• Title/Summary/Keyword: Particle size of spray

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Atomization Characteristics of Effervescent Atomizer with the Variations of Operating Conditions (작동조건 변화에 따른 기체주입미립화기의 미립화 특성)

  • Kim, Hyung-Gon;Yano, Toshiaki;Song, Kyu-Keun
    • Proceedings of the KSME Conference
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    • 2003.11a
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    • pp.869-874
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    • 2003
  • The atomization characteristics were investigated through the influence of the change of GLR and the change of working fluid on droplet size distribution and mean diameter of drop produced by effervescent atomizer. For simultaneous injection of water and high viscous waste vegetable oil, effervescent atomizer with two aerator tubes was specially designed. From the experimental results, regardless of mass fraction of vegetable oil in working fluids, it is expected that effervescent atomizer will exhibit excellent atomization performance at the high GLR conditions.

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Effect of Grain Growth Inhibitor on Sintering of Nanophase WC-10wt%Co (초미립 WC-l0wt%Co 초경 분말의 소결시 입자 성장 억제제 첨가 효과 연구)

  • 김병기
    • Journal of Powder Materials
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    • v.1 no.2
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    • pp.208-216
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    • 1994
  • A radically new approach to the in situ synthesis of the consituent phases of a composite structure has enabled the production of a new WC/Co materials with an ultrafine microstructure. The process for synthesizing nanophase WC/Co powders consists of spray drying from solution to form a homogeneous precursor powder, and thermochemical conversion of the precursor powder to the nanophase WC/Co powder. Near theoretical density of pure nanophase WC-10 wt%Co has been obtained in only 30 sec at 140$0^{\circ}C$. But WC particles were grown up very rapidly with longer sintering time to get full density. To overcome coarsening of WC particle during sintering, VC, TaC and VC/TaC were used as the grain growth inhibitor with different amount respectively. VC/TaC doped WC-10 wt%Co was shown superior hardness and TRS and microstructure was maintained ultrafine scale (average WC size is less than 0.1 ${\mu}{\textrm}{m}$).

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Spherical-shaped Zn2SiO4:Mn Phosphor Particles with Gd3+/Li+ Codopant (Gd3+/Li+ 부활성제가 첨가된 구형의 Zn2SiO4:Mn 형광체 입자)

  • Roh, Hyun Sook;Lee, Chang Hee;Yoon, Ho Shin;Kang, Yun Chan;Park, Hee Dong;Park, Seung Bin
    • Korean Chemical Engineering Research
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    • v.40 no.6
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    • pp.752-756
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    • 2002
  • Green-emitting $Zn_2SiO_4:Mn$ phosphors for PDP(Plasma Display Panel) application were synthesized by colloidal seed-assisted spray pyrolysis process. The codoping with $Gd^{3+}/Li^+$, which replaces $Si^{4+}$ site in the willemite structure, was performed to improve the luminous properties of the $Zn_2SiO_4:Mn$ phosphors. The particles prepared by spray pyrolysis process using fumed silica colloidal solution had a spherical shape, small particle size, narrow size distribution, and non-aggregation characteristics. The $Gd^{3+}/Li^+$ codoping amount affected the luminous characteristics of $Zn_2SiO_4:Mn$ phosphors. The codoping with proper amounts of $Gd^{3+}/Li^+$ improved both the photoluminescence efficiency and decay time of $Zn_2SiO_4:Mn$ phosphor particles. In spray pyrolysis, the post-treatment temperature is another factor controlling the luminous performance of $Zn_2SiO_4:Mn$ phosphors. The $Zn_{1.9}SiO_4:Mn_{0.1}$ phosphor particles containing 0.1 mol% $Gd^{3+}/Li^+$ co-dopant had a 5% higher PL intensity than the commercial product and 5.7 ms decay time after post-treatment at $1,145^{\circ}C$.

Improvements in the Physical Properties of Agglomerated Milk Protein Isolate/Skim Milk Powder Mixtures Via Fluidized Bed Agglomeration

  • Seo, Chan Won
    • Journal of Dairy Science and Biotechnology
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    • v.40 no.3
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    • pp.134-142
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    • 2022
  • Protein-enriched dairy powder is widely consumed to promote muscle synthesis. Recently, in Korea, elderly people have also begun consuming protein powder products to prevent muscle loss. However, these protein-enriched powders have poor flowability and hydration properties because of the fine particles of spray-dried milk protein powder. Therefore, in this study, the fluidized bed agglomeration process was used to solve these problems. The rheological and physical properties of milk protein isolate (MPI)/skim milk powder (SMP) mixtures were effectively improved via fluidized bed agglomeration. The particle size of the MPI/SMP mixtures significantly increased from 35.7-58 ㎛ to 118-136 ㎛, the flowability level improved from fair (21.4-26.3) to good (15.7-16.3), and the cohesiveness level changed from intermediate (1.27-1.36) to low (1.18-1.19) after fluidized bed agglomeration. In addition, the wetting time of the agglomerated MPI/SMP mixtures was effectively reduced to 4.67-58.3 s by fluidized bed agglomeration. These findings may be useful for manufacturing protein-enriched dairy powders with good instant properties.

Synthesis of Cu/Al2O3 Nanostructured Composite Powders for Electrode Application by Thermochemical Process (열화학적 방법에 의한 전극용 나노 Cu/Al2O3 복합분말 합성)

  • 이동원;배정현;김병기
    • Journal of Powder Materials
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    • v.10 no.5
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    • pp.337-343
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    • 2003
  • Nanostructured Cu-$Al_2O_3$ composite powders were synthesized by thermochemical process. The synthesis procedures are 1) preparation of precursor powder by spray drying of solution made from water-soluble copper and aluminum nitrates, 2) air heat treatments to evaporate volatile components in the precursor powder and synthesis of nano-structured CuO + $Al_2O_3$, and 3) CuO reduction by hydrogen into pure Cu. The suggested procedures stimulated the formation of the gamma-$Al_2O_3$, and different alumina formation behaviors appeared with various heat treating temperatures. The mean particle size of the final Cu/$Al_2O_3$ composite powders produced was 20 nm, and the electrical conductivity and hardness in the hot-extruded bulk were competitive with Cu/$Al_2O_3$ composite by the conventional internal oxidation process.

A Synthesis and Characteristics for ZrO2-Y2O3 System Powders by Coprecipitation Method ; I. The Properties and Sinterabilities of ZrO2-8m/o Y2O3 (공침법에 의한 ZrO2-Y2O3계 분말합성 및 특성;I. ZrO2-8m/o Y2O3의 특성 및 소결성)

  • 방대규;윤종석;이희수
    • Journal of the Korean Ceramic Society
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    • v.26 no.2
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    • pp.242-248
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    • 1989
  • The powder properties and sinterability of ZrO2-8m/o Y2O3 prepared by coprecipitation were investigated. The specific surface area and the total pore volume were increased with increasing pH of sediment and using of ethyl alcohol for washing. The powders of prepared by freeze drying method were showed the smallest particle size and lowest agglomerate rate, and the powders obtained from spray drying method were showed porous structure. At 130$0^{\circ}C$, their relative density were 94-96%, so these sintered bodies have revealed high sinterability in spite of low sintering temperature.

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A Study on the Characteristics Analysis of Cutting Fluid Aerosol Using Dual-PDA System(II) - for Cutting Fluid Aerosol Prediction in Turning Process (Dual-PDA를 이용한 절삭유 에어로졸 특성분석에 관한 연구(II) - 선삭공정의 절삭유 에어로졸 예측)

  • Chung, E.S.;Hwang, D.C.;Woo, C.K.;Hwang, J.
    • Journal of ILASS-Korea
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    • v.10 no.2
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    • pp.32-40
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    • 2005
  • This paper presents the analytical approaches to predict cutting fluid aerosol formation characteristics in machining process. The prediction model which is based on the rotary atomization theory analyzes aerosol behaviors in terms of size and concentration. Experiments were tarried out to verify the aerosol formation prediction model under various operational conditions. The experimental results which are obtained by Dual-PDA measurement show resonable agreement with prediction results of aerosol concentration. This study can be provided as a basis to estimate and control the hazardous cutting fluid aerosol in machining process in view of environmental consciousness.

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Effect of Particle Size of Tungsten Powder on the Properties of Vacuum Plasma Sprayed Tungsten coatings

  • Kim, Ho-Seok;Mun, Se-Yeon;Hong, Bong-Geun
    • Proceedings of the Korean Vacuum Society Conference
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    • 2016.02a
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    • pp.205.1-205.1
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    • 2016
  • 핵융합로에서 고온, 고에너지 플라즈마에 장기간 노출되는 플라즈마 대면재는 고속 입자와 중성자에 의한 열화 및 침식과 높은 열부하를 견뎌야 하므로 높은 수준의 재료기술과 표면 코팅기술의 개발이 필요하다. 텅스텐은 용융점이 높고, 스퍼터링(Sputtering) 현상이 적으며, Tritium 재침적 현상이 제한되는 우수한 특성 때문에 핵융합로 대면제에 적용하기 위한 다양한 연구가 진행되고 있다. 본 연구에서는 VPS(vacuum plasma spray) 장비를 이용하여 5, 10, $25{\mu}m$ 크기의 텅스텐 분말을FM(ferritic-martenitic) steel 기판에 용사 코팅하였다. 입자 크기를 달리하여 제작한 3종의 시편은 시편 전후 두께 및 무게 변화, 현미경이미지, 비커스 경도, 3D 표면 형상, XRD를 이용하여 코팅층의 특성을 평가하였으며, $10{\mu}m$ 크기의 텅스텐 분말 시편이 가장 우수한 특성을 나타내는 것을 확인하였다.

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ENHANCED BIOAVAILABILITY OF NIFEDIPINE USING COATED DRY ELIXIR

  • Park, Jae-Yoon;Kim, Chong-Kook
    • Proceedings of the Korean Society of Applied Pharmacology
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    • 1996.04a
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    • pp.282-282
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    • 1996
  • The purpose of this study was to prepare the nifedipine dry elixir (NDE) and coated nifedipine dry elixir (CNDE) containing nifedipine ethanol solution for improving the dissolution rate and bioavailability of nifedipine. NDE containing nifedipine and ethanol in wall materials of dextrin was prepared using a spray-dryer and then NDE was coated with eudragit acrylic resin to make CNDE. Shape and size of the NDE and CNDE were monitored by scanning electron micrograph and laser particle size analyzer In vitro dissolution tests were performed in simulated gastric and intestinal fluid. Bioavailability of NDE and CNDE were compared with drug powder suspension and commercial soft capsule after oral administration of the preparations to rats. NDE and CNDE are spherical in shape. Cross-sectional view of dry elixirs indicates the large inter cavity containing ethanolic drug solution in shell. Geometric mean diameter of NDE and CNDE is about 6.64 and 8.70 $\mu\textrm{m}$, respectively. Drug dissolution rate within first 5 min from NDE increased dramatically irrespective of dissolution medium. However, CNDE showed a particularly retarded dissolution rate in pH 1.2 simulated gastric fluid compared with NDE. The bioavailability of nifedipine in the NDE was increased dramatically compared with drug powder suspension. CNDE reduced initial burst-out plasma peak compared with NDE. CNDE as a sustained release delivery system could reduce the initial burst-out plasma peak due to controlling the release rate of nifedipine from NDE and maintain the effective plasma level over a longer period within therapeutic window with enhanced bioavailability of nifedipine.

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Experimental Study for the Optimum Conditions of Painting Using Phase Doppler Particle Analyzer (PDPA를 이용한 도장의 최적 조건에 관한 실험)

  • 황승식;김종철;하옥남;전운학;정회원
    • Transactions of the Korean Society of Automotive Engineers
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    • v.5 no.4
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    • pp.1-20
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    • 1997
  • The automotive industry as the major industry of the nation has affected both society and economy since the automobile was invented, and the main technique that help to performance improvement of the automobile has been developed. But, the painting technique lags behind the main technique of the automobile because that was neglected. Specially, we can say that in case of the painting technique of the automobile of our nation is so weak situation. After we changed the injecting pressure, the composition ratio (paint, hardener, thinner) and the injecting flow rate from spray-gun by PDPA, we studied the character of the injecting velocity and droplet size, and found the fittest condition. So, we got the following result to help mending paint technique of automobile surface. We could know the following fact from the experiment result. When it does mending paint of automobile, there is most suitable that to inject the paint as injecting pressure 200∼300 kPa and to inject the ratio of paint 10 : 1 : 1 when the fluid adjective knob valve spay-gun is open full.

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