• 제목/요약/키워드: Particle Sizing

검색결과 36건 처리시간 0.021초

Characterization of the PAC Modified Cationic Rosin Size and its Sizing Effect

  • Yan, Yong-Xiang;Chandranupap, Fu-Shan;Wang, Gao-Sheng
    • 한국펄프종이공학회:학술대회논문집
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    • 한국펄프종이공학회 2006년도 PAN PACIFIC CONFERENCE vol.2
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    • pp.387-390
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    • 2006
  • Cationic rosin sizes are prepared by premixing extremely pure ployaluminum chloride (PAC) and dispersed rosin size (DRS). It turned out that zeta potential and particle size of the sizing agents took a big change by Plus90 analyzer's and FTIR analyzer's analysis. It turned out that -C=O and -COOH of the DRS have both chemical reaction with PAC to form the muti-hydroxyl aluminum rosin acid and that the cationic rosin sizes modified by PAC has dissymmetric and symmetric flexible vibration two absorbing peaks of the groups (its absorbing peaks $at1596cm^{-1}\;and\;1425cm^{-1}$). By DRS reacting with PAC, zeta potential of the resin size varied from negative to cationic. $Al_{2}O_{3}/rosin=1:0.3$, zeta potential of premixed admixture is tiptop28.8mv, When joined continuously PAC, zeta potential of cationic rosin sizes descend on the contrary.

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입경측정을 위한 영상처리기법에서 입자 초점면 존재 판단 기준의 설정 (Determination of In-focus Criteria In Image Processing Method for Particle Size Measurement)

  • 고광웅;김주연;이상용
    • 대한기계학회논문집B
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    • 제23권3호
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    • pp.398-407
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    • 1999
  • In the present image processing technique, the concept of the gradient indicator(GI) has been introduced to find out the depth-of-field in sizing large particles ranging from $30{\mu}m$ to $30{\mu}m$ where using of the concept of the normalized contrast value(VC) is not appropriate. The gradient indicator is defined as the ratio of the local value to the maximum possible value of the gray-level gradient in an image frame. The gradient indicator decreases with the increases of the particle size and the distance from the exact focal plane. A particle is considered to be in focus when the value of the gradient indicator at its image boundary stays above a critical value. This critical gradient indicator($GI_{critical}$) is defined as the maximum gradient indicator($GI_{max}$) subtracted by a constant ${\Delta}GI$ which is to account for the particle-size effect. In the present ca.so, the value of ${\Delta}GI$ was set to 0.28 to keep the standard deviation of the measured particles mostly within 0.1. It was also confirmed that, to find the depth-of-field for small particles(${\leq}30{\mu}m$) with the same measurement accuracy, tho concept of the critical normalized contrast($VC_{critical}$) is applicable with 85% of the maximum normalized contrast value($VC_{max}$). Finally, the depth-of-field was checked for the size range between $10{\mu}m$ and $300{\mu}m$ when the both in-focus criteria ($GI_{critical}$ and $VC_{critical}$) were adopted. The change of the depth-of-field with the particle size shows good linearity in both the VC-applicable and the GI-applicable ranges with a reasonable accuracy.

항공기 구름 관측에 사용되는 전방산란 관측 기기의 정확도 향상을 위한 구름입자의 광학적 특성 계산 (Calculations of Optical Properties of Cloud Particles to Improve the Accuracy of Forward Scattering Probes for In-Situ Aircraft Cloud Measurements)

  • 엄준식
    • 대기
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    • 제30권1호
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    • pp.75-89
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    • 2020
  • Current in-situ airborne probes that measure the sizes of ice crystals smaller than 50 ㎛ are based on the concept that the measured intensity of light scattered by a particle in the forward and/or backward direction can be converted to particle size. The relationship between particle size and scattered light used in forward scattering probes is based on Mie theory, which assumes the refractive index of particle is known and all particles are spherical. Not only are small crystals not spherical, but also there are a wide variety of non-spherical shapes. Although it is well known that the scattering properties of non-spherical ice crystals differ from those of spherical shapes, the impacts of non-sphericity on derived in-situ particle size distributions are unknown. Thus, precise relationships between the intensity of scattered light and particle size and shape are required, as based on accurate calculations of scattering properties of ice crystals. In this study, single-scattering properties of ice crystals smaller than 50 ㎛ are calculated at a wavelength of 0.55 ㎛ using a numerically exact method (i.e., discrete dipole approximation). For these calculations, hexagonal ice crystals with varying aspect ratios are used to represent the shapes of natural small ice crystals to determine the errors caused by non-spherical ice crystals measured by forward scattering probes. It is shown that the calculated errors in sizing nonspherical ice crystals are at least 13% and 26% in forward (4~12°) and backward (168~176°) directions, respectively, and maximum errors are up to 120% and 132%.

CMP Conditioner의 오염방지를 위한 V-SAM 공정개발과 박막특성 분석 (Development of V-SAM Process and Surface Characterization for Anti-contamination of CMP Conditioner)

  • 김동찬;김인권;김정;전종선;박문석;박진구
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2009년도 하계학술대회 논문집
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    • pp.56-56
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    • 2009
  • 반도체 device가 점점 고집적화, 다층화 되면서 막질의 평탄화를 위한 CMP (chemical mechanical planarization) 공정은 반도체 제작 공정에서 필수 요건이 되었다. 특히 pad conditioning은 CMP 공정 중, 막질의 제거율과 균일도를 유지시키기 위한 중요한 공정이다. 하지만, conditioner를 장시간 사용할 경우 slurry residue와 같은 잔류 오염물질들이 conditioner의 표면의 오염을 유발할 수 있고 이로 인해 conditioner의 수명이 단축되거나 웨이퍼 표면에 결함을 유발할 수도 있다. 본 연구에서는 이를 방지하기 위해 vapor SAM을 이용하여 Ni conditioner 표면에 소수성 박막을 증착하여 오염여부를 평가해 보았다. 먼저, Ni wafer를 이용하여 증착 온도와 압력에 따라 소수성 박막을 증착하여 표면특성을 평가해 보았다. 증착전과 후에 Ni wafer 표면의 접촉각은 contact angle analyzer (Phoenix 400, SEO, Korea)를 이용하여 측정하였다. 박막 표면 형상과 거칠기는 AFM (XE-100, PSIA, Korea)를 이용하여 평가되었고 묘면 성분 분석을 위해 FT-IR (Nicolet 6700, Thermo Scientific, USA)이 사용되었다. SEM (S-4800, Hitach, Japan)은 박막 증착 전과 후의 conditioner를 이용하여 실제 conditioning후 conditioner 표면의 particle 오염정도를 관찰하기 위해 사용되었다. 또한, conditioner 표면에 실제 오염되어있는 particle 개수를 평가하기 위해 particle size analyzer (Accusizer 780A, Particle Sizing Systems Co., USA)을 사용하였다. 본 실험을 통해 최적 증착 조건을 확립하였으며 실제 conditioner 표면에 소수성 박막을 증착 후 $100^{\circ}$ 이상의 높은 contact angle을 확인할 수 있었다. 또한, 소수성 박막이 증착된 conditioner의 경우 실제 conditioning후 표면 particle 오염이 현저히 감소되었음을 확인할 수 있었다.

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The simulation of the liberation and size distribution of shredder products under the material characteristic coding method

  • Ni, Shiuh-Sheng;Wen, Shaw-Bing;Chu, Chung-Cheng
    • 대한전자공학회:학술대회논문집
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    • 대한전자공학회 2001년도 The 6th International Symposium of East Asian Resources Recycling Technology
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    • pp.693-698
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    • 2001
  • This paper establishes a coding method system including the liberation and size distribution of recycling materials in the shredder operation. Every particle in the shredded product becomes a code number using the liberation model and size distribution equation transforming of weight percentage into particles number percentage. One set of database can be obtained after all particles have been coded. This database is suitable for the size reduction operation in the process simulation of waste recycling. Coupling with the developed air classification, sizing and separating operations, the whole process simulation will be completely established for diversified application. A typical simulation for the rolling cutting shredder product of waste TV had been demonstrated under this coding system. The breakage size distribution of Gaudin and Schumann equation were selected for the shredding operation simulation. The Gaudin's liberation model was suitable fur the liberation simulation. Both of these equations were transformed weight percentage into particles distribution for the necessary of particle coding method. A better recycling operation for this shredded solid waste can be concluded from the comparison of simulation results with their sorted grade, recovery or economic of materials in different processes.

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SCR 시스템의 요소용액 미립화 및 분해반응 특성 예측에 관한 전산 해석 연구 (A Research on the Characteristics of Spray-Induced Mixing and Thermal Decomposition of Urea Solution in SCR System)

  • 김주연;민병수;하지수;류승협
    • Journal of Advanced Marine Engineering and Technology
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    • 제28권5호
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    • pp.818-826
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    • 2004
  • The spray-induced mixing characteristics and thermal decomposition of aqueous urea solution into ammonia have been studied to design optimum sizes and geometries of the mixing chamber in SCR(Selective Catalytic Reduction) system. The cold flow tests about the urea-injection nozzle were performed to clarify the parameters of spray mixing characteristics such as mean diameter and velocity of drops and spray width determined from the interactions between incoming air and injected drops. Discrete particle model in Fluent code was adopted to simulate spray-induced mixing process and the experimental results on the spray characteristics were used as input data of numerical calculations. The simulation results on the spray-induced mixing were verified by comparing the spray width extracted from the digital images with the simulated Particle tracks of injected drops. The single kinetic model was adopted to predict thermal decomposition of urea solution into ammonia and solved simultaneously along with the verified spray model. The hot air generator was designed to match the flow rate and temperature of the exhaust gas of the real engines The measured ammonia productions in the hot air generator were compared with the numerical predictions and the comparison results showed good agreements. Finally, we concluded that the design capabilities for sizing optimum mixing chamber were established.

분무 유동에서 중첩 인자 분리 알고리즘의 개발 (Development of Separation Algorithm of Overlapped Particles in Spay Flow)

  • 양창조;김정환;조대환;오종환;이영호
    • 한국마린엔지니어링학회:학술대회논문집
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    • 한국마린엔지니어링학회 2005년도 후기학술대회논문집
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    • pp.118-119
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    • 2005
  • Recently, fire extinguishing systems based on water mists have been attracting public attentions in marine engineering. Performance of the fire extinguishing systems is influenced by the size and distribution of spayed water mists. Droplet analyzing method based on image processing technique for measuring droplet size and distribution has been developed. The morphological method based on partial curvature information of pre-processed images was adopted for recognition and separation of overlapped particles. Tested results show that the present method may be reliable for the analysis of the size and distribution of droplets produced by water mist spay flow.

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선박용 미분무 소화기노즐 수적 입자경 계측기법 개발

  • 김태형;김정환;양창조;오종환;최장운
    • 한국마린엔지니어링학회:학술대회논문집
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    • 한국마린엔지니어링학회 2006년도 전기학술대회논문집
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    • pp.307-308
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    • 2006
  • Recently, fire extinguishing systems based on water mists have been attracting public attentions in marine engineering. Performance of the fire extinguishing systems is influenced by the size and distribution of spayed water mists. Droplet analyzing method based on image processing technique for measuring droplet size and distribution has been developed. The morphological method based on partial curvature information of pre-processed images was adopted for recognition and separation of overlapped particles. Tested results show that the present method may be reliable for the analysis of the size and distribution of droplets produced by water mist spay flow.

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광학적 입자열 측정법에 의한 폴리스티렌구의 평균지름 측정 (Calibration of monodisperse polystylene spheres of size from 1 to 10 ${\mu}m$ by using optical array sizing method)

  • 강주식
    • 한국광학회지
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    • 제10권1호
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    • pp.21-26
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    • 1999
  • 광학적 입자열 측정법을 사용하여 공칭크기가 1, 2, 3, 5, 그리고 10$\mu$m인 플로스티렌 표준구의 평균지름을 측정하고 불확도를 분석하였다. 광학적 입자열 측정법이란, 슬라이드 글라스 위에 표준입자를 6각형 구조로 배열시킨 후, 입자열의 길이를 측정하고 이를 입자의 개수로 나누어 평균지름을 구하는 평균지름을 구하는 방법을 말하는데, 본 연구에서는 CCD 카메라와 화상처리를 도입함으로써 기존의 목측에 의한 측정방법보다 정확하고 편리하게 측정할 수 있도록 하였다. 입자열의 현미경 상을 CCD카메아로 얻은 후 소프트웨어 필터를 적용시켜 입자열의 길이를 화면의 픽셀단위로 측정하였으며, 이를 실제 길이로 환산하기 위해, 스템이지 마이크로미터의 현미경 상에 역시 필터를 적용시켜 구한 길이환산계수응 곱하였다. 이 길이를 입자열을 이루는 입자의 개수로 나누고, 공기층에 의한 입자의 찌그러짐 효과를 보정한 결과, 각 입자의 평균지름은 제조 회사의 인증값과 0.7% 이내로 일치하였며, 측정불확도는 1.5% 이내로 얻어졌다.

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A study on the efficacy of low viscous nanosized biopolymer on the mechanical and hydraulic properties of organic silt

  • Govindarajan Kannan;Evangelin Ramani Sujatha
    • Geomechanics and Engineering
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    • 제34권3호
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    • pp.221-231
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    • 2023
  • Biopolymer stabilization is a sustainable alternative to traditional techniques that cause a lesser negative impact on the environment during production and application. The study aims to minimize the biopolymer dosages by sizing the bio-additives to the nanoscale. This study combines the advantages of bio and nanomaterials in geotechnical engineering applications and attempts to investigate the behaviour of a low viscous biopolymer, nano sodium carboxymethyl cellulose (nCMC), to treat organic soil. Soil is treated with 0.25%, 0.50%, 0.75% and 1.00% of nano-bio additive, and its effect on the plastic behaviour, compaction characteristics, strength, hydraulic conductivity (HC) and compressible nature are investigated. The strength increased by 1.68 times after 90 days of curing at a dosage of 0.5% nCMC through the formation of gel threads connecting the soil particles that stiffened the matrix. The viscosity of 1% nCMC increased exponentially, deterring fluid flow through the voids and reduced the HC by 0.85 times after curing for 90 days. Also, beyond the optimum dosage of 0.50%, the nCMC forms a film around the soil particles that inhibits the inter-particle cohesion causing a reduction in strength. Experimental results show that nCMC can effectively substitute conventional additives to stabilize the soil.