• 산업기술연구
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• 제21권B호
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• pp.149-153
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• 2001

A study on the particle growth in $TEOS/O_2$ plasma was performed, and particle size and its distribution was measured by the electrical aerosol analyzer (EAA), light scattering particle size analyzer and the particle size was also determined by SEM. The effects of process variables such as total gas flow rate, reactor pressure, supplied power and initial reactant concentration on the particle growth were investigated. From the EAA results, the particle size distribution is divided into three groups of the cluster size and the small and large size particles. The particle size distribution measured by the light scattering particle size analyzer becomes bimodal, because the cluster size particles smaller than 20 nm in diameter cannot be detected by the light scattering particle size analyzer. The size of particles measured by the light scattering particle size analyzer is in good agreements with those by the SEM. Also we could understand that the particle formation is very sensitive to the changes of reactor pressure and reactant concentration. As the total gas flow rate increases, the particle size decreases because of the shorter residence time. As the reactor pressure, or the reactant concentration increases, the particle concentration increases and the particles grow more quickly by the faster coagulation between particles.

• 한국분말야금학회:학술대회논문집
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• 한국분말야금학회 2006년도 Extended Abstracts of 2006 POWDER METALLURGY World Congress Part 1
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• pp.18-19
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• 2006

To improve the properties of fine metal powder, such as particle size distribution and geometric standard deviation, this work was done at various atomizing conditions. The new atomization mechanism and the correlation equation were proposed to estimate the mean particle diameter.

• 한국추진공학회:학술대회논문집
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• 한국추진공학회 2008년도 제31회 추계학술대회논문집
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• pp.171-174
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• 2008

소형 회전연료 분사장치의 분열과정 특성을 연구하기 위한 실험적 연구를 수행하였다. 이러한 분열과정의 특성을 이해하기 위해 PDPA(Phase Doppler Particle Analyzer)시스템을 사용하여 분무입자의 크기와 속도를 측정하였다. 또한 Nd-Yag Laser를 광원으로 사용하여 분무를 가시화하였다. 실험결과 Injection Orifice로부터 생성된 액주는 회전수에 의해 지배되고, SMD(Sauter Mean Diameter)와 분무특성은 Injection Orifice의 직경에 큰 영향을 받는다는 것을 알 수 있었다.

• Journal of Biosystems Engineering
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• 제20권3호
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• pp.236-244
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• 1995

Droplet size is one of the important factors in the deposition and drift of agrichemical application. In this study, droplet size and its distribution of the three different sizes of ceramic hollow cone nozzles being used in the air carrier sprayer for apple production were investigated at the various nozzle pressures and the three air velocities. The Malvern particle size analyzer were used for the measurement of droplet size and its distribution. The important results emerged from th is study can be summarized as follows. 1. Discharged rate was increase with the increase of the nozzle diameter and pressure, amount of the difference was remarkable between the nozzle diameter of 1.0, 1.2 and 1.5 mm, but no difference were found between the diameter of 1.0 and 1.2 mm in the same nozzle pressure. 2. Mass median diameter were varied as 40~160 ${mu}m$ at the air velocity of 0 m/s, 70~140 ${mu}m$ of 15 m/s and 100~160 ${mu}m$ of 20 m/s 3. It appeared that the air velocity range of 15~20 m/s was desirable for both drift and deposition control in the given experimental conditions.

• 한국대기환경학회지
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• 제2권2호
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• pp.60-65
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• 1986

Atmospheric particulates were collected at a site near the front gate of the Yonsei University using nine stages Andersen air sampler and the distribution of seasonal particle size was investigated. Rubber, Pb and Zn contents of the collected particulates in each stage were determined. Particle size distribution of atmospheric particulate, which was made by concentration distribution curve method, was usually divided into two groups, course (particles larger than 1 - 2 $\mu m in diameter$) and fine (particles smaller than 1 - 2 \mu m in diameter$) groups, regardless of sampling period. More than 80 percent of the total rubber contents in atmospheric particulates were larger than $5 \mu m$ in diameter, meaning that most of rubber particles were originated from tire tread. After benzene extraction for 4 hrs, the extracts were analyzed by Curie-point pyrolysis gas chromatography for rubber content. Pb and Zn contents were determined by atomic absorption spectroscopy. The annual average concentration of rubber particles was $4.2 \mu g/m^3$, which corresponded to 2.2% of the annual average total suspended particulates. Average concentration of styrene brtadiene rubber was about five times that of natural rubber. Annual average concentrations of Pb and Zn were $1.2 \mu g/m^3 and 0.4 \mu g/m^3$ respectively, which corresponded to about 0.7% and 0.2% of the annual average total suspended particulates.

• 한국분무공학회지
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• 제6권2호
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• pp.16-21
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• 2001

This paper describes the macroscopic behavior and atomization characteristics of the high-pressure gasoline swirl injector in direct-injection gasoline engine. The global spray behavior of fuel injector was visualized by shadowgraph technique. The atomization characteristics of gasoline spray such as mean diameter and mean velocity of droplets were measured by the phase Doppler particle analyzer system. The macroscopic visualization and experiment of particle measurement on the fuel spray were investigated at 7 and 10 MPa of injection pressure under different spray cone angle. The results of this work show that the geometry of injector was more dominant over the macroscopic characteristics of spray than the fuel injection pressure and injection duration. As for the atomization characteristics, the increase of injection pressure resulted in the decrease of fuel droplet diameter and the atomization characteristics differed as to the spray cone angle. The most droplets had under $25{\mu}m$ diameter and for the large droplets(upper $40{\mu}m$) as the spray grew the atomization presses were very slow. Comparison results between the measured droplet distribution and the droplet distribution functions revealed that the measured droplet distribution is very closed to the Normal distribution function and Nukiyama-Tanasawa's function.

• Macromolecular Research
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• 제17권1호
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• pp.51-57
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• 2009

Using glycidyl methacrylate-linked poly(dimethylsiloxane), methyl methacrylate was polymerized in supercritical $CO_2$. The effects of $CO_2$ pressure, reaction time, and mixing on the yield, molecular weight, and molecular weight distribution (MWD) of the poly(methyl methacrylate) (PMMA) products were investigated. The shape, number average particle diameter, and particle size distribution (PSD) of the PMMA were characterized. Between 69 and 483 bar, the yield and molar mass of the PMMA products showed a trend of increasing with increasing $CO_2$ pressure. However, the yield leveled off at around 345 bar and the particle diameter of the PMMA increased until the pressure reached 345 bar and decreased thereafter. With increasing pressure, MWD became more uniform while PSD was unaffected. As the reaction time was extended at 207 bar, the particle diameter of PMMA decreased at $0.48{\pm}0.03%$ AIBN, but increased at 0.25% AIBN. Mixing the reactant mixture increased the PMMA yield by 18.6% and 9.3% at 138 and 207 bar, respectively.

• 한국인쇄학회지
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• 제16권2호
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• pp.11-22
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• 1998

For the purpose of preparation of monodispersed spherical zinc oxide fine particles, an experimental research on the preparation of zinc oxide particles from zinc salts solutions by high temperature precipitation reaction was performed. Zinc oxide particles were precipitated from all the precipitation solutions tested if the precipitation temperature was higher than 60$^{\circ}$. As the precipitation temperature Increased until 80$^{\circ}$, the average particle diameter of zinc oxide particles decreased and the narrower particle size distribution were obtained. Spherical zinc oxide fine particles with relatively narrow particle size distribution were precipitated from the ZnSO$_4$ solutions with NaOH as precipitant. Final pH of precipitation solution had an effect on the amount of zinc oxide precipitated, but had no effect on the their particle size or size distribution.

• 한국분말재료학회지
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• 제20권2호
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• pp.129-133
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• 2013

In this paper we have studied the effect of water droplet size on nano-particle size distribution using SMPS(Scanning Mobility Particle Sizer)system. It can be seen that the unknown peak at >100 nm was caused by water droplets which did not dry completely when DI water was used as a solvent in the SMPS system. Therefore, it is important to dry water droplets generated from atomizer in the SMPS system when measuring the particle size distribution using less than 100 nm nano-particles in diameter. From this study, It can be concluded that the napion was a useful material as dryer ones and using EAG(Electro Aerosol Generator) as a particle generator was the most effective in reducing the effect of water droplets.

• 대한기계학회논문집B
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• 제21권3호
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• pp.380-391
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• 1997

A numerical study has been done on the evolution of particle size distribution in particle laden high temperature jet flows undergoing convection, diffusion, thermophoresis and coagulation. The dynamic behavior of these particles have been modelled by approximating the particle size distribution by a lognormal function throughout the process and the moments of the particle size distribution have been used to solve the general dynamic equation. The size distributions of spherical particles in the radial and axial direction have been obtained including the effect of buoyancy. Of particular interests are the variations of geometric mean diameter, number concentration and polydispersity. Results show that buoyancy significantly alters the size distribution in both axial and radial direction. One dimensional analysis for non-spherical particles has also been done and the results have been compared with the existing experimental data.