• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2009.11a
• /
• pp.83-83
• /
• 2009

우수한 압전성을 가지는 PZT는 인체에 유해한 다량의 PbO을 함유하여 심각한 환경문제를 야기함은 물론 제조 공정 중 PbO 휘발 억제 시설 구비에 따른 경제적 부담 등 문제점이 지적되었다. 따라서 환경오염 및 가격경쟁력을 갖추기 위해 현재 무연 조성 세라믹스에 대한 많은 연구가 진행되고 있다. 최근 비납계 압전 세라믹의 연구는 비스무스 레이어형과 페로브스카이트 형 비납계 세라믹스의 연구가 활발히 진행되고 있다. 특히 $(Na,K)NbO_3$ 계는 페로브스카이트 구조를 가지는 비납계 세라믹으로 현재 많은 연구가 진행되고 있다. 이 물질은 PZT계와 유사하게 상전이(morphotropic phase boundary:MPB)영역을 가지고 있 으며 이 영역에서 높은 압전 특성을 보여주고 있다. 최근 $Na_{0.5}K_{0.5}NbO_3$에 $LiTaO_3$를 치환하여 우수한 압전 특성을 지니는 조성이 개발되고 있지만, 보통 소성법으로 제조된 세라믹스는 PZT계 세라믹스와 비교하여 특성이 떨어진다. 본 연구에서는 압전성이 우수한 $(Na_{0.44}K_{0.52}Li_{0.44})(Nb_{0.90}Sb_{0.06}Ta_{0.04})O_3$ 조성에 도너 도핑과 억셉터 도핑을 한 다음 전기기계결합계수, 압전상수, 유전상수의 변화를 평가하고, hardener 와 softener 특성이 본조성에서 나타나는지를 관찰하였다. 실험방법은 보통 소성법을 사용하였으며, 분쇄와 혼합은 직경 3 mm zirconia ball을 사용하여 볼밀 하였다. $850^{\circ}C$ 에서 5h 하소 후 $1100{\sim}1200^{\circ}C$ 에서 소결하고, 두께 1 mm로 연마한 다음 silver paste를 $650^{\circ}C$ 에서 소부하여 전극을 형성하였다. 제작된 시편은 $90^{\circ}C$의 실리콘유에서 3~4 kV/mm의 전계를 가해 20분간 분극 처리를 수행하였다. 제작된 시편의 압전전하 상수 값은 d33-meter(APC-8000)를 이용하여 측정하였고, 유전율, 전기기계결합계수 및 기계적품질계수 등은 임피던스 분석기 (impedance/gain phase analyzer)를 이용하여 특성을 측정 하였다. 또한 전압-분극 특성의 평가에는 강유전특성 측정기(ferroelectric tester: Precision-LC, Radiant Technologies, USA)를 이용하였다.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.29 no.10
• /
• pp.601-607
• /
• 2016

Piezoelectric thick films of soft $Pb(Zr,Ti)O_3$ (PZT) based commercial material (S55) were fabricated using a conventional tape casting method. Ag-Pd electrodes were printed on the piezoelectric film at room temperature and all 5 layered films with a dimension of $12mm{\times}16mm$ were successfully laminated for a multi-layered piezoelectric ceramic actuator. The laminated specimens were co-fired at $1,100^{\circ}C$ for 1 h. A flat layered and dense microstructure was obtained for the $112{\mu}m$ thick piezoelectric actuator after sintering process. Thereafter, a prototype piezoelectric speaker was fabricated using the multi-layered piezoelectric ceramic actuator which can operate as a bimorph. Its SPL (sound pressure level) characteristic was also evaluated for speaker application. Frequency response revealed that the output SPL with a root mean square voltage of 10 V increased gradually to the highest peak of 87.5 dB for 1.5 kHz and exhibited a relatively stable behavior over the measured frequency range (${\leq}20kHz$) at a distance of 10 cm, implying that the fabricated piezoelectric speaker is potential for speaker applications.

• Proceedings of the Korean Institute of Electrical and Electronic Material Engineers Conference
• /
• 2001.05c
• /
• pp.135-139
• /
• 2001

Contour vibration mode piezoelectric transformers were designed and fabricated to the square plate with size of $27.5{\times}27.5{\times}2.5(2.6,\;3.0)mm^3$ using PNW-PMN-PZT ceramics. Electrical characteristics of the piezoelectric transformer were investigated for fluorescent lamp ballast application. The electrical properties and characteristic temperature rise were measured using oscilloscope and infrared temperature sensor. A 28W fluorescent lamp was successfully driven by the fabricated transformers. After driving the lamp using Power Amplifier for 24 min, the output power, efficiency and characteristic temperature rise of PT2 piezoelectric transformer showed the appropriate values of 28.01 W, 99.43% and $11^{\circ}C$, respectively. The electronic ballast using PT2 piezoelectric transformer showed an excellent output power of 28.85 W and efficiency of 86.3%, respetively.

• Journal of Microbiology and Biotechnology
• /
• v.15 no.6
• /
• pp.1267-1272
• /
• 2005

The effects of coexpression of GroEL/ES and DnaK/DnaJ/GrpE chaperones on the productivity of the soluble form of human granulocyte colony stimulating factor (hG-CSF) in E. coli were examined. Recombinant hG-CSF protein was coexpressed with DnaK/DnaJ/GrpE or GroEL/ES chaperones under the control of the araB or Pzt-1 promoter, respectively. The optimal concentration of L-arabinose for the expression of DnaK/DnaJ/GrpE was found to be 1 mg/ml. When L-arabinose was added at $OD_{600}$=0.2 (early-exponential phase), soluble hG-CSF production was greatly increased. In addition, it was observed that the DnaK/DnaJ/GrpE and GroEL/ES chaperones had no synergistic effects on preventing aggregation of hG-CSF protein. Consequently, by coexpression of the DnaK/DnaJ/GrpE chaperone, the signal intensity of the hG-CSF protein band in the soluble fraction of cell lysate was increased from $3.5\%\;to\;13.9\%$, and Western blot analysis also revealed about a 4-5-fold increase of production of soluble hG-CSF over the non-induction case of DnaK/DnaJ/GrpE.

• Journal of the Korean Institute of Electrical and Electronic Material Engineers
• /
• v.11 no.11
• /
• pp.963-968
• /
• 1998

The stress distribution in multilayer piezoelectric ceramic actuators was investigated by Finite element analysis. The y direction stress was concentrated at electrode tip. The y direction maximum stress was decreased to 4.9$\times10^ 7 N/m^2$ with internal electrode gap(a) until 0.4 mm and was not much difference with external electrode thickness(c). The stress distribution with internal layers was almost same and the stress distribution of load condition was higher than that of no load condition The y direction maximum stress increased with the number of layer and saturated at 260 layers. In the case of defective actuator, the stress distribution was disconnected around the defect and larger than that of normal actuator.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.26 no.2
• /
• pp.283-290
• /
• 2002

In this paper, we consider the dynamic electromechanical behavior of an eccentric Yoffe permeable crack in a piezoelectric ceramic strip sandwiched between two elastic orthotropic materials under the combined anti-plane mechanical shear and in-plane electrical loadings. Fourier transforms are used to reduce the problem to the solution of two pairs of dual integral equations, which are then expressed to a Fredholm integral equation of the second kind. The initial crack propagation orientation for PZT-5H piezoceramics is predicted by maximum energy release rate criterion.

• Transactions of the Korean Society of Mechanical Engineers A
• /
• v.24 no.6 s.177
• /
• pp.1601-1607
• /
• 2000

Using the theory of linear piezoelectricity, we consider the problem of piezoelectric ceramic infinite strip containing a finite crack with free surface traction and surface charge under anti-plane shear. The crack is symmetrically parallel to the edges of infinite strip. Fourier transforms are used to reduce the problem to two pairs of dual integral equations, which are then expressed in terms of Fredholm integral equations of the second kind. Numerical results for PZT-5H ceramic are obtained and discussed.

• Proceedings of the KSME Conference
• /
• 2001.11a
• /
• pp.22-26
• /
• 2001

In this paper, we examine the steady state dynamic electromechanical behavior of an eccentric Yoffe crack in a piezoelectric ceramic layer bonded between two orthotropic elastic layers under the combined anti-plane mechanical shear and in-plane electrical loadings. We adopted permeable crack face condition. Numerical values on the dynamic energy release rate are obtained. The initial crack propagation orientation for PZT-5H piezoceramic is also predicted by maximum energy release rate criterion.

• Proceedings of the KSME Conference
• /
• 2001.06a
• /
• pp.304-309
• /
• 2001

In this paper, we consider the dynamic electromechanical behavior of an eccentric Yoffe permeable crack in a piezoelectric ceramic strip sandwiched between two elastic materials under the combined anti-plane mechanical shear and in-plane electrical loadings. Fourier transforms are used to reduce the problem to the solution of two pairs of dual integral equations, which are then expressed to a Fredholm integral equation of the second kind. The initial crack propagation orientation for PZT-5H piezoceramics is predicted by maximum energy release rate criterion.

• 제어로봇시스템학회:학술대회논문집
• /
• 2001.10a
• /
• pp.22.5-22
• /
• 2001

Robust control of a GFR composite beam with a distributed PVDF sensor and piezo-ceramic actuator is presented En this paper. Modal analysis method and modal coordinates are introduced to obtain the state educations of the structural system. 1st and 2nd natural frequencies are considered In the modeling, because robust control theory which is robustness to structured uncertainty is adopted to suppress the vibration. If the controllers designed by H$\^$$\infty$/ theory do not satisfy control performance, it is improved by ${\mu}$-synthesis method with D-K Iteration so that the ${\mu}$-controller based on the structured singular value satisfies the nominal performance and robust performance.