• 제목/요약/키워드: PZT Ceramics

검색결과 493건 처리시간 0.024초

Fabrication and Characterization of PZT Suspensions for Stereolithography based on 3D Printing

  • Cha, JaeMin;Lee, Jeong Woo;Bae, Byeonghoon;Lee, Seong-Eui;Yoon, Chang-Bun
    • 한국세라믹학회지
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    • 제56권4호
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    • pp.360-364
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    • 2019
  • PZT suspensions for photo-curable 3D printing were fabricated and their characteristics were evaluated. After mixing the PZT, photopolymer, photo-initiator, and dispersant for 10 min by using a high-shear mixer, the viscosity characteristics were investigated based on the powder content. To determine an appropriate dispersant content, the dispersant was mixed at 1, 3, and 5 wt% of the powder and a precipitation test was conducted for two hours. Consequently, it was confirmed that the dispersibility was excellent at 3 wt%. Through thermogravimetric analysis, it was confirmed that weight reduction occurred in the photopolymer between 120? and 500?, thereby providing a debinding heat treatment profile. The fabricated suspensions were cured using UV light, and the polymer was removed through debinding. Subsequently, the density and surface characteristics were analyzed by using the Archimedes method and field-emission scanning electron microscopy. Consequently, compared with the theoretical density, an excellent characteristic of 97% was shown at a powder content of 87 wt%. Through X-ray diffraction analysis, it was confirmed that the crystallizability improved as the solid content increased. At the mixing ratio of 87 wt% powder and 13 wt% photo-curable resin, the viscosity was 3,100 cps, confirming an appropriate viscosity characteristic as a stereolithography suspension for 3D printing.

Sol-gel법에 의한 $PbZrO_3-PbTiO_3-Pb(Ni_{1/3}Nb_{2/3})O_3$박막의 물리적 특성 (Physical properties of $PbZrO_3-PbTiO_3-Pb(Ni_{1/3}Nb_{2/3})O_3$ thin films by sol-gel method)

  • 임무열;구경완;김성일;유영각
    • E2M - 전기 전자와 첨단 소재
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    • 제9권10호
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    • pp.991-1000
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    • 1996
  • PbTiO$_{3}$-PbZrO$_{3}$-Pb(Ni$_{1}$3/Nb$_{2}$3/O$_{3}$) (PZT-PNN) thin films were prepared from corresponding metal organics partially stabilized with diethanolamine by the sol-gel spin coating method. Each mol ratio of PT:PZ:PNN solutions were #1(50:40:10), #2(50:30:20), #3(45:35:20), #4(40:40:20), #5(40:50:10), #6(35:45:20) and #7(30:50:20) respectively. The spin-coated PZT-PNN films were heat-treated at 350.deg. C for decomposition of residual organics, and were sintered from 450.deg. C to 750.deg. C for crystallization. The substrates, such as Pt and Pt/TiN/Ti/TiN/Si were used for the spin coating of PZT PNN films. The perovskite phase was observed in the PZT-PNN films heat-treated at 500.deg. C. The crystalline of the PZT-PNN films was optimized at the sintering of 700.deg. C. By the result of AES analysis, It is confirmed that the films of TiN/Ti/TiN was a good diffusion barrier and that co-diffusion into the each films was not observed.

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화재감지센서용 PZN-PSS-PZT계 초전재료의 전기적 특성에 미치는 Mn $O_2$ 첨가제의 영향 (Effect of Mn $O_2$ additive on the electrical characteristics of PZN-PSS-PZT Pyroelectric materials for the fire detactor)

  • 김용혁;백동현;최일수
    • 한국화재소방학회논문지
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    • 제9권2호
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    • pp.29-36
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    • 1995
  • In this study, the effect of Mn $O_2$ additive on the electrical characteristics of PZN-PSS-PZT Pyroelectric materials for the fire detactor was studies. PZT ceramics used this experimental is 4 composite system $[$Pb(Z $n_{1}$3/ N $b_{2}$3/) $O_3$+Pb(S $n_{1}$3/ S $b_{2}$3/) $O_3$+PbTi $O_3$+PbZr $O_3$$]$The dielectric constants and dissipation factors decreases as to Mn $O_2$ concentration increases. At the Mn $O_2$ 0.5($\omega$t%), Pyroelectric coefficient shows 8(10$^{-8C}$$\textrm{cm}^2$$^{\circ}C$) which have the highst value among other additive contents. It is found that output voltage shows maximum peck at Mn $O_2$0.7($\omega$t%) is associated with the higher pyroelectric coefficient and Lowered dielectric constant.t.

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NiO 및 $Cr_2O_3$를 첨가한 0.02PYW-0.98PZT계 세라믹의 압전특성에 관한 연구 (A study on the piezoelectric characteristic of 0.02PYW-0.98PZT system piezoelectric ceramics dopped with NiO, $Cr_2O_3$)

  • 김진섭;김현철;윤현상;배선기
    • 대한전기학회:학술대회논문집
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    • 대한전기학회 1999년도 하계학술대회 논문집 D
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    • pp.1789-1791
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    • 1999
  • In consideration of piezoelectric characteristic and Temperature stability, 3-element system dopped with NiO, $Cr_2O_3$ well-known as Hardner and Stabilizer whose primary element is PZT was eximanated its structure, piezoelectric characteristics, dopping with Nio, $Cr_2O_3$. We think that piezoelectric Characteristic is developed, remenent polarization and $E_c$ can developed in specimens by dopping with NiO, $Cr_2O_3$ additive. also, electromechanical quality factor largely showed tendency of decrement. According to dopping NiO, $Cr_2O_3$ more.

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압출가공방법에 의한 PZT세라믹스-고분자 압전복합재료의 제조 및 특성 연구 (Study on the Preparation of the Piezoelectric Composite Materials in PZT Ceramics-Polymers by Extrusion Method and its Properties)

  • 이덕출;김진수
    • 한국세라믹학회지
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    • 제27권1호
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    • pp.74-78
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    • 1990
  • In this study, to develope the ultrasonic transducer element, the extrusion method which is the processing technique of the piezoelectric composite materials is introduced, the connectivity of the piezoelectric composite materials is the 1-3 type, and we study the properties of the materials. The electromechanical coupling factor(kt) of the materials is above 0.6, the resonance property(fr) is the thickness mode in the frequency range of 0.5 to 2 [MHz] and the acoustic impedance(Zac) is about 5 to 7 [Maryl]. From these results, it is known that the piezoelectric composite materials manufactured byt he extrusion method will be able to develope the ultrasonic transducer elements.

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압전 바이몰프 액츄에이터의 진동에 따른 자가 발전특성 (Self Power Generation from Vibration using Piezoelectric Bimorph Actuator)

  • 김창일;정영훈;이영진;백종후;남산
    • 한국전기전자재료학회논문지
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    • 제21권12호
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    • pp.1071-1076
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    • 2008
  • This paper presents the self power generation from vibration using the piezoelectric bimorph actuator. The piezoelectric bimorph actuator was well developed with PZT-PNN-Fe piezoelectric ceramics. As the applied voltage was increased, a linear change of displacement was obtained with a relatively high ratio of 12.53 um/V for the bimorph actuator. Moreover, when the motor's rotational speed was 2000 rpm, the bimorph actuator, which has a resonance frequency of 68 Hz, exhibited the most efficient generation voltage of 10.4 V. This bimorph actuator could make the LED, emitting 60 mW, working successfully. Therefore, it is anticipated that the bimorph actuator will be useful as a power source for the next-generation electronic devices.

PPF 제어기법을 적용한 전기점성유체가 함유된 보의 진동제어 (Vibration Control of Beam Containing ER Fluid Using PPF Control Scheme)

  • 윤신일;진도훈;윤문철
    • 한국공작기계학회논문집
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    • 제14권3호
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    • pp.32-37
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    • 2005
  • Several types of smart materials and control scheme are available to adjust the structure actively in various external disturbances. A control scheme was introduced for a specific material. But the effectiveness of the control scheme has some limitation according to the choice of the smart materials and the response of the structure. The ER(Electrorheological) fluid is adequate for a large control force, and the PZT(lead zirconate titanate) patches are suitable for small but arbitrary control force at any point of the structure. It can be used for active control of structure by changing the dynamic characteristics of the structure. But it has some difficulty in suppressing the excited vibration in broad band. To compensate this resonance of the controlled structure, a hybrid controller was constructed using PPF(Positive position feedback) control with PZT and ER fluid control.

준강유전 BLZ-PZT 세라믹의 광변조특성 (Light modulation properties of the penferroelectric BLN-PZT ceramics)

  • 류기원;정장호;박인길;이영희
    • E2M - 전기 전자와 첨단 소재
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    • 제6권5호
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    • pp.454-460
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    • 1993
  • 본 연구에서는 준강유전 특성을 갖는 xBa(L $a_{1}$2/N $b_{1}$2/) $O_{3}$- (1-x)Pb(Z $r_{y}$ $Ti_{1-y}$) $O_{3}$ (x=8.5, 9.0[mol.%], y=65, 70[mol.%]) 세라믹을 2단 소성법으로 제작한 후, 조성 및 인가전계에 따른 전기광학 특성 및 광변조 특성을 측정하였다. 인가전계가 증가함에 따라 8.5/65/35 시편을 제외한 전조성에서 유효복굴절이 2차 함수적으로 변화하는 2차 전기광학 특성을 나타내었으며 2차 전기광학계수, 반파장전압 및 ON-OFF ratio는 9.0/65/35 시편에서 각각 6.17x$10^{-16}$[ $m^{2}$/ $v^{2}$], 136[V], 252의 가장 우수한 값을 나타내었다. 9.0/70/30, 9.0/65/35 및 8.5/70/30 시편에 대해 광변조 특성을 측정한 결과, 입사광의 세기를 인가전압에 의해 변조시킬 수 있음을 관찰하였다.다.

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저온소결 PCW-PMN-PZT 세라믹스를 적용한 압전변압기의 전기적 특성 (Electrical Characteristics of Piezoelectric Transformer using Low Temperature Sintering PCW-PMN-PZT Ceramics)

  • 정광현;류주현
    • 한국전기전자재료학회논문지
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    • 제19권4호
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    • pp.350-356
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    • 2006
  • In this study, piezoelectric transformer was manufactured at the sintering temperature of $950^{\circ}C$, and then the feasibility of application to low temperature sintering piezoelectric transformers was investigated by evaluating the electrical characteristics of it. The voltage ratio of piezoelectric transformer showed the maximum value at the resonant frequency of input part, and increased according to the increase of load resistance. The output power and efficiency of piezoelectric transformer showed the superior properties when the output impedance of it coincides with the load resistance. Piezoelectric transformer manufactured at the low temperature of $950^{\circ}C$ showed the heat generation less than $20^{\circ}C$ at the output power of 30 W, and stable driving characteristics.

PMB-PZT계 세라믹의 압전특성에 관한 연구 (A study on the piezoelectric characteristics of PMB-PZT ceramics)

  • 김현철;신혜경;김진섭;임인호;배선기
    • 한국전기전자재료학회:학술대회논문집
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    • 한국전기전자재료학회 2001년도 하계학술대회 논문집
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    • pp.806-808
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    • 2001
  • In this thesis, specimens was manufactured in general method annexing PMB-PZT system ceramic, and the following conclusion has been deduced. In XRD, the crystal structure of ceramic has the tetragonal structure which is close to rombohedral structure, and consequently the specimen characterized by MPB was manufactured. According to dopping with xPMB, electromechanical factor(kp) little is changed. kp was maximum value 23.37[%] at xPMB 0.03[mol%]. mechanical quality factor(Qm) was maximum value 237.04 at xPMB 0.03[mo1%].

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