemical Properties of Airborne Particulates Containing Naturally Occurring Radioactive Materials (천연방사성물질을 함유한 공기 중 부유입자 흡입 시 입자의 물리화학적 특성에 따른 호흡방사선량 민감도 평가)

  • Kim, Si Young;Choi, Cheol Kyu;Park, Il;Kim, Yong Geon;Choi, Won Chul;Kim, Kwang Pyo
    • Journal of Radiation Protection and Research
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    • v.40 no.4
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    • pp.216-222
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    • 2015
  • Facilities processing raw materials containing naturally occurring radioactive materials (NORM) may give rise to enhanced radiation dose to workers due to chronic inhalation of airborne particulates. Internal radiation dose due to particulate inhalation varies depending on particulate properties, including size, shape, density, and absorption type. The objective of the present study was to assess inhalation dose sensitivity to physicochemical properties of airborne particulates. Committed effective doses to workers resulting from inhalation of airborne particulates were calculated based on International Commission on Radiological Protection 66 human respiratory tract model. Inhalation dose generally increased with decreasing particulate size. Committed effective doses due to inhalation of $0.01{\mu}m$ sized particulates were higher than doses due to $100{\mu}m$ sized particulates by factors of about 100 and 50 for $^{238}U$ and $^{230}Th$, respectively. Inhalation dose increased with decreasing shape factor. Shape factors of 1 and 2 resulted in dose difference by about 18 %. Inhalation dose increased with particulate mass density. Particulate mass densities of $11g{\cdot}cm^{-3}$ and $0.7g{\cdot}cm^{-3}$ resulted in dose difference by about 60 %. For $^{238}U$, inhalation doses were higher for absorption type of S, M, and F in that sequence. Committed effective dose for absorption type S of $^{238}U$ was about 9 times higher than dose for absorption F. For $^{230}Th$, inhalation doses were higher for absorption type of F, M, and S in that sequence. Committed effective dose for absorption type F of $^{230}Th$ was about 16 times higher than dose for absorption S. Consequently, use of default values for particulate properties without consideration of site specific physiochemical properties may potentially skew radiation dose estimates to unrealistic values up to 1-2 orders of magnitude. For this reason, it is highly recommended to consider site specific working materials and conditions and use the site specific particulate properties to accurately access radiation dose to workers at NORM processing facilities.

입자자기기록재료

  • 양창선
    • Electrical & Electronic Materials
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    • v.1 no.3
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    • pp.184-196
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    • 1988
  • 통칭 particulate media(P.M.)로 일컬어지는 입자형 기록매체는 자성재료가 개개의 particle로 구성되는 자기 기록매체를 말한다. 이 P.M.는 20네기초 정보기록매체로서 steel wire, steel tape이후 등장하여 현재까지 가장 광범위하게 사용되고 있다. P.M.를 포함한 자기 기록매체의 발전사를 요약해 보면 표1과 같다. P.M.중에서도 자기 tape가 차지하는 비중은 절대적이며 특히 viedo tape는 전체 자성체사용량의 약 55%를 점하면서 대량생산에 의한 고품질, 저가격의 장점을 전세계 소비자에게 제공하고 있다. 여기서는 P.M.의 기본물성을 좌우하는 자성체에 대하여 알아보고 P.M.를 품목별로 소개한 다음, P.M.중 가장 많은 생산량을 나타내고 있는 viedo tape의 제조과정을 소개하고자 한다.

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On the Relationship between Material Removal and Interfacial Properties at Particulate Abrasive Machining Process (연마가공에서의 접촉계면 특성과 재료제거율간의 관계에 대한 연구)

  • Sung, In-Ha
    • Tribology and Lubricants
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    • v.25 no.6
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    • pp.404-408
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    • 2009
  • In this paper, the relationship between the material removal rate and the interfacial mechanical properties at particle-surface contact situation, which can be seen in an abrasive machining process using micro/nano-sized particles, was discussed. Friction and stiffnesses were measured experimentally on an atomic force microscope (AFM) by using colloidal probes which have a silica colloid particle in place of tip to simulate a particle-flat surface contact in an abrasive machining process. From the experimental investigation and theoretical contact analysis, the interfacial contact properties such as lateral stiffness of contact, friction, the material removal rate were presented with respect to some of material surfaces and the relationship between the properties as well.

Algal Pigments and their Degradation Products in Suspended and Sinking Particulate Material in the Gulf of Mexico (멕시코 만의 부유 및 침강고형물에 존재하는 조류색소 및 그 분해산물)

  • Noh, Il
    • Journal of Environmental Science International
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    • v.5 no.2
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    • pp.153-170
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    • 1996
  • Photosynthetic pigments and their degradation products in suspended and sinking particles collected from the Gulf of Mexico waters 1987~88, were measured using High Performance liquid Chromatography (HPIC). The short term variations in flux rates of chlorophylls and carotenoids as well as-their degradation products were compared at the mesoscale cyclonic and anticyclonic circulation features (cold joie rink and warm core ring). Chlorophyll a was the predominant porphyrin of suspended particulate matter at both CCR -and WCR. Among carotenoid pigments, 19'-hexanoyloxyfucoxanthin, which is a biomarker of prymnesiophytes, was dominant pigment at both rinds. Phaeophorbide a, which is produced through the Brazing processes of grazers, was the predominant degraded pigment in sinking particles ai the study aiea. Total pigment flux in CCR was an order of magnitude higher than that in WCR. Less than l% of the standing stock of the pigments measured sank out of the upper 200m of the WCR on any given day. Thus, suspended particulate matter in Gulf of Medico was not recycled rapidly.

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An Experimental Study on Effects of Soot Loading and Mass Flow Rate on Pressure Drop and Heat Transfer in Catalyzed Diesel Particulate Filter (촉매 코팅 DPF의 soot loading과 유량 변화에 따른 압력강하 및 열전달에 관한 실험적 연구)

  • Cho, Yong-Seok;Noh, Young-Chang;Park, Young-Joon;Kim, Duk-Sang
    • Transactions of the Korean Society of Automotive Engineers
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    • v.15 no.3
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    • pp.72-78
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    • 2007
  • A diesel particulate filter causes progressive increase in back pressure of an exhaust system due to the loading of soot particles. To maintain the pressure drop caused by DPF under proper level, a regeneration process is mandatory when excessive loading of soot is detected in the filter. It is a major reason why the relation between the amount of soot and the pressure drop in a DPF becomes crucial. On the other hand, pressure drop varies with not only the soot loading but also conditions of exhaust gas such as mass flow rate. Therefore, the relation among them becomes complicated. Furthermore, the characteristics of heat transfer in a DPF is another crucial parameter in order for the filter to avoid thermal crack during regeneration period. This study presents characteristics of pressure drop under various conditions of soot loading and mass flow rate in catalyzed diesel particulate filter. This study also shows characteristics of heat transfer in DPF when high temperature gas flows into the filter. Experiments reveal that the soot loading and mass flow rate affect characteristics pressure drop independently. Experiments also indicate that the amount of coating material has little influence on pressure drop with changes in soot loading and mass flow rate. However, increased catalyst coating may lead to the improved heat transfer which is efficiency to reduce thermal stress of the filter.

Fracture Energy and Displacement Field Characteristics of Particulate Reinforced Composites Using DIC Method (DIC법에 의한 입자강화 복합재료의 파괴에너지 및 변위장 특성)

  • Lee, Jeongwon;Na, Seonghyeon;Lee, Sangyoun;Park, Jaebeom;Jung, Gyoodong;Kim, Jaehoon
    • Journal of the Korean Society of Propulsion Engineers
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    • v.21 no.6
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    • pp.15-20
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    • 2017
  • In this study, the fracture energy and displacement fields characteristics of particulate reinforced composite is evaluated. Wedge splitting test was performed at various temperatures. Fracture energy of material is calculated at room temperature, $-40^{\circ}C$ and $-60^{\circ}C$. Displacement and strain fields of specimen surface were visualized by using digital image correlation. The surface displacement fields of the specimens were analyzed by mark tracking method using digital image correlation. The results showed that, the fracture energy was decreased as temperature decreased. The surface displacement fields at room temperature were similar to there at $-40^{\circ}C$. The surface displacement fields at $-60^{\circ}C$ was significantly reduced because of the brittle behavior. The strain fields of the specimen surface decreased as temperature decreased form room temperature to $-60^{\circ}C$.