• Title/Summary/Keyword: Partial-boiling

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Basic Study on the Heat Transfer During Rapid Freezing of Syobean Seed by Liquid Nitrogen

  • Kawano, Toshio;Nakano, Kohei;Murata, Satoshi
    • Proceedings of the Korean Society for Agricultural Machinery Conference
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    • 1993.10a
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    • pp.443-452
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    • 1993
  • Direct freezing tests of soybean seed by liquid nitrogen were carried out at various moisture contents and the following important conclusions were drawn from the results of temperature measurements of soybean seed and photographs of bubbles generated on its surface : 1) Assuming that the temperature gradient in a soybean seed is negligible because of its small seed size and the freezing ratio is followed the Heiss's formula, and a differential equation based on the heat energy balance was introduced . The equation was easily solved by the Runge-Kutta-Gill method and the predicted values of the temperature were in good agreement with the observed data. 2) The photographs of bubble generation during freezing showed the boiling mode was nucleate, and then the most suitable formula on the nucleate boiling heat transfer was introduced from many formulate proposed up to now by fitting the calculated values based on the formula to the observed data. The formula used for the predict on of the seed temperature was as follows: $\frac{{\partial}T_s}{\partial\theta}\;=\;-\frac{{\alpha}(T_s\;-\;T_L)^{3.3}}{W(C_s\;-\;\frac{{\delta}m(CT_s\;+\;{\sigma})}{T_s^2})}$ where C = difference of the specific heat between pure ice and water m=moisture content of soybean seed $T_s$ = seed temperature $T_L$ = Temperature of liquid nitrogen W = mass of soybean seed $\alpha$ = proportional constant $\delta$ = constant depends on variety or the type of seed $\theta$ = time $\sigma$ = latent heat of melting of pure ice This study will give important information in the hydro-freezing technique by liquid nitrogen, available as a new technique of processing agricultural products in the near future.

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한국산 도꼬마리 추출물의 항균효과 및 분리 정제

  • 김현수;신재욱
    • Microbiology and Biotechnology Letters
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    • v.25 no.2
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    • pp.183-188
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    • 1997
  • Antimicrobial activity of various extracts of Xanthium strumarium L. was tested against 25 strains of bacteria, yeast and fungus. The crude ethylacetate extract exhibited strong growth inhibition to the tested strains with the exception of partial Gram-negative bacteria. The property of antimicrobial compound was very stable under heat treatment at $120^{\circ}C$, but it was unstable in acid (pH 3.0) and alkali (pH 10.0) treatment. The antimicrobial compounds were purified by boiling water extraction, ethylacetate extraction, charcoal column chromatography, silica gel column chro- matography and reverse phase HPLC. The purified compound A and B were detected in a single peak (each above 98% purity) through the HPLC analysis. The compound A and B showed a strong growth inhibition against Gram-negative and positive bacteria in the agar diffusion method. When tested by the FDA method using the esterase, compound A mainly inhibited the growth of bacteria and compound B showed the growth inhibition of both bacteria and yeasts.

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A Study of PBD and BD Voltage Characteristics in the Simulate Electrode System of Solenoid Type High Temperature Superconducting Coils (솔레노이드형 고온초전도코일 모의전극계에서 부분 및 완전파괴전압특성 연구)

  • 석복렬
    • Progress in Superconductivity and Cryogenics
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    • v.4 no.1
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    • pp.94-98
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    • 2002
  • The Partial breakdown (PBD) and complete breakdown (BD) voltage characteristics in a composite insulation system of glass fiber reinforced plastics (GFRP) and liquid nitrogen are investigated to find the PBB and BD characteristics in solenoid type high temperature superconducting (HTS) coils at quench. The electrode system used is made from a coaxial spiral coil-to-cylindrical electrode with an insulation barrier and spacers, and is immersed in liquid nitrogen. A heater is mounted inside the coil electrode to generate boiling which occurs on quenched superconducting coils. The experimental results show that: (1) breakdown voltages are affected severely by the risetime of the applied voltage and the PBD inception voltage, (2) two kinds of BD mechanisms are found depending on the shape of the spacer, length of cooling channel and heater power.

Sensory Properties and Drivers of Liking Sanchae namul (seasoned dish with wild edible greens) (산채나물의 관능적 특성에 근거한 소비자 기호도 유도 인자 분석)

  • Yang, Jeong Eun;Lee, Ji Hyeon;Kim, Da Yoon;Choe, Eunok;Chung, Lana
    • Korean journal of food and cookery science
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    • v.30 no.2
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    • pp.200-211
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    • 2014
  • This study was conducted to identify the sensory characteristics of four kinds of wild vegetables (samnamul, miyeokchwi, daraesoon and bangpung namul), which were prepared through three different soaking methods: SBS (soaking both before and after boiling), BS (soaking only after boiling) and B (never soaking). Moreover, it also compared the consumer acceptance of these samples in Korea. A descriptive analysis was performed on 12 samples (Sam_SBS, Sam_BS, Sam_B, Miyeokchwi_SBS, Miyeokchwi_BS, Miyeokchwi_B, Daraesoon_SBS, Daraesoon_BS, Daraesoon_B, Bangpung_SBS, Bangpung_BS and Bangpung_B) by 10 trained panelists. Furthermore, 115 consumers evaluated the overall acceptance (OL), acceptance of appearance (APPL), odor (ODL), flavor (FLL), and texture (TXTL) of the samples using a 9-point hedonic scale; they also rated the perceived intensities of toughness, roughness and moistness using a 9-point just-about-right (JAR) scale. According to the results of the PLSR data, the Sam_SBS sample, which had significantly (p<0.05) high muddiness, moistness, brightness, redness, oily appearance, sesame oil flavor, softness and greasy attribute scores, presented the highest acceptability and consumer desire scores for consumers. On the other hand, the Miyeokchwi_B and Bangpung_B samples, which had relatively high toughness, crispiness, roughness, bitterness and, astringent attributes scores, were the least preferred samples. Therefore, the muddiness, moistness, brightness, oily appearance, sesame oil flavor, softness and greasy attributes were drivers of "liking," whereas toughness, crispiness, roughness, bitterness, astringent attributes acted as drivers of "disliking" for consumers.

Genetic Analysis on Quantitative Characters of Silkworm (Bombyx mori.) by Diallel Crosses (가잠의 이면교잡에 의한 유용 형질의 유전분석)

  • 정원복;이상풍
    • Journal of Sericultural and Entomological Science
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    • v.31 no.1
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    • pp.25-36
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    • 1989
  • In this experiment, gene action were analyzed for seven silkworm varieties in order to obtain basic information on their genetic improvement by diallel crosses. The results obtained were summarized as follows : In F1 generation, over-dominance was shown by Vr-Wr graphic analysis in four characters such as cocoon length in female, bave weight, cocoon weight and boiling off ratio in both male and female, and partial dominance in four characters such as fifth instar period, cocoon layer weight, cocoon layer ratio and bave length. In F2 generation, the partial dominance in all characters were obtained. Components of genetic variance analyzed for five characters such as fifth instar period, cocoon width, cocoon layer weight, cocoon layer ratio and fibroin contents in F1 generation, and for four characters such as cocoon width, cocoon layer weight, cocoon layer ratio and frbroin contents in F2 generation showed that addition effects were higher than dominant effects.

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Impurity profiling and chemometric analysis of methamphetamine seizures in Korea

  • Shin, Dong Won;Ko, Beom Jun;Cheong, Jae Chul;Lee, Wonho;Kim, Suhkmann;Kim, Jin Young
    • Analytical Science and Technology
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    • v.33 no.2
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    • pp.98-107
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    • 2020
  • Methamphetamine (MA) is currently the most abused illicit drug in Korea. MA is produced by chemical synthesis, and the final target drug that is produced contains small amounts of the precursor chemicals, intermediates, and by-products. To identify and quantify these trace compounds in MA seizures, a practical and feasible approach for conducting chromatographic fingerprinting with a suite of traditional chemometric methods and recently introduced machine learning approaches was examined. This was achieved using gas chromatography (GC) coupled with a flame ionization detector (FID) and mass spectrometry (MS). Following appropriate examination of all the peaks in 71 samples, 166 impurities were selected as the characteristic components. Unsupervised (principal component analysis (PCA), hierarchical cluster analysis (HCA), and K-means clustering) and supervised (partial least squares-discriminant analysis (PLS-DA), orthogonal partial least squares-discriminant analysis (OPLS-DA), support vector machines (SVM), and deep neural network (DNN) with Keras) chemometric techniques were employed for classifying the 71 MA seizures. The results of the PCA, HCA, K-means clustering, PLS-DA, OPLS-DA, SVM, and DNN methods for quality evaluation were in good agreement. However, the tested MA seizures possessed distinct features, such as chirality, cutting agents, and boiling points. The study indicated that the established qualitative and semi-quantitative methods will be practical and useful analytical tools for characterizing trace compounds in illicit MA seizures. Moreover, they will provide a statistical basis for identifying the synthesis route, sources of supply, trafficking routes, and connections between seizures, which will support drug law enforcement agencies in their effort to eliminate organized MA crime.

Improvement in the DNBR Modeling of RETRAN for Safety Analyses of Westinghouse Nuclear Power Plants

  • Cheong, Ae-Ju;Kim, Yo-Han
    • Nuclear Engineering and Technology
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    • v.34 no.6
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    • pp.596-609
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    • 2002
  • Korea Electric Power Research Institute has developed the in-house safety analysis methodologies for non-LOCA(Loss Of Coolant Accident) events based on codes and methodologies of vendors and Electric Power Research Institute . According to the new methodologies, analyses of system responses and calculation of DNBR(Departure from Nucleate Boiling Ratio) during the transient have been carried out with RETRAN code and a sub-channel analysis code, respectively. However, it takes too much time to calculate DNBR for each case using the two codes to search for the limiting case from sensitivity study. To simplify the search for the limiting case, accordingly, RETRAN code has been modified to roughly calculate DNBR using hot channel modeling. The W-3 correlation is already included in RETRAN as one of the auxiliary DNBR models. However, WRB-1 and WRB-2 correlations required to analyze some Westinghouse type fuels are not considered in RETRAN DNBR models. In this paper, the RETRAN DNBR models using the correlations have been developed and the partial and complete loss of forced reactor coolant flow events have been analyzed for Yonggwang units 1 and 2 with the new methodologies to validate the models. The results of the analyses have been compared with those mentioned in the chapter 15 of the Final Safety Analysis Report.

Utilization of Pyrolysis Oil from Pine Wood as Thermosetting Wood Adhesive Resins

  • Kim, Jae-Woo;Myers, Deland J.;Brown, Robert C.;Kuo, Monlin
    • Journal of the Korean Wood Science and Technology
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    • v.35 no.2
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    • pp.51-60
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    • 2007
  • In this study, the possibility of using pyrolysis oil as wood adhesives was explored. Especially, adhesives were formulated by reacting pyrolysis oil and formaldehyde and also partially replacing phenol with pyrolysis oil in phenol-formaldehyde (PF) adhesive and soy hydrolizate/PF adhesive formulation. The pine wood was fast pyrolyized and the oils were obtained from a series of condensers in the pyrolysis system. The oils from each condenser were first reacted with formaldehyde to explore potential use of the oil itself as adhesive. The lap-shear bond strength test results indicated that the oil itself could be polymerized and form bonds between wood adherends. The oils from each condenser were then mixed together and used as partial replacement of phenol (25, 33, and 50% by weight) in phenol-formaldehyde adhesive. The bond strength of the oil containing PF adhesives was decreased as percent phenol replacement level increased. However, no significant difference was found between 25 and 33% of phenol replacement level. The oil-contained PF resins at 25, 33, and 50% phenol replacement level with different NaOH/Phenol (Pyrolysis oil) molar ratio were further formulated with soy hydrolizate to make soy hydrolizate/pyrolysis oil-phenol formaldehyde adhesive at 6:4 weight (wt) ratio and used for fiberboard manufacturing. Surface internal bond strength (IB) of the boards bonded with 33% replacement at 0.3 NaOH/Phenol (Pyrolysis oil) molar ratio performed better than other replacement levels and molar ratios. Thickness swelling after 24 hr cold water soaking and after 2 hr in boiling water was increased as % replacement of pyrolysis oil increased.

Conditioned Medium from Dying Smooth Muscle Cell Induced Apoptotic Death

  • Bu, Moon-Hyun;Lee, Kyeong-Ah;Kim, Koan-Hoi;Rhim, Byung-Yong
    • The Korean Journal of Physiology and Pharmacology
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    • v.9 no.6
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    • pp.315-322
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    • 2005
  • In this study, the authors investigated whether death of vascular smooth muscle cell (VSMC) had a pathological pertinence. Conditioned media obtained from rat aorta smooth muscle cell (SMC) that were induced death by expressing FADD in the absence of tetracycline (FADD-SMC) triggered death of normal SMC. DNA fragmentation and caspase-3 activation were observed in dying SMC by conditioned media. FADD-SMC showed transcriptional activation of tumor necrosis factor $(TNF)-{\alpha}$. Conditioned medium contained $TNF-{\alpha}$, indicating secretion of the cytokine from dying FADD-SMC. It was investigated if secreted $TNF-{\alpha}$ was functional. Conditioned medium activated ERK and p38 MAPK pathways and induced MMP-9 expression, whereas depletion of the cytokine with its soluble receptor (sTNFR) remarkably inhibited induction of MMP-9 by conditioned medium. These findings suggest that $TNF-{\alpha}$ in conditioned medium seems to be active. Then, contribution of $TNF-{\alpha}$ on death-inducing activity of conditioned medium was examined. Depletion of $TNF-{\alpha}$ with soluble $TNF-{\alpha}$ receptor decreased the death activity of conditioned medium by 35%, suggesting that $TNF-{\alpha}$ play a partial role in the death activity. Boiling of medium almost completely abolished the death-inducing activity, suggesting that other heat labile death inducing proteins existed in conditioned medium. Taken together, these results indicate that SMC undergoing death could contribute to inflammation by expressing inflammatory cytokines and pathological complications by inducing death of neighboring cells.

A New Microassay for the Determination of Serum TBA (Thiobarbituric Acid) Value Enhanced by $FeCl_{3}$ under Anaerobic Condition (무산소상태에서 $FeCl_{3}$로 촉진된 Thiobarbituric Acid 반응을 이용한 혈청중 TBA 반응물의 새로운 정량법)

  • Lee, Joung-Won;Mo, Su-Mi;Lee, Tae-Young
    • Journal of Nutrition and Health
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    • v.17 no.1
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    • pp.31-40
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    • 1984
  • A new microassay was proposed for the determination of serum thiobarbituric acid(TBA) value greatly enhanced by ferric ion under anaerobic condition. One ${\mu}mole$ of $FeCl_{3}$ per $10{\mu}l$ of serum was added to the TBA reaction mixture containing serum protein precipitate. The reaction mixture was heated on boiling water-bath for 50min under $N_{2}$ flushing. The sensitivity of this assay was greatly enhanced by 40 times comparing with that of Yagi's method (1976). In favour of the enhancement, this test could be measured by colorimetry or spectrophotometry with the sample size of $10-20{\mu}l$ serum. The sensitivity and reproducibility were also improved by means of partial dehydration of the butanol extract with $(NH_{4})_{2}SO_{4}$ salting-out. Serum TBA values of healthy human at different age groups were determined by this proposed method.

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